loading system configuration loading override configuration from /home/nexmap/pkwi/mxtest/mctest/../mccodelib/mcxtrace-test/McXtrace_CPU_MPICC_KISS/mccode_config.json INFO: Using directory: "1" INFO: Using existing c-file: ./Test_SX.c INFO: Using existing binary: ./Test_SX.out INFO: === Simulation 'Test_SX' (/home/nexmap/pkwi/xTESTS/2023-02-01/McXtrace_CPU_MPICC_KISS_5e7/Test_SX/Test_SX.instr): running on 16 nodes (master is 'elearn1.fysik.dtu.dk', MPI version 3.1). Opening input file '/home/nexmap/pkwi/McXtrace/mcxtrace/3.x-dev/tools/Python/mxrun/../mccodelib/../../../data/Mo.lau' (Table_Read_Offset) Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46397e-09 l2=1.76356e-05 x=-4.92167e-05 y=0.00047888 z=-8.81696e-06 kx=5.17531e-05 ky=7.33211e-05 kz=1.64521 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.43175e-09 l2=3.85736e-06 x=4.99628e-05 y=-0.000149652 z=-1.934e-06 kx=0.000243868 ky=-0.000133268 kz=4.67133 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49264e-09 l2=2.02844e-05 x=4.89608e-05 y=-0.000185604 z=-1.01423e-05 kx=-6.59046e-05 ky=-3.14216e-06 kz=4.62437 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19372e-09 l2=2.46602e-05 x=4.84556e-05 y=-0.00045724 z=-1.23323e-05 kx=2.02142e-05 ky=-3.402e-05 kz=0.608373 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13391e-09 l2=1.66375e-05 x=4.9303e-05 y=0.000276824 z=-8.3205e-06 kx=0.000105588 ky=0.000282133 kz=4.37302 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.0225e-09 l2=1.07025e-05 x=-4.97131e-05 y=-0.000306795 z=-5.35188e-06 kx=9.10151e-05 ky=-0.000198862 kz=5.14215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32336e-09 l2=1.44231e-05 x=-4.9477e-05 y=-0.000142222 z=-7.21423e-06 kx=-0.000210638 ky=-7.56282e-05 kz=5.14596 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08697e-09 l2=3.915e-05 x=4.60088e-05 y=-0.000283112 z=-1.95763e-05 kx=3.94785e-05 ky=-1.86396e-05 kz=2.38636 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10223e-09 l2=1.49532e-05 x=-4.94378e-05 y=0.000459194 z=-7.47801e-06 kx=-8.13462e-05 ky=0.000258129 kz=4.69844 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03573e-09 l2=2.27852e-05 x=-4.86849e-05 y=0.000427203 z=-1.13933e-05 kx=-2.57807e-05 ky=0.000304093 kz=6.00296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03878e-09 l2=1.53332e-05 x=4.94086e-05 y=0.000369042 z=-7.66854e-06 kx=2.57512e-05 ky=7.91617e-06 kz=0.900583 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57355e-09 l2=1.26796e-05 x=-4.95966e-05 y=-0.000268442 z=-6.3401e-06 kx=6.38001e-05 ky=-0.000280839 kz=6.21603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19227e-09 l2=2.2762e-05 x=-4.86876e-05 y=-0.000313882 z=-1.1382e-05 kx=-1.76999e-05 ky=-1.60315e-05 kz=2.39446 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30692e-09 l2=1.79284e-05 x=4.91898e-05 y=0.000482408 z=-8.96561e-06 kx=0.00010457 ky=0.000520728 kz=6.71286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37034e-09 l2=1.70697e-05 x=4.92661e-05 y=0.000150544 z=-8.53653e-06 kx=0.00014097 ky=5.23076e-05 kz=6.97842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67453e-09 l2=1.66867e-05 x=4.92991e-05 y=-0.000223174 z=-8.34515e-06 kx=6.52872e-05 ky=-0.000469398 kz=6.77954 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.65535e-09 l2=1.6462e-05 x=4.93183e-05 y=0.000225782 z=-8.23088e-06 kx=-0.000128215 ky=9.96465e-05 kz=4.37651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51276e-09 l2=1.09676e-05 x=-4.96984e-05 y=0.000468512 z=-5.48515e-06 kx=-7.64374e-06 ky=2.31352e-05 kz=0.658371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28449e-09 l2=1.97054e-05 x=-4.90202e-05 y=-6.17802e-05 z=-9.85136e-06 kx=2.38059e-05 ky=-1.82288e-05 kz=0.582984 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.93284e-09 l2=1.39205e-06 x=4.99952e-05 y=-0.000351572 z=-6.99931e-07 kx=-6.22397e-05 ky=3.05603e-05 kz=5.53016 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14371e-09 l2=2.77382e-05 x=-4.80381e-05 y=0.00017527 z=-1.38698e-05 kx=-8.89096e-06 ky=0.000147962 kz=3.46623 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01947e-09 l2=1.55749e-05 x=-4.93902e-05 y=-7.56325e-05 z=-7.78593e-06 kx=0.000199348 ky=0.000177415 kz=4.89132 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71984e-09 l2=1.82729e-05 x=4.91585e-05 y=0.000336768 z=-9.13652e-06 kx=-1.32862e-05 ky=2.0614e-05 kz=0.816001 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11859e-09 l2=3.31043e-05 x=-4.71805e-05 y=-0.000468535 z=-1.65541e-05 kx=-0.000171916 ky=-0.000209177 kz=5.73864 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15001e-09 l2=3.48152e-05 x=-4.68713e-05 y=4.21379e-05 z=-1.74104e-05 kx=-0.000167055 ky=5.99819e-05 kz=3.46544 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30622e-09 l2=1.6822e-05 x=4.92875e-05 y=0.00043209 z=-8.41212e-06 kx=1.59453e-05 ky=-4.45796e-06 kz=1.7712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14322e-09 l2=2.9145e-05 x=4.78293e-05 y=0.000335743 z=-1.45738e-05 kx=3.36165e-05 ky=0.00010151 kz=2.13355 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10778e-09 l2=1.17672e-05 x=4.96528e-05 y=0.000394757 z=-5.8841e-06 kx=-6.80025e-05 ky=0.000233364 kz=6.2399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17453e-09 l2=3.07998e-05 x=-4.75696e-05 y=-6.40136e-05 z=-1.54004e-05 kx=1.84939e-05 ky=1.06333e-07 kz=6.53623 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09234e-09 l2=2.22903e-05 x=4.87426e-05 y=0.000486982 z=-1.11437e-05 kx=-6.47415e-05 ky=6.18809e-05 kz=1.54816 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42425e-09 l2=2.51976e-05 x=4.83871e-05 y=0.00018543 z=-1.25986e-05 kx=-8.44659e-05 ky=0.000252635 kz=4.3636 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32459e-09 l2=2.05159e-05 x=4.89369e-05 y=0.000318577 z=-1.02572e-05 kx=-0.000101902 ky=0.000143176 kz=3.60015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80266e-09 l2=1.36489e-05 x=4.95322e-05 y=-3.87262e-05 z=-6.82569e-06 kx=1.05159e-05 ky=4.76878e-05 kz=1.4617 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30769e-09 l2=3.68716e-05 x=4.64782e-05 y=-0.000420009 z=-1.84344e-05 kx=-8.34751e-05 ky=1.16741e-05 kz=1.86606 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29364e-09 l2=1.39663e-05 x=4.95099e-05 y=-0.000158169 z=-6.98473e-06 kx=2.76904e-05 ky=-3.50316e-05 kz=1.4818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5233e-09 l2=9.33842e-06 x=-4.97818e-05 y=3.60986e-05 z=-4.66961e-06 kx=4.0902e-05 ky=2.02024e-05 kz=1.49686 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06661e-09 l2=1.94091e-05 x=4.90489e-05 y=0.000436724 z=-9.70683e-06 kx=0.000205269 ky=7.25938e-05 kz=5.8014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17308e-09 l2=3.68265e-05 x=4.64856e-05 y=0.000454481 z=-1.84156e-05 kx=0.000121024 ky=0.00030115 kz=3.21659 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67449e-09 l2=9.76902e-06 x=4.97608e-05 y=0.000195192 z=-4.88733e-06 kx=0.000142253 ky=8.6748e-05 kz=4.78915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14454e-09 l2=2.71713e-05 x=4.81195e-05 y=-0.000416159 z=-1.35849e-05 kx=-0.000127924 ky=-6.58931e-05 kz=4.58685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13991e-09 l2=1.42858e-05 x=-4.9487e-05 y=6.77764e-05 z=-7.14492e-06 kx=-0.000123575 ky=7.25037e-05 kz=4.18038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14207e-09 l2=2.63571e-05 x=-4.82315e-05 y=-0.000392417 z=-1.31816e-05 kx=-0.000174014 ky=-9.1996e-05 kz=3.386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.96766e-09 l2=4.09609e-06 x=-4.99581e-05 y=-0.000477717 z=-2.05157e-06 kx=-0.000106258 ky=-0.000288876 kz=3.4343 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25453e-09 l2=2.23642e-05 x=-4.87338e-05 y=-0.000128414 z=-1.11832e-05 kx=2.88122e-07 ky=2.07563e-05 kz=1.76397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32459e-09 l2=2.05159e-05 x=4.89369e-05 y=0.000318577 z=-1.02572e-05 kx=-0.000101902 ky=0.000143176 kz=3.60015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29364e-09 l2=1.39663e-05 x=4.95099e-05 y=-0.000158169 z=-6.98473e-06 kx=2.76904e-05 ky=-3.50316e-05 kz=1.4818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05412e-09 l2=2.94482e-05 x=-4.77826e-05 y=-8.19818e-05 z=-1.47259e-05 kx=-4.50357e-05 ky=-8.67624e-05 kz=1.69241 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18165e-09 l2=3.6998e-05 x=4.6453e-05 y=-7.18615e-06 z=-1.84977e-05 kx=-8.92809e-05 ky=-4.23242e-05 kz=2.13657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33711e-09 l2=2.06227e-05 x=-4.89258e-05 y=-0.000278953 z=-1.03101e-05 kx=0.000193012 ky=-0.000157726 kz=4.87222 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18068e-09 l2=3.24381e-05 x=-4.72971e-05 y=0.00040555 z=-1.62179e-05 kx=0.00019534 ky=0.000332155 kz=5.14822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23284e-09 l2=3.00226e-05 x=4.76937e-05 y=0.000115299 z=-1.50115e-05 kx=-5.93333e-05 ky=2.43541e-05 kz=7.00911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.29191e-09 l2=8.30211e-06 x=4.98276e-05 y=0.000225707 z=-4.15133e-06 kx=-5.34411e-05 ky=4.1016e-05 kz=1.94781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.48867e-09 l2=1.35608e-05 x=-4.95386e-05 y=8.07899e-05 z=-6.77948e-06 kx=0.000254792 ky=5.19271e-05 kz=5.88114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80716e-09 l2=1.24323e-05 x=4.96122e-05 y=0.000492232 z=-6.21715e-06 kx=1.17427e-05 ky=0.000164331 kz=5.16107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88891e-09 l2=1.3584e-05 x=-4.95367e-05 y=-0.000230022 z=-6.7926e-06 kx=4.01757e-05 ky=-0.000153574 kz=5.46986 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49199e-09 l2=7.4358e-06 x=-4.98618e-05 y=0.000365729 z=-3.71692e-06 kx=0.000238532 ky=0.000526397 kz=6.9196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21382e-09 l2=4.73654e-06 x=-4.99438e-05 y=-0.000126864 z=-2.37048e-06 kx=-0.000218752 ky=-0.000207145 kz=6.83209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.78871e-09 l2=3.15143e-06 x=-4.99752e-05 y=0.000433698 z=-1.57841e-06 kx=-8.90545e-05 ky=0.000458232 kz=5.58963 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54341e-09 l2=2.45561e-05 x=-4.84696e-05 y=0.000330257 z=-1.22774e-05 kx=0.000104226 ky=0.000152604 kz=3.57443 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0328e-09 l2=1.1392e-05 x=-4.96746e-05 y=-0.000427914 z=-5.69646e-06 kx=8.3065e-06 ky=-0.000108215 kz=5.48773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14236e-09 l2=3.22149e-05 x=4.73341e-05 y=-0.000490142 z=-1.61096e-05 kx=0.000149399 ky=-0.000173638 kz=4.45317 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42913e-09 l2=1.64648e-05 x=-4.93174e-05 y=0.00021424 z=-8.23521e-06 kx=-3.01683e-06 ky=8.19798e-07 kz=0.0705517 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.401e-09 l2=7.91048e-06 x=-4.98436e-05 y=0.000392499 z=-3.95453e-06 kx=2.2232e-05 ky=1.96152e-05 kz=0.578787 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2488e-09 l2=3.71946e-05 x=4.64125e-05 y=0.000333921 z=-1.85992e-05 kx=5.00016e-05 ky=7.94092e-05 kz=1.86454 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.96631e-09 l2=1.04478e-05 x=-4.97266e-05 y=0.000251799 z=-5.22415e-06 kx=2.60068e-05 ky=1.79625e-05 kz=1.06298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05525e-09 l2=1.57886e-05 x=-4.93727e-05 y=-0.000380313 z=-7.89612e-06 kx=-7.76674e-05 ky=-0.000193763 kz=2.9795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21873e-09 l2=4.60611e-06 x=-4.9947e-05 y=-0.000263582 z=-2.30516e-06 kx=-1.37326e-05 ky=-3.23751e-05 kz=1.3937 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09049e-09 l2=1.72614e-05 x=-4.92492e-05 y=-0.0002356 z=-8.63344e-06 kx=-0.000112763 ky=-0.000179191 kz=2.50531 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7153e-09 l2=2.36117e-05 x=-4.85863e-05 y=-0.000408847 z=-1.18074e-05 kx=-2.96597e-05 ky=-7.06128e-05 kz=2.0629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24104e-09 l2=1.25152e-05 x=-4.96067e-05 y=2.86582e-05 z=-6.2614e-06 kx=-0.000377966 ky=-5.51196e-06 kz=7.03074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34211e-09 l2=3.51171e-05 x=4.68155e-05 y=6.48788e-05 z=-1.75602e-05 kx=0.000100311 ky=0.000174447 kz=4.78053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64407e-09 l2=2.29055e-06 x=4.9987e-05 y=0.000403237 z=-1.14388e-06 kx=-0.000264159 ky=0.000532308 kz=5.97149 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05525e-09 l2=1.57886e-05 x=-4.93727e-05 y=-0.000380313 z=-7.89612e-06 kx=-7.76674e-05 ky=-0.000193763 kz=2.9795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96222e-09 l2=2.13416e-05 x=-4.88481e-05 y=0.000391909 z=-1.06725e-05 kx=-6.90174e-05 ky=0.000114883 kz=4.78537 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29682e-09 l2=4.24507e-06 x=4.9955e-05 y=0.000450572 z=-2.12172e-06 kx=-3.15582e-05 ky=8.03655e-05 kz=1.08 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.08395e-09 l2=2.99853e-05 x=4.77e-05 y=-0.00015538 z=-1.49924e-05 kx=-0.000185969 ky=-9.26468e-05 kz=6.57074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05477e-09 l2=2.22228e-05 x=-4.87498e-05 y=-0.000457492 z=-1.1112e-05 kx=-3.36466e-06 ky=-8.58397e-05 kz=2.66366 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84809e-09 l2=7.04732e-06 x=-4.98756e-05 y=-2.50206e-05 z=-3.52652e-06 kx=-3.82903e-05 ky=-4.9881e-06 kz=0.986078 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2266e-09 l2=1.1866e-05 x=-4.96466e-05 y=0.000222945 z=-5.93504e-06 kx=-6.19482e-05 ky=-4.05286e-05 kz=2.14809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33283e-09 l2=1.73288e-05 x=4.92436e-05 y=-0.000126857 z=-8.66557e-06 kx=4.47306e-05 ky=-0.000169388 kz=4.45367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43053e-09 l2=2.41951e-05 x=4.85142e-05 y=0.0004797 z=-1.21e-05 kx=0.000146383 ky=5.57415e-05 kz=4.04408 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10065e-09 l2=1.20879e-05 x=-4.96335e-05 y=0.000345989 z=-6.04483e-06 kx=4.99351e-06 ky=3.49123e-06 kz=1.50082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29125e-09 l2=2.99128e-05 x=4.77106e-05 y=4.70824e-05 z=-1.49578e-05 kx=0.000104602 ky=0.000189277 kz=6.48796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.51907e-09 l2=3.42025e-06 x=4.99707e-05 y=0.000363285 z=-1.71468e-06 kx=0.0002573 ky=0.000358873 kz=5.61089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07849e-09 l2=1.73413e-05 x=4.92424e-05 y=-0.000109344 z=-8.67201e-06 kx=2.54392e-05 ky=3.17454e-05 kz=1.49706 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79922e-09 l2=2.18031e-05 x=4.87973e-05 y=-1.54942e-05 z=-1.09025e-05 kx=3.25622e-07 ky=3.57199e-05 kz=1.62945 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.92753e-09 l2=1.25114e-06 x=4.99961e-05 y=-0.000190215 z=-6.28951e-07 kx=-1.36313e-05 ky=1.06581e-05 kz=1.1673 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03675e-09 l2=4.34233e-05 x=-4.50404e-05 y=-0.000155734 z=-2.17118e-05 kx=3.40998e-05 ky=-0.000107047 kz=4.46316 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22038e-09 l2=1.86045e-05 x=4.91271e-05 y=0.000334514 z=-9.30325e-06 kx=4.64978e-05 ky=0.000411655 kz=5.98018 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01339e-09 l2=1.28752e-05 x=4.9584e-05 y=-0.000451188 z=-6.43712e-06 kx=-2.46495e-06 ky=-4.34305e-06 kz=0.12711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17658e-09 l2=2.99858e-05 x=-4.76994e-05 y=0.000108692 z=-1.49934e-05 kx=1.57889e-05 ky=0.000323324 kz=5.93156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14473e-09 l2=1.69458e-05 x=4.92773e-05 y=-9.02541e-05 z=-8.47133e-06 kx=-0.000130796 ky=-5.39785e-05 kz=2.99603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18768e-09 l2=2.13089e-05 x=-4.88521e-05 y=-0.000299746 z=-1.06537e-05 kx=6.87791e-05 ky=-7.45853e-05 kz=2.4473 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04045e-09 l2=1.17726e-05 x=-4.96524e-05 y=0.000275879 z=-5.88628e-06 kx=3.4767e-05 ky=6.58252e-05 kz=3.15487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43053e-09 l2=2.41951e-05 x=4.85142e-05 y=0.0004797 z=-1.21e-05 kx=0.000146383 ky=5.57415e-05 kz=4.04408 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11942e-09 l2=2.79377e-05 x=4.80085e-05 y=-6.69077e-05 z=-1.39719e-05 kx=0.00035622 ky=-0.000249693 kz=6.88975 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5199e-09 l2=1.33922e-05 x=4.95493e-05 y=0.000373482 z=-6.69955e-06 kx=0.000262072 ky=0.000171209 kz=4.86165 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34974e-09 l2=9.85332e-06 x=-4.9757e-05 y=-0.000430711 z=-4.92561e-06 kx=8.49134e-05 ky=-3.591e-05 kz=1.89988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.41179e-09 l2=7.79569e-06 x=4.98478e-05 y=-0.000296714 z=-3.90126e-06 kx=7.71928e-05 ky=1.53961e-05 kz=1.74244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.99124e-09 l2=7.76331e-06 x=-4.98494e-05 y=-0.000333603 z=-3.88228e-06 kx=9.62788e-05 ky=-0.000150106 kz=3.50302 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16236e-09 l2=1.94546e-05 x=-4.90448e-05 y=0.000469545 z=-9.72801e-06 kx=-1.15576e-05 ky=0.000109779 kz=4.73723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43542e-09 l2=1.62733e-05 x=-4.93339e-05 y=3.47547e-05 z=-8.13585e-06 kx=2.71904e-05 ky=4.58212e-05 kz=0.86767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09385e-09 l2=2.29922e-05 x=-4.86608e-05 y=0.000334082 z=-1.14956e-05 kx=7.1461e-05 ky=0.00015051 kz=3.30485 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63246e-09 l2=6.00047e-06 x=4.991e-05 y=-0.000145335 z=-3.00056e-06 kx=-2.97926e-05 ky=3.09168e-05 kz=1.50082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34974e-09 l2=9.85332e-06 x=-4.9757e-05 y=-0.000430711 z=-4.92561e-06 kx=8.49134e-05 ky=-3.591e-05 kz=1.89988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02251e-09 l2=8.16022e-06 x=4.98332e-05 y=-0.000485972 z=-4.08227e-06 kx=2.23362e-05 ky=-4.12054e-05 kz=0.674763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20298e-09 l2=8.23746e-06 x=4.98302e-05 y=-0.000234232 z=-4.11868e-06 kx=-3.93175e-05 ky=6.99396e-05 kz=2.99627 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09223e-09 l2=9.55273e-06 x=-4.97714e-05 y=-9.31582e-05 z=-4.77673e-06 kx=2.08975e-05 ky=-1.75233e-05 kz=5.67315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04535e-08 l2=4.11982e-06 x=4.99577e-05 y=0.000326365 z=-2.06611e-06 kx=5.78305e-05 ky=0.000110498 kz=2.97044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01583e-09 l2=2.01158e-05 x=4.89776e-05 y=-0.00012751 z=-1.00607e-05 kx=0.000287542 ky=-0.000212202 kz=6.18653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08855e-09 l2=4.49246e-05 x=-4.46716e-05 y=-0.000489977 z=-2.24609e-05 kx=0.000221871 ky=-0.00043826 kz=5.19141 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27268e-09 l2=2.36422e-05 x=-4.85824e-05 y=0.000370017 z=-1.18227e-05 kx=-1.90944e-05 ky=9.93253e-06 kz=0.960251 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39276e-09 l2=9.78394e-06 x=4.976e-05 y=-0.000173397 z=-4.89414e-06 kx=5.12905e-05 ky=-0.000114806 kz=1.72767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43022e-09 l2=3.53633e-05 x=4.67699e-05 y=6.59239e-05 z=-1.76813e-05 kx=-7.33604e-05 ky=0.000164953 kz=3.26822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00783e-09 l2=3.86109e-05 x=-4.6122e-05 y=0.000237398 z=-1.93081e-05 kx=-1.33084e-05 ky=6.28619e-06 kz=0.28911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29259e-09 l2=1.53156e-05 x=-4.94101e-05 y=0.000482464 z=-7.65926e-06 kx=-9.04139e-05 ky=0.000500021 kz=5.41796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31186e-09 l2=1.14697e-05 x=4.967e-05 y=0.00038014 z=-5.73676e-06 kx=0.000174579 ky=0.000381906 kz=6.90194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6454e-09 l2=2.31767e-05 x=-4.8639e-05 y=0.000259712 z=-1.15882e-05 kx=0.000125344 ky=-0.000137287 kz=6.50456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.83505e-09 l2=5.48684e-06 x=-4.99249e-05 y=-0.000480111 z=-2.74757e-06 kx=2.46842e-06 ky=-3.50887e-06 kz=0.456553 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03266e-09 l2=5.75694e-05 x=-4.08828e-05 y=-0.000234833 z=-2.87863e-05 kx=-0.000190459 ky=-0.000354439 kz=6.94323 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19491e-09 l2=2.01251e-05 x=4.89771e-05 y=0.0004609 z=-1.00633e-05 kx=8.91267e-06 ky=3.57849e-05 kz=3.37197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61889e-09 l2=1.28237e-05 x=4.9587e-05 y=-0.000359462 z=-6.41493e-06 kx=4.53959e-05 ky=-1.76989e-05 kz=1.00298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50981e-09 l2=2.3401e-05 x=-4.8612e-05 y=-0.000133996 z=-1.1701e-05 kx=3.31605e-05 ky=-0.000154221 kz=5.95885 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43935e-09 l2=3.02671e-05 x=-4.76546e-05 y=-4.78686e-05 z=-1.51355e-05 kx=-0.000134384 ky=0.000149136 kz=4.97274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23667e-09 l2=3.88674e-05 x=4.60691e-05 y=-0.000294983 z=-1.94341e-05 kx=-2.70086e-05 ky=-0.000279684 kz=6.7491 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24196e-09 l2=3.74904e-05 x=4.63534e-05 y=-0.000129294 z=-1.8746e-05 kx=2.10382e-05 ky=4.37945e-05 kz=6.54022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.99466e-09 l2=1.32981e-05 x=-4.95565e-05 y=0.0002314 z=-6.64908e-06 kx=1.67752e-05 ky=1.81986e-06 kz=0.420913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04541e-09 l2=2.83747e-05 x=-4.79456e-05 y=7.01794e-05 z=-1.41864e-05 kx=0.000195 ky=0.000255671 kz=6.23368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.94747e-09 l2=1.92903e-05 x=4.90609e-05 y=-0.000262938 z=-9.64729e-06 kx=0.000105028 ky=-0.000309 kz=4.36133 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07049e-09 l2=2.3122e-05 x=4.86454e-05 y=7.46427e-05 z=-1.15608e-05 kx=-3.483e-05 ky=-6.37477e-05 kz=2.26351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33843e-09 l2=1.66944e-05 x=4.92981e-05 y=-4.18317e-05 z=-8.34986e-06 kx=0.000217665 ky=-0.000229915 kz=5.3924 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33981e-09 l2=1.33734e-05 x=4.95506e-05 y=-0.000318939 z=-6.68972e-06 kx=0.000164486 ky=6.11708e-05 kz=3.43003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.48791e-09 l2=8.98452e-06 x=-4.9798e-05 y=-0.000323658 z=-4.49228e-06 kx=8.88441e-05 ky=-5.1133e-05 kz=3.62355 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22008e-09 l2=2.10334e-05 x=4.88816e-05 y=-3.35516e-05 z=-1.05175e-05 kx=1.77031e-05 ky=0.000200246 kz=5.42812 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.40785e-09 l2=7.36204e-06 x=4.98643e-05 y=-0.000245035 z=-3.68414e-06 kx=0.000150755 ky=-5.4761e-05 kz=3.91501 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74751e-09 l2=1.76657e-05 x=4.92136e-05 y=-0.000238235 z=-8.83446e-06 kx=9.23173e-05 ky=-0.000360261 kz=5.95634 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05508e-09 l2=4.69347e-05 x=4.41515e-05 y=-3.66131e-05 z=-2.3467e-05 kx=-8.98647e-05 ky=0.000108101 kz=4.39327 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01288e-09 l2=1.12276e-05 x=-4.96839e-05 y=-0.000348541 z=-5.61563e-06 kx=-5.22753e-05 ky=-0.000134097 kz=3.17476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30221e-09 l2=3.05768e-05 x=-4.76059e-05 y=-0.000141097 z=-1.52879e-05 kx=0.000146858 ky=4.72554e-05 kz=5.76635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.80672e-09 l2=8.82822e-06 x=-4.9805e-05 y=-0.000168448 z=-4.41486e-06 kx=8.45414e-05 ky=-0.00010693 kz=6.49387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84374e-09 l2=2.48016e-05 x=4.84382e-05 y=0.000340067 z=-1.24012e-05 kx=-7.51374e-05 ky=2.46089e-05 kz=6.52234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21019e-09 l2=2.06322e-05 x=-4.89245e-05 y=0.000484756 z=-1.03161e-05 kx=2.85999e-05 ky=8.78044e-05 kz=2.23116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09189e-09 l2=2.14281e-05 x=-4.88384e-05 y=0.0003308 z=-1.07169e-05 kx=-0.000156997 ky=0.000343431 kz=4.29249 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.88876e-09 l2=1.16581e-05 x=4.96594e-05 y=-3.70461e-05 z=-5.83012e-06 kx=-1.44386e-05 ky=2.63768e-05 kz=0.835963 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04203e-09 l2=4.22398e-05 x=4.53204e-05 y=0.000221945 z=-2.11212e-05 kx=7.38478e-05 ky=-1.07295e-05 kz=4.02879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33374e-09 l2=2.4762e-05 x=4.84433e-05 y=-0.000442742 z=-1.23815e-05 kx=-5.80821e-05 ky=-5.90122e-05 kz=4.18644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.3382e-09 l2=7.34903e-06 x=-4.9865e-05 y=0.000168123 z=-3.67563e-06 kx=7.48665e-05 ky=-7.97579e-05 kz=3.53039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23786e-09 l2=2.60602e-05 x=-4.82719e-05 y=0.000314304 z=-1.30328e-05 kx=-0.000157124 ky=0.000100217 kz=3.6443 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3928e-09 l2=2.34203e-05 x=-4.86099e-05 y=0.000491449 z=-1.17092e-05 kx=2.30648e-05 ky=5.55283e-05 kz=0.678668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28555e-09 l2=1.90359e-05 x=-4.90862e-05 y=-0.00040548 z=-9.51677e-06 kx=0.00018657 ky=-0.000283097 kz=5.03103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75809e-09 l2=1.56534e-05 x=-4.9384e-05 y=0.000345626 z=-7.82586e-06 kx=0.000114608 ky=7.88068e-05 kz=3.27258 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00275e-09 l2=2.87013e-05 x=-4.78967e-05 y=2.78098e-05 z=-1.43504e-05 kx=7.29772e-05 ky=-2.70863e-05 kz=4.79152 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2886e-09 l2=1.93431e-05 x=4.90555e-05 y=0.000467782 z=-9.67401e-06 kx=0.000192038 ky=0.000267089 kz=5.25314 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00575e-09 l2=2.21052e-05 x=-4.87626e-05 y=7.08789e-07 z=-1.10557e-05 kx=-0.000271061 ky=0.000216927 kz=5.12884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22645e-09 l2=1.81147e-05 x=-4.91727e-05 y=-6.90896e-05 z=-9.0591e-06 kx=-0.000102432 ky=-0.000136519 kz=4.43701 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5249e-09 l2=8.26037e-06 x=4.98291e-05 y=0.000223838 z=-4.13142e-06 kx=4.57572e-05 ky=0.000169543 kz=4.8039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27194e-09 l2=3.05194e-05 x=-4.76144e-05 y=-0.000131372 z=-1.52612e-05 kx=-0.000116213 ky=-0.00039562 kz=6.29979 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30887e-09 l2=2.29709e-05 x=-4.86629e-05 y=0.000419994 z=-1.14871e-05 kx=-2.97026e-05 ky=3.70313e-05 kz=1.51627 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20314e-09 l2=3.60442e-05 x=4.66388e-05 y=0.00028949 z=-1.80241e-05 kx=0.000123311 ky=8.23977e-05 kz=4.12857 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29077e-09 l2=2.55322e-05 x=-4.83426e-05 y=0.000114038 z=-1.2768e-05 kx=-0.000182104 ky=-0.000227176 kz=6.93262 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25495e-09 l2=3.0428e-05 x=-4.76297e-05 y=0.000371229 z=-1.52134e-05 kx=0.000123325 ky=6.27108e-05 kz=4.73753 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.63515e-09 l2=6.97678e-06 x=-4.98784e-05 y=-0.000171313 z=-3.48859e-06 kx=6.95613e-05 ky=3.1828e-05 kz=2.14826 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17675e-09 l2=2.61115e-05 x=4.8265e-05 y=-7.98121e-06 z=-1.30583e-05 kx=0.000214534 ky=0.000127921 kz=5.14085 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15586e-09 l2=3.07077e-05 x=-4.75846e-05 y=0.000271616 z=-1.5354e-05 kx=6.30952e-05 ky=-8.70122e-05 kz=6.67306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18907e-09 l2=1.90456e-05 x=4.90852e-05 y=0.000174601 z=-9.52204e-06 kx=-3.13921e-05 ky=-2.44691e-05 kz=1.12477 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.97088e-09 l2=1.44538e-05 x=-4.94754e-05 y=0.000263406 z=-7.22709e-06 kx=0.000137872 ky=0.000335535 kz=5.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60574e-09 l2=1.7567e-05 x=-4.92229e-05 y=0.000208426 z=-8.7827e-06 kx=0.000224127 ky=0.000107942 kz=6.85082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86049e-09 l2=6.78558e-06 x=4.98847e-05 y=8.58182e-05 z=-3.39544e-06 kx=8.82382e-05 ky=-5.28683e-05 kz=2.56591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92442e-09 l2=1.90272e-05 x=-4.90871e-05 y=-0.000254625 z=-9.51305e-06 kx=5.12812e-05 ky=-0.000106003 kz=1.64585 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.57166e-09 l2=5.89896e-06 x=-4.99131e-05 y=0.000286131 z=-2.94931e-06 kx=8.80587e-05 ky=-5.8757e-05 kz=3.03184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70714e-09 l2=1.69332e-05 x=-4.92778e-05 y=-0.000485783 z=-8.46919e-06 kx=-0.000133114 ky=-0.000298459 kz=3.77892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23457e-09 l2=3.1115e-05 x=4.75188e-05 y=-0.00036545 z=-1.55564e-05 kx=-0.00018177 ky=-2.75446e-05 kz=4.92082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51209e-09 l2=1.47493e-05 x=-4.94533e-05 y=0.00042568 z=-7.37541e-06 kx=1.1606e-06 ky=0.000179869 kz=3.78974 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07434e-09 l2=2.1291e-05 x=4.88535e-05 y=0.000400682 z=-1.06469e-05 kx=8.03433e-05 ky=6.05356e-05 kz=4.48707 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14121e-09 l2=2.66863e-05 x=-4.81873e-05 y=-4.24013e-05 z=-1.33421e-05 kx=0.000187234 ky=8.51267e-05 kz=5.5335 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06428e-09 l2=1.81144e-05 x=-4.91725e-05 y=-4.19159e-06 z=-9.06027e-06 kx=-0.000353127 ky=0.000185991 kz=6.86638 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15155e-09 l2=2.56312e-05 x=-4.83299e-05 y=-8.24042e-05 z=-1.28158e-05 kx=3.52199e-05 ky=5.06565e-05 kz=4.63059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35937e-09 l2=1.33279e-05 x=-4.95542e-05 y=6.35482e-05 z=-6.66313e-06 kx=6.04256e-05 ky=-5.53163e-05 kz=1.96462 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24382e-09 l2=1.24743e-05 x=-4.96094e-05 y=-0.000129778 z=-6.23968e-06 kx=-6.73413e-05 ky=5.05493e-06 kz=2.33792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51812e-09 l2=2.55794e-05 x=-4.83369e-05 y=-0.000427155 z=-1.27901e-05 kx=3.20573e-05 ky=4.73807e-06 kz=4.61379 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60233e-09 l2=1.72175e-05 x=4.92535e-05 y=-8.2208e-05 z=-8.60904e-06 kx=-4.11246e-05 ky=8.6071e-05 kz=4.08798 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17231e-09 l2=5.92142e-06 x=4.99124e-05 y=0.000231242 z=-2.96103e-06 kx=-4.27425e-05 ky=-5.55287e-05 kz=2.7652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08298e-09 l2=1.90653e-05 x=4.90834e-05 y=-9.29464e-05 z=-9.53107e-06 kx=-4.23093e-05 ky=-1.98191e-05 kz=0.984142 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64814e-09 l2=1.85764e-05 x=4.91298e-05 y=-0.00042392 z=-9.28924e-06 kx=1.37857e-05 ky=-0.000182683 kz=2.90545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37073e-09 l2=1.79946e-05 x=4.91835e-05 y=0.000488494 z=-9.0003e-06 kx=0.000297639 ky=0.000387501 kz=6.34112 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3641e-09 l2=2.36566e-05 x=4.85806e-05 y=0.000127722 z=-1.18304e-05 kx=0.000139069 ky=0.000274941 kz=4.63629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08794e-09 l2=4.11625e-05 x=-4.55688e-05 y=-0.000416696 z=-2.05798e-05 kx=8.00744e-05 ky=-0.000110747 kz=1.80338 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01355e-09 l2=2.82853e-05 x=4.79583e-05 y=1.02859e-05 z=-1.41433e-05 kx=1.79372e-05 ky=0.000262395 kz=6.54801 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00337e-09 l2=3.33943e-05 x=-4.71305e-05 y=0.000379153 z=-1.66959e-05 kx=0.00024364 ky=0.000192211 kz=6.44657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29718e-09 l2=3.60911e-06 x=4.99675e-05 y=5.43617e-05 z=-1.80297e-06 kx=-9.09899e-06 ky=-2.02499e-06 kz=0.203538 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53655e-09 l2=1.56992e-05 x=4.93799e-05 y=0.000116626 z=-7.85193e-06 kx=0.000107596 ky=0.00010243 kz=3.37918 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06258e-09 l2=4.77936e-05 x=-4.39203e-05 y=-8.74303e-05 z=-2.38968e-05 kx=8.28698e-05 ky=-0.000235556 kz=6.44682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76987e-09 l2=1.12794e-05 x=4.9681e-05 y=0.000392169 z=-5.64119e-06 kx=3.39217e-05 ky=7.28392e-06 kz=2.72886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.35065e-09 l2=4.70074e-06 x=-4.99449e-05 y=-0.000113231 z=-2.35074e-06 kx=0.000110181 ky=7.52625e-05 kz=3.04035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02783e-09 l2=1.76793e-05 x=4.92124e-05 y=-0.000444095 z=-8.84174e-06 kx=3.04841e-06 ky=-1.2947e-05 kz=0.142484 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64768e-09 l2=1.71784e-05 x=-4.9257e-05 y=-0.000479966 z=-8.58915e-06 kx=8.78501e-05 ky=-0.000277203 kz=5.0365 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75972e-09 l2=1.90491e-05 x=4.9085e-05 y=8.75896e-05 z=-9.52367e-06 kx=-0.000208705 ky=-0.00023493 kz=5.80257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09004e-09 l2=3.41859e-06 x=-4.99708e-05 y=0.000118702 z=-1.70932e-06 kx=1.11837e-05 ky=-2.0432e-05 kz=0.551021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13324e-09 l2=2.29318e-05 x=4.86681e-05 y=0.000284774 z=-1.1465e-05 kx=-0.000105526 ky=2.91106e-05 kz=3.55208 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.8442e-09 l2=1.8509e-05 x=-4.91363e-05 y=-0.000296747 z=-9.25501e-06 kx=5.5999e-05 ky=-0.00025573 kz=6.94047 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.26883e-09 l2=5.08934e-06 x=-4.99353e-05 y=-0.000406771 z=-2.54533e-06 kx=0.000121764 ky=-0.000400844 kz=6.25032 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0799e-09 l2=7.54015e-06 x=-4.98575e-05 y=0.000498252 z=-3.77373e-06 kx=-0.000248221 ky=0.000160975 kz=4.72774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22766e-09 l2=1.52808e-05 x=4.9413e-05 y=-0.000341335 z=-7.64148e-06 kx=-3.6966e-06 ky=-0.000361123 kz=5.25799 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37926e-09 l2=2.80016e-05 x=-4.80005e-05 y=0.000252454 z=-1.39997e-05 kx=8.02644e-05 ky=-5.0691e-05 kz=2.11656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17873e-09 l2=4.50674e-05 x=-4.46348e-05 y=-0.000311466 z=-2.25341e-05 kx=2.23106e-05 ky=-0.000289262 kz=4.89599 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05459e-09 l2=2.20725e-05 x=4.87666e-05 y=0.000369141 z=-1.10383e-05 kx=0.000199387 ky=0.000304297 kz=6.46161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06474e-09 l2=2.65842e-05 x=-4.82008e-05 y=-0.000290564 z=-1.32931e-05 kx=-1.62266e-05 ky=-8.12635e-05 kz=1.59 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12239e-09 l2=1.74911e-05 x=-4.92293e-05 y=-7.75214e-05 z=-8.747e-06 kx=-3.67141e-05 ky=-0.000193019 kz=4.44472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.46003e-09 l2=1.00174e-05 x=-4.97489e-05 y=-2.13712e-05 z=-5.00824e-06 kx=1.78853e-05 ky=-2.41466e-06 kz=0.411064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.74676e-09 l2=1.93136e-05 x=4.90585e-05 y=0.000403364 z=-9.66018e-06 kx=1.66458e-05 ky=2.26549e-05 kz=0.404028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35508e-09 l2=1.06252e-05 x=4.97172e-05 y=-0.000327679 z=-5.31197e-06 kx=-4.98353e-05 ky=-4.64692e-05 kz=1.87015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0628e-09 l2=4.07341e-05 x=-4.56634e-05 y=0.000187359 z=-2.0369e-05 kx=-0.000218108 ky=-4.59615e-06 kz=6.96313 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14986e-09 l2=2.26804e-05 x=4.86966e-05 y=0.000164704 z=-1.13432e-05 kx=2.26148e-05 ky=-1.35501e-05 kz=0.449085 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38325e-09 l2=1.46545e-05 x=-4.94605e-05 y=-9.74159e-06 z=-7.32782e-06 kx=3.31735e-06 ky=6.1156e-06 kz=0.256425 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13351e-09 l2=9.83317e-06 x=4.9758e-05 y=-0.000409885 z=-4.91547e-06 kx=-0.000230674 ky=-0.000263716 kz=5.25221 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34354e-09 l2=1.0269e-05 x=-4.97358e-05 y=0.000455622 z=-5.1356e-06 kx=6.49244e-06 ky=0.000158919 kz=3.31922 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65146e-09 l2=1.89199e-05 x=4.90971e-05 y=-5.23699e-05 z=-9.46093e-06 kx=1.78994e-06 ky=1.64704e-05 kz=0.478069 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71769e-09 l2=1.97462e-05 x=-4.90159e-05 y=-7.28478e-05 z=-9.8731e-06 kx=0.000113052 ky=-0.00027558 kz=6.38629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67655e-09 l2=3.13827e-05 x=-4.74737e-05 y=-0.000324677 z=-1.56939e-05 kx=-3.08983e-05 ky=1.9953e-06 kz=0.842381 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44536e-09 l2=3.29093e-05 x=-4.72155e-05 y=-0.000352271 z=-1.64544e-05 kx=1.89945e-05 ky=-1.1114e-05 kz=0.954777 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30258e-09 l2=1.60769e-05 x=4.93496e-05 y=1.84579e-05 z=-8.03955e-06 kx=1.39262e-05 ky=5.85305e-05 kz=1.55071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22318e-09 l2=1.05881e-05 x=-4.97189e-05 y=5.67805e-05 z=-5.29608e-06 kx=-7.02459e-05 ky=-4.90546e-05 kz=2.44907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75598e-09 l2=4.85951e-06 x=-4.9941e-05 y=0.000252024 z=-2.43107e-06 kx=1.66027e-06 ky=-6.19696e-06 kz=1.31756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2611e-09 l2=1.85371e-05 x=-4.91334e-05 y=0.000204888 z=-9.2701e-06 kx=-6.63715e-05 ky=3.45659e-05 kz=3.54287 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24877e-09 l2=3.72646e-05 x=-4.63997e-05 y=0.000232191 z=-1.86309e-05 kx=0.000165711 ky=-8.01819e-05 kz=3.7523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91066e-09 l2=1.60208e-05 x=4.93542e-05 y=-4.61533e-05 z=-8.01236e-06 kx=8.3528e-05 ky=-6.9992e-05 kz=4.01927 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09558e-09 l2=2.78073e-05 x=4.80278e-05 y=-0.000399797 z=-1.39054e-05 kx=7.11153e-05 ky=-0.000206299 kz=2.90209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.65457e-09 l2=6.78186e-06 x=4.9885e-05 y=0.000270425 z=-3.39245e-06 kx=-3.64917e-05 ky=0.000395396 kz=5.97608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16131e-09 l2=7.11422e-06 x=4.98732e-05 y=0.000409632 z=-3.55926e-06 kx=2.93906e-05 ky=9.69348e-06 kz=0.930399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17197e-09 l2=3.29112e-05 x=4.7215e-05 y=-0.0003402 z=-1.64554e-05 kx=-1.91475e-05 ky=-6.12388e-05 kz=1.20055 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63816e-09 l2=1.49918e-05 x=4.94348e-05 y=-0.000387395 z=-7.49814e-06 kx=4.27776e-05 ky=1.05875e-05 kz=1.49525 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06883e-09 l2=2.66342e-05 x=4.81936e-05 y=-0.000287312 z=-1.33194e-05 kx=0.000123457 ky=7.15388e-06 kz=3.44956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44536e-09 l2=3.29093e-05 x=-4.72155e-05 y=-0.000352271 z=-1.64544e-05 kx=1.89945e-05 ky=-1.1114e-05 kz=0.954777 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18531e-09 l2=2.04933e-05 x=-4.89391e-05 y=-0.000173349 z=-1.02464e-05 kx=1.55445e-05 ky=-1.58e-05 kz=0.87304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18863e-09 l2=3.06334e-05 x=4.7597e-05 y=-7.30775e-05 z=-1.53154e-05 kx=-0.00023405 ky=5.71387e-05 kz=5.70888 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00129e-09 l2=1.06459e-05 x=-4.97161e-05 y=-0.000240407 z=-5.32251e-06 kx=1.97587e-05 ky=6.83017e-06 kz=0.670423 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.54121e-09 l2=9.67375e-06 x=4.97657e-05 y=-0.000440285 z=-4.83869e-06 kx=7.62938e-07 ky=-5.8332e-05 kz=0.854869 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67962e-09 l2=1.50331e-05 x=-4.94321e-05 y=-3.47451e-05 z=-7.51621e-06 kx=8.8935e-05 ky=-4.4405e-05 kz=3.7783 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43312e-09 l2=6.932e-06 x=4.98799e-05 y=-0.000180607 z=-3.46546e-06 kx=-9.11024e-06 ky=7.48343e-06 kz=0.361879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15128e-09 l2=4.24742e-05 x=-4.5265e-05 y=0.000456694 z=-2.12399e-05 kx=-0.000327007 ky=5.42953e-05 kz=6.67045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18684e-09 l2=2.32421e-05 x=4.86308e-05 y=0.000286849 z=-1.16219e-05 kx=2.61027e-05 ky=0.000266529 kz=5.70037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59884e-09 l2=9.41305e-06 x=-4.97781e-05 y=9.39077e-05 z=-4.70729e-06 kx=1.3591e-06 ky=0.000103205 kz=1.98371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37779e-09 l2=1.63977e-05 x=4.93234e-05 y=0.000322432 z=-8.19924e-06 kx=-2.24316e-06 ky=1.02651e-05 kz=0.36186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.36422e-09 l2=4.6154e-06 x=4.99468e-05 y=-0.00014671 z=-2.31105e-06 kx=6.1994e-06 ky=-2.83521e-05 kz=0.46652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60082e-09 l2=3.01309e-05 x=4.76767e-05 y=5.22741e-05 z=-1.50659e-05 kx=-4.39707e-05 ky=0.000309699 kz=5.90954 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27115e-09 l2=8.1552e-06 x=-4.98335e-05 y=-0.000421178 z=-4.07777e-06 kx=1.70194e-06 ky=-9.43907e-06 kz=0.181518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15248e-09 l2=4.53154e-05 x=-4.45722e-05 y=2.39788e-05 z=-2.26576e-05 kx=9.69773e-05 ky=-0.000320732 kz=6.90101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48912e-09 l2=2.39871e-05 x=-4.85398e-05 y=0.000458206 z=-1.19969e-05 kx=-0.000209787 ky=0.000246126 kz=3.92794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71762e-09 l2=1.42027e-05 x=-4.94929e-05 y=-1.33402e-06 z=-7.10484e-06 kx=-0.000267075 ky=-0.000126736 kz=5.06711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22547e-09 l2=3.21301e-05 x=4.73497e-05 y=-0.00046376 z=-1.60637e-05 kx=-0.000183759 ky=-0.000261313 kz=4.29034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89673e-09 l2=1.23273e-05 x=4.96185e-05 y=-0.000436998 z=-6.16661e-06 kx=0.000135107 ky=-3.61541e-05 kz=3.31167 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.157e-09 l2=3.42983e-05 x=4.69667e-05 y=-3.47872e-05 z=-1.71514e-05 kx=0.000128634 ky=-1.72664e-05 kz=3.57943 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13335e-09 l2=4.56489e-05 x=-4.44862e-05 y=0.000337546 z=-2.28261e-05 kx=-6.87759e-06 ky=1.91332e-05 kz=0.284004 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00202e-09 l2=2.84908e-05 x=4.79272e-05 y=0.00033418 z=-1.42483e-05 kx=0.000207747 ky=-1.12074e-05 kz=4.12587 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.27134e-09 l2=2.23716e-05 x=4.87332e-05 y=0.000381481 z=-1.11861e-05 kx=-3.13261e-05 ky=-1.48736e-05 kz=1.72655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43257e-09 l2=1.83922e-05 x=-4.91473e-05 y=0.000226077 z=-9.1972e-06 kx=6.00579e-06 ky=6.72276e-06 kz=2.40955 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22547e-09 l2=3.21301e-05 x=4.73497e-05 y=-0.00046376 z=-1.60637e-05 kx=-0.000183759 ky=-0.000261313 kz=4.29034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96076e-09 l2=1.53015e-05 x=4.94115e-05 y=-5.51259e-05 z=-7.65041e-06 kx=-0.000151802 ky=-5.79075e-05 kz=5.63965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34183e-09 l2=1.43119e-05 x=4.94852e-05 y=-0.000451026 z=-7.1576e-06 kx=0.000125467 ky=1.15849e-05 kz=6.40052 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2382e-09 l2=1.9742e-05 x=4.90161e-05 y=-0.000369356 z=-9.87131e-06 kx=-3.97197e-05 ky=-7.45418e-05 kz=5.94745 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4723e-09 l2=1.11268e-05 x=4.96893e-05 y=-0.000183513 z=-5.56685e-06 kx=0.000365087 ky=-0.000308724 kz=6.69763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.03166e-09 l2=8.60685e-06 x=4.98144e-05 y=0.00044461 z=-4.30817e-06 kx=0.000124053 ky=3.06885e-06 kz=2.26434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25428e-09 l2=1.15675e-05 x=4.96644e-05 y=0.000432064 z=-5.78473e-06 kx=1.10674e-05 ky=0.00010253 kz=1.61381 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17083e-09 l2=1.0974e-05 x=-4.96981e-05 y=0.000186253 z=-5.48815e-06 kx=-1.53676e-06 ky=-3.20334e-05 kz=1.13826 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06213e-09 l2=2.59295e-05 x=4.829e-05 y=-0.000203571 z=-1.29654e-05 kx=5.44586e-07 ky=1.04804e-06 kz=0.408224 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6659e-09 l2=1.20615e-05 x=4.96351e-05 y=-0.000117953 z=-6.03099e-06 kx=-2.62464e-05 ky=-8.37491e-05 kz=2.17154 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.86492e-09 l2=2.02231e-05 x=-4.89667e-05 y=-0.000361802 z=-1.01151e-05 kx=-0.000282159 ky=-0.000258878 kz=6.42015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28781e-09 l2=2.60376e-05 x=4.8276e-05 y=-0.000231498 z=-1.30176e-05 kx=-3.86292e-05 ky=-8.20985e-06 kz=1.04682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22101e-09 l2=3.24806e-05 x=4.72895e-05 y=-0.000466873 z=-1.62403e-05 kx=-2.16854e-05 ky=-0.000133191 kz=1.63794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40424e-09 l2=1.6878e-05 x=-4.92826e-05 y=-0.00027869 z=-8.44105e-06 kx=-0.000102282 ky=-0.00012192 kz=3.69326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09824e-09 l2=3.38801e-05 x=4.70424e-05 y=-0.00032712 z=-1.69427e-05 kx=0.000264741 ky=-0.000314902 kz=5.99603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1101e-09 l2=1.59308e-05 x=-4.93614e-05 y=-0.000494386 z=-7.96694e-06 kx=-0.000139761 ky=-0.000429516 kz=7.02168 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34368e-09 l2=9.30227e-06 x=-4.97835e-05 y=0.00048936 z=-4.64958e-06 kx=8.20362e-05 ky=5.85061e-06 kz=1.83583 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.60649e-09 l2=7.55882e-06 x=4.9857e-05 y=-0.000385732 z=-3.78163e-06 kx=1.12133e-05 ky=-4.33833e-05 kz=0.609371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95271e-09 l2=2.05437e-05 x=-4.89337e-05 y=0.000297534 z=-1.02728e-05 kx=7.98217e-09 ky=7.17197e-06 kz=0.225502 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16867e-09 l2=3.09128e-05 x=4.75508e-05 y=4.33644e-05 z=-1.54584e-05 kx=5.53216e-05 ky=5.33032e-05 kz=1.89045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2216e-09 l2=1.66212e-05 x=-4.93045e-05 y=-0.00049338 z=-8.31197e-06 kx=-0.00010249 ky=-0.000524543 kz=6.59463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04876e-09 l2=2.57673e-05 x=4.83118e-05 y=0.000467777 z=-1.28838e-05 kx=-3.39975e-05 ky=0.000262092 kz=4.98408 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22101e-09 l2=3.24806e-05 x=4.72895e-05 y=-0.000466873 z=-1.62403e-05 kx=-2.16854e-05 ky=-0.000133191 kz=1.63794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01804e-09 l2=3.84267e-05 x=-4.61617e-05 y=0.000108572 z=-1.92129e-05 kx=9.13754e-05 ky=-5.94315e-05 kz=4.37758 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75188e-09 l2=3.64375e-06 x=4.99668e-05 y=1.35791e-05 z=-1.82556e-06 kx=0.000219135 ky=0.000163919 kz=4.75095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03617e-09 l2=4.83013e-05 x=4.37799e-05 y=0.000454904 z=-2.41531e-05 kx=0.000204451 ky=0.000122502 kz=4.53404 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75977e-09 l2=7.87145e-06 x=4.98451e-05 y=-0.000105277 z=-3.93563e-06 kx=-0.000159662 ky=-8.98292e-06 kz=5.39194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.92278e-09 l2=6.5434e-06 x=4.9893e-05 y=0.000455963 z=-3.27342e-06 kx=-3.07361e-05 ky=0.00046405 kz=6.4156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00411e-09 l2=1.87658e-05 x=-4.91116e-05 y=-0.000268006 z=-9.38437e-06 kx=-1.49757e-05 ky=1.1982e-05 kz=0.7461 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36865e-09 l2=1.82692e-05 x=4.91582e-05 y=-0.000259184 z=-9.13788e-06 kx=0.000216182 ky=3.90724e-05 kz=4.07507 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14115e-09 l2=2.0872e-05 x=4.88986e-05 y=0.00015181 z=-1.04379e-05 kx=0.000190454 ky=0.000241799 kz=6.911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45322e-09 l2=3.40973e-05 x=4.70033e-05 y=0.000351537 z=-1.70511e-05 kx=9.31608e-05 ky=0.000116492 kz=2.53153 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44242e-09 l2=6.91742e-06 x=4.98803e-05 y=3.03328e-05 z=-3.46068e-06 kx=3.05263e-05 ky=6.34801e-06 kz=2.03017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49073e-09 l2=1.22219e-05 x=4.96254e-05 y=1.27187e-06 z=-6.11061e-06 kx=-0.000119849 ky=-0.000248344 kz=5.50915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12249e-09 l2=4.02704e-05 x=4.57666e-05 y=0.000458884 z=-2.01361e-05 kx=1.06105e-05 ky=0.000119763 kz=1.64592 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53239e-09 l2=3.19826e-05 x=4.73746e-05 y=-0.000282647 z=-1.59906e-05 kx=-0.000106505 ky=-6.86544e-05 kz=3.43208 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37794e-09 l2=3.77327e-05 x=-4.6304e-05 y=0.000432877 z=-1.88678e-05 kx=-7.90216e-05 ky=0.00039666 kz=4.64387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7187e-09 l2=1.17852e-05 x=-4.96517e-05 y=-0.000119085 z=-5.89344e-06 kx=3.17357e-06 ky=-7.91141e-05 kz=3.96703 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.63821e-09 l2=6.55721e-06 x=-4.98927e-05 y=-0.000268032 z=-3.28092e-06 kx=2.06672e-06 ky=1.88162e-06 kz=0.102536 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28723e-09 l2=2.21104e-05 x=4.87628e-05 y=-0.000300573 z=-1.10551e-05 kx=-0.000107409 ky=0.000108145 kz=6.91048 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30248e-09 l2=3.05902e-05 x=4.7604e-05 y=-0.00023492 z=-1.52938e-05 kx=-7.00656e-05 ky=-3.56241e-05 kz=1.68609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82065e-09 l2=1.81102e-05 x=-4.91732e-05 y=0.000496629 z=-9.05785e-06 kx=-0.00017655 ky=0.00050315 kz=6.45275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45934e-09 l2=3.08062e-05 x=-4.7568e-05 y=-0.000208311 z=-1.54054e-05 kx=-0.000136241 ky=-0.000134508 kz=3.96355 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19108e-09 l2=3.33484e-05 x=-4.71383e-05 y=7.58091e-05 z=-1.66738e-05 kx=0.000146558 ky=5.07247e-05 kz=6.99178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06851e-09 l2=3.32307e-05 x=4.71589e-05 y=-4.51472e-06 z=-1.66154e-05 kx=-1.74847e-05 ky=3.55726e-05 kz=1.61989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.81479e-09 l2=5.8304e-06 x=-4.99151e-05 y=-0.000404375 z=-2.91624e-06 kx=0.000108208 ky=-0.000185644 kz=6.23733 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13651e-09 l2=2.51971e-05 x=-4.83869e-05 y=0.000399928 z=-1.25992e-05 kx=-1.01611e-05 ky=9.82719e-05 kz=3.80526 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20199e-09 l2=1.39358e-05 x=4.95122e-05 y=-0.0001627 z=-6.96835e-06 kx=-4.05936e-07 ky=1.1387e-06 kz=0.146879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13289e-09 l2=3.4234e-05 x=4.69786e-05 y=-0.000470447 z=-1.71188e-05 kx=6.66777e-05 ky=-4.37082e-05 kz=2.5965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52958e-09 l2=2.06734e-05 x=-4.89196e-05 y=-0.000305072 z=-1.03395e-05 kx=-8.90176e-05 ky=-0.000160265 kz=2.12159 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32779e-09 l2=8.79801e-06 x=-4.98063e-05 y=9.86258e-05 z=-4.39922e-06 kx=0.000123541 ky=-0.000228191 kz=6.45495 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74206e-09 l2=2.21381e-05 x=4.87593e-05 y=0.000487783 z=-1.1071e-05 kx=7.34113e-05 ky=0.000162372 kz=3.43602 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.72215e-09 l2=1.09747e-05 x=4.9698e-05 y=-9.81529e-05 z=-5.48971e-06 kx=0.00010269 ky=-0.000247023 kz=5.19514 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21194e-09 l2=4.1794e-05 x=4.54235e-05 y=1.94019e-05 z=-2.08987e-05 kx=4.76082e-05 ky=-3.93927e-06 kz=2.02523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14777e-09 l2=2.1641e-05 x=4.88156e-05 y=-6.62421e-05 z=-1.08206e-05 kx=-8.48709e-05 ky=-0.000211953 kz=4.3108 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31077e-09 l2=3.25901e-05 x=-4.72698e-05 y=-0.000498531 z=-1.62975e-05 kx=-0.000184053 ky=-0.000311799 kz=4.91001 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17019e-09 l2=1.5121e-05 x=4.94252e-05 y=0.000221791 z=-7.56087e-06 kx=-2.89945e-05 ky=-4.69505e-05 kz=6.51247 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84621e-09 l2=9.93609e-06 x=4.97524e-05 y=8.04979e-05 z=-4.97167e-06 kx=0.000154349 ky=-1.22186e-05 kz=2.84591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02652e-09 l2=1.04466e-05 x=-4.97267e-05 y=4.59524e-05 z=-5.22162e-06 kx=0.000243081 ky=0.000108004 kz=5.45858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39016e-09 l2=1.98881e-05 x=-4.90012e-05 y=0.000270905 z=-9.94547e-06 kx=-4.78384e-05 ky=1.83978e-05 kz=3.24212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44889e-09 l2=1.64259e-05 x=-4.93207e-05 y=-0.000131303 z=-8.21531e-06 kx=-0.000216563 ky=0.000160764 kz=6.61203 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65875e-09 l2=1.14349e-05 x=4.96718e-05 y=-9.65476e-05 z=-5.72101e-06 kx=0.000321023 ky=0.000161972 kz=5.89641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04321e-09 l2=3.20541e-05 x=4.73628e-05 y=6.07515e-05 z=-1.60259e-05 kx=-5.09056e-05 ky=-3.99231e-05 kz=1.13432 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07166e-09 l2=3.63253e-05 x=4.65849e-05 y=-0.000204209 z=-1.81627e-05 kx=-3.31008e-05 ky=-2.76406e-05 kz=3.44664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72081e-09 l2=3.19267e-05 x=-4.73828e-05 y=8.2839e-05 z=-1.59664e-05 kx=-0.00016186 ky=-0.000119485 kz=3.48703 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36211e-09 l2=1.77279e-05 x=-4.92083e-05 y=0.000381926 z=-8.86361e-06 kx=1.9377e-05 ky=4.64046e-05 kz=0.909288 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1106e-09 l2=2.12815e-05 x=-4.88549e-05 y=0.000164004 z=-1.06408e-05 kx=1.66631e-05 ky=5.08497e-05 kz=1.60911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47077e-09 l2=3.34755e-05 x=-4.71154e-05 y=-6.0248e-05 z=-1.67389e-05 kx=-3.24082e-05 ky=0.00013584 kz=3.70107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19643e-09 l2=2.3268e-05 x=4.86275e-05 y=4.36989e-05 z=-1.16359e-05 kx=8.03058e-05 ky=5.5718e-05 kz=2.99859 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19355e-09 l2=3.36215e-05 x=4.70894e-05 y=0.000473758 z=-1.68117e-05 kx=4.35101e-05 ky=0.000118242 kz=5.99911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38936e-09 l2=2.77851e-05 x=4.80313e-05 y=-0.000319452 z=-1.38935e-05 kx=8.8539e-06 ky=3.42244e-06 kz=1.49958 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33391e-09 l2=2.1444e-05 x=-4.8837e-05 y=0.000362562 z=-1.07225e-05 kx=2.6796e-06 ky=5.14688e-05 kz=0.726943 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.18305e-09 l2=4.83591e-06 x=-4.99416e-05 y=0.000341692 z=-2.41982e-06 kx=1.23732e-06 ky=1.5628e-05 kz=0.272042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14037e-09 l2=1.97771e-05 x=4.90128e-05 y=0.000142135 z=-9.88799e-06 kx=-6.30341e-05 ky=-3.40175e-05 kz=2.77748 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21823e-09 l2=2.57246e-05 x=4.8317e-05 y=-7.78683e-05 z=-1.28648e-05 kx=8.07455e-05 ky=-0.000118716 kz=2.08298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88351e-09 l2=1.21443e-05 x=-4.963e-05 y=-5.29234e-05 z=-6.07311e-06 kx=-6.96523e-07 ky=-4.69946e-05 kz=0.892857 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47077e-09 l2=3.34755e-05 x=-4.71154e-05 y=-6.0248e-05 z=-1.67389e-05 kx=-3.24082e-05 ky=0.00013584 kz=3.70107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19355e-09 l2=3.36215e-05 x=4.70894e-05 y=0.000473758 z=-1.68117e-05 kx=4.35101e-05 ky=0.000118242 kz=5.99911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55314e-09 l2=2.37186e-05 x=-4.85732e-05 y=-3.27449e-05 z=-1.18607e-05 kx=-2.76291e-05 ky=1.03663e-06 kz=2.05401 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.53448e-09 l2=6.7039e-06 x=-4.98877e-05 y=0.000156199 z=-3.35727e-06 kx=-6.35764e-05 ky=0.000119794 kz=2.04565 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34217e-09 l2=3.80909e-05 x=-4.62307e-05 y=0.000237491 z=-1.90466e-05 kx=-1.95392e-05 ky=0.000121067 kz=1.7052 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44399e-09 l2=1.88936e-05 x=4.90999e-05 y=-0.000110776 z=-9.44595e-06 kx=-6.50246e-05 ky=7.12534e-05 kz=2.05826 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67299e-09 l2=1.33179e-05 x=4.95548e-05 y=0.000412922 z=-6.66027e-06 kx=-2.69856e-07 ky=2.68901e-05 kz=0.3602 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34217e-09 l2=3.80909e-05 x=-4.62307e-05 y=0.000237491 z=-1.90466e-05 kx=-1.95392e-05 ky=0.000121067 kz=1.7052 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90065e-09 l2=1.08245e-05 x=-4.9706e-05 y=0.000410633 z=-5.41588e-06 kx=-0.000300819 ky=0.000458094 kz=5.60448 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6156e-09 l2=1.95474e-05 x=4.90356e-05 y=-8.13207e-05 z=-9.77429e-06 kx=-1.84491e-05 ky=-0.000103868 kz=4.15379 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77015e-09 l2=8.0621e-06 x=-4.98374e-05 y=0.000312983 z=-4.03131e-06 kx=5.69461e-05 ky=0.000109397 kz=4.522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35566e-09 l2=1.29062e-05 x=4.95817e-05 y=-0.000325353 z=-6.45523e-06 kx=9.45341e-05 ky=-0.000160421 kz=3.18779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33748e-09 l2=1.36636e-05 x=4.95314e-05 y=-0.000267512 z=-6.83138e-06 kx=-2.7623e-05 ky=-6.17859e-09 kz=0.872661 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84898e-09 l2=1.20198e-05 x=-4.96374e-05 y=-8.8652e-05 z=-6.01285e-06 kx=-5.92807e-05 ky=-6.87435e-06 kz=1.44055 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03224e-09 l2=1.27437e-05 x=-4.95927e-05 y=-0.000472011 z=-6.37036e-06 kx=0.000167815 ky=-0.000305293 kz=4.14609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87457e-09 l2=9.36478e-06 x=4.97803e-05 y=5.65167e-05 z=-4.68433e-06 kx=0.000124782 ky=0.000189479 kz=6.19489 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19177e-09 l2=2.55657e-05 x=-4.83386e-05 y=4.5975e-05 z=-1.27832e-05 kx=3.21915e-05 ky=-5.19878e-05 kz=5.88767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19973e-09 l2=1.80046e-05 x=4.91827e-05 y=-0.000350033 z=-9.00445e-06 kx=0.000114264 ky=-0.000229556 kz=3.61521 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49161e-09 l2=1.98978e-05 x=-4.89998e-05 y=0.000411346 z=-9.95211e-06 kx=-0.000214133 ky=0.000118457 kz=4.27313 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63842e-09 l2=1.75058e-05 x=4.92278e-05 y=-0.000328277 z=-8.75618e-06 kx=7.68648e-05 ky=-6.40001e-05 kz=1.91594 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.20614e-09 l2=1.1437e-05 x=4.96722e-05 y=-0.000250829 z=-5.71953e-06 kx=-5.45425e-05 ky=-5.75294e-05 kz=4.86365 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07835e-09 l2=3.24298e-05 x=-4.72983e-05 y=0.000350298 z=-1.62143e-05 kx=8.56917e-05 ky=0.000265371 kz=3.48077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00558e-09 l2=2.17322e-05 x=-4.88048e-05 y=2.86136e-05 z=-1.08682e-05 kx=-1.62044e-05 ky=6.65554e-06 kz=0.50784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.92726e-09 l2=1.57784e-05 x=4.9374e-05 y=-0.000300928 z=-7.89006e-06 kx=-1.2446e-05 ky=-1.28879e-05 kz=0.977451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84195e-09 l2=1.26571e-05 x=-4.9598e-05 y=0.000444078 z=-6.32953e-06 kx=-4.52239e-06 ky=6.94529e-05 kz=3.5416 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.89314e-09 l2=2.30631e-06 x=4.99867e-05 y=-0.000433665 z=-1.15705e-06 kx=4.76335e-05 ky=-7.40006e-05 kz=2.50885 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89754e-09 l2=1.54597e-05 x=4.93987e-05 y=-0.000230976 z=-7.73288e-06 kx=0.000282496 ky=-6.92572e-05 kz=6.61333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54654e-09 l2=2.04708e-05 x=-4.89411e-05 y=0.000220899 z=-1.02372e-05 kx=-0.000139787 ky=0.000210196 kz=6.3777 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07046e-09 l2=3.33213e-05 x=4.71421e-05 y=-9.54305e-05 z=-1.66631e-05 kx=5.26336e-05 ky=-2.74033e-05 kz=1.31759 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82061e-09 l2=1.20959e-05 x=4.96328e-05 y=0.000336086 z=-6.05058e-06 kx=0.000165638 ky=-5.2258e-05 kz=4.7925 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20686e-09 l2=2.00182e-05 x=-4.89885e-05 y=-0.000285269 z=-1.00076e-05 kx=0.000107499 ky=-6.30613e-05 kz=2.49063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.52417e-09 l2=1.28074e-05 x=-4.95881e-05 y=-0.000451063 z=-6.407e-06 kx=-0.000169508 ky=-0.000247304 kz=4.10344 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4564e-09 l2=1.38644e-05 x=4.95171e-05 y=0.000302383 z=-6.9335e-06 kx=3.4702e-05 ky=0.000192557 kz=2.99365 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93505e-09 l2=1.39817e-05 x=-4.95087e-05 y=0.00027065 z=-6.99366e-06 kx=-0.000245819 ky=0.000107112 kz=6.63603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02659e-09 l2=4.95213e-05 x=4.34384e-05 y=0.000120049 z=-2.47619e-05 kx=4.70046e-05 ky=3.21879e-05 kz=2.67481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22018e-09 l2=1.69784e-05 x=-4.92745e-05 y=-0.000480465 z=-8.48789e-06 kx=0.000254485 ky=-0.000506652 kz=6.51717 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9664e-09 l2=1.07593e-05 x=-4.97097e-05 y=0.000145562 z=-5.38231e-06 kx=-9.84698e-05 ky=2.28585e-05 kz=2.88938 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06922e-09 l2=4.78315e-05 x=-4.39096e-05 y=8.42222e-05 z=-2.39164e-05 kx=-1.43591e-05 ky=0.000307187 kz=6.43628 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35247e-09 l2=1.76874e-05 x=4.92118e-05 y=0.000236248 z=-8.84414e-06 kx=-2.78481e-05 ky=0.000412414 kz=6.01524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.32468e-09 l2=5.17942e-06 x=4.99329e-05 y=6.27212e-05 z=-2.59406e-06 kx=0.000126192 ky=-6.45879e-05 kz=2.87671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.70172e-09 l2=5.93087e-06 x=4.9912e-05 y=-5.42939e-05 z=-2.96923e-06 kx=0.000139962 ky=-0.000153639 kz=3.59691 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43871e-09 l2=1.219e-05 x=-4.9627e-05 y=0.000389004 z=-6.09756e-06 kx=-3.87974e-05 ky=1.20119e-05 kz=1.04053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0925e-09 l2=2.80582e-05 x=-4.79916e-05 y=-0.000155364 z=-1.403e-05 kx=-6.51628e-06 ky=-2.23795e-05 kz=0.889017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68923e-09 l2=8.06652e-06 x=4.98371e-05 y=0.000414537 z=-4.03482e-06 kx=9.88198e-06 ky=4.54114e-05 kz=0.684778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34623e-09 l2=9.22934e-06 x=4.97865e-05 y=-0.000397824 z=-4.61672e-06 kx=2.32742e-05 ky=-3.4521e-05 kz=0.843305 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74364e-09 l2=1.69862e-05 x=4.92733e-05 y=0.000156336 z=-8.49564e-06 kx=5.108e-05 ky=6.75142e-05 kz=1.51612 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00147e-09 l2=1.99579e-05 x=-4.89947e-05 y=5.1884e-05 z=-9.97794e-06 kx=0.000219125 ky=0.000217246 kz=5.3325 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09507e-09 l2=2.65669e-05 x=-4.82028e-05 y=0.000213548 z=-1.32861e-05 kx=-0.000129313 ky=-5.01806e-06 kz=2.99196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.14202e-09 l2=7.67483e-06 x=-4.98526e-05 y=-0.000245 z=-3.83914e-06 kx=-1.93671e-06 ky=-1.61806e-05 kz=0.61637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95789e-09 l2=9.5597e-06 x=-4.97709e-05 y=0.000329473 z=-4.78269e-06 kx=-8.36211e-05 ky=-1.59358e-06 kz=2.2308 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17072e-09 l2=3.30491e-05 x=-4.71908e-05 y=-0.000191361 z=-1.65248e-05 kx=4.04384e-05 ky=-6.74676e-05 kz=5.17017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56926e-09 l2=1.96222e-05 x=4.90283e-05 y=7.78897e-05 z=-9.81087e-06 kx=-0.000106995 ky=-2.46818e-05 kz=5.20112 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.8574e-09 l2=1.89757e-05 x=-4.9092e-05 y=0.000184586 z=-9.48759e-06 kx=0.000158054 ky=0.000257067 kz=6.48396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16423e-09 l2=1.43088e-05 x=4.94856e-05 y=0.000340867 z=-7.15477e-06 kx=-1.13532e-05 ky=0.000184312 kz=2.44321 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15202e-09 l2=2.01566e-05 x=4.89737e-05 y=6.48895e-05 z=-1.00799e-05 kx=5.21026e-05 ky=6.6693e-05 kz=2.57092 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18833e-09 l2=3.24879e-05 x=4.72886e-05 y=4.80696e-05 z=-1.62429e-05 kx=-3.42603e-05 ky=-1.65154e-05 kz=0.981183 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14181e-09 l2=1.38909e-05 x=4.95151e-05 y=-0.000365436 z=-6.94801e-06 kx=0.000187896 ky=-2.36271e-05 kz=4.62861 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.01899e-09 l2=1.17758e-05 x=4.96521e-05 y=-2.18321e-05 z=-5.89111e-06 kx=0.000137352 ky=-0.000200537 kz=4.03771 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14103e-09 l2=2.57508e-05 x=4.83133e-05 y=0.000364702 z=-1.28784e-05 kx=0.000352619 ky=0.000565417 kz=6.88975 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71972e-09 l2=2.28537e-05 x=4.86774e-05 y=-0.000239653 z=-1.1426e-05 kx=-0.000231868 ky=-0.000356993 kz=6.5991 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04902e-09 l2=3.3138e-05 x=4.71757e-05 y=-6.52106e-06 z=-1.65678e-05 kx=-0.00012917 ky=-3.33492e-05 kz=3.49282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06669e-09 l2=1.73197e-05 x=-4.92448e-05 y=-0.000413734 z=-8.65852e-06 kx=0.000113226 ky=-6.46455e-05 kz=2.99961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07358e-09 l2=2.60389e-05 x=-4.82754e-05 y=-0.000119421 z=-1.30198e-05 kx=1.19334e-05 ky=4.98454e-05 kz=3.51928 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37569e-09 l2=1.42658e-05 x=-4.94884e-05 y=0.000184767 z=-7.1357e-06 kx=-0.000211769 ky=7.31078e-05 kz=4.91656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.73235e-09 l2=4.45294e-06 x=4.99504e-05 y=0.000447385 z=-2.23039e-06 kx=0.000235427 ky=0.000201771 kz=4.60053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.86003e-09 l2=6.82567e-06 x=4.98836e-05 y=0.000320398 z=-3.41304e-06 kx=-0.000239066 ky=0.000110153 kz=6.90899 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.46732e-09 l2=5.3524e-06 x=4.99285e-05 y=-0.000210677 z=-2.67903e-06 kx=4.12648e-07 ky=-1.09602e-05 kz=0.211076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02352e-09 l2=1.24898e-05 x=4.96082e-05 y=-0.000348831 z=-6.24799e-06 kx=3.40537e-05 ky=-7.37826e-06 kz=0.654982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16137e-09 l2=2.03968e-05 x=-4.89487e-05 y=0.000127287 z=-1.02004e-05 kx=-0.000109057 ky=0.000205783 kz=3.67484 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65153e-09 l2=6.69075e-06 x=-4.9888e-05 y=-0.000328241 z=-3.34572e-06 kx=6.47805e-05 ky=-0.000355735 kz=6.7504 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90466e-09 l2=1.65846e-05 x=4.93079e-05 y=-0.000479587 z=-8.29216e-06 kx=-0.000105747 ky=-0.000397347 kz=4.81948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38141e-09 l2=2.54901e-05 x=4.83491e-05 y=-7.33343e-05 z=-1.27436e-05 kx=-0.000219882 ky=-0.000116059 kz=4.93237 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.99868e-09 l2=9.91853e-06 x=-4.97535e-05 y=0.000296281 z=-4.96107e-06 kx=-3.6737e-05 ky=7.31745e-05 kz=2.26113 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12195e-09 l2=1.88868e-05 x=-4.90998e-05 y=0.000243583 z=-9.44604e-06 kx=-6.93274e-05 ky=-2.26497e-05 kz=1.62653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37119e-09 l2=2.6908e-05 x=-4.81565e-05 y=0.000289463 z=-1.34532e-05 kx=0.000147581 ky=0.000198997 kz=4.91509 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.2182e-09 l2=4.92265e-06 x=-4.99395e-05 y=-5.26798e-06 z=-2.46101e-06 kx=9.76792e-05 ky=-3.91996e-05 kz=3.42045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06565e-09 l2=2.62769e-05 x=4.82431e-05 y=-0.000179921 z=-1.31391e-05 kx=3.76204e-06 ky=-3.34893e-05 kz=1.71351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00848e-09 l2=2.45724e-05 x=4.84672e-05 y=0.000228549 z=-1.22865e-05 kx=-1.70095e-05 ky=0.000297224 kz=4.24903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82597e-09 l2=7.94044e-06 x=4.98421e-05 y=0.000474239 z=-3.97199e-06 kx=4.73654e-05 ky=0.000144476 kz=2.73947 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.11279e-09 l2=1.04022e-05 x=4.97287e-05 y=6.14714e-05 z=-5.20427e-06 kx=0.000110546 ky=3.35397e-05 kz=3.45858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21203e-09 l2=2.62812e-05 x=-4.82419e-05 y=-0.000443889 z=-1.31434e-05 kx=-0.000168111 ky=-3.00241e-05 kz=3.65891 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37844e-09 l2=1.94018e-05 x=4.90504e-05 y=-0.000487709 z=-9.69996e-06 kx=-9.66658e-05 ky=-0.000141568 kz=2.88735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63763e-09 l2=2.42762e-05 x=-4.85046e-05 y=-9.42371e-05 z=-1.21386e-05 kx=3.42217e-05 ky=-0.000220033 kz=4.3315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12155e-09 l2=3.97575e-05 x=-4.58793e-05 y=-0.000126555 z=-1.9878e-05 kx=6.58056e-05 ky=-4.55203e-05 kz=2.19893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23039e-09 l2=2.5378e-05 x=-4.83637e-05 y=-7.86006e-05 z=-1.26878e-05 kx=7.36068e-05 ky=-3.74425e-05 kz=1.93065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90121e-09 l2=4.75828e-06 x=-4.99435e-05 y=0.000295802 z=-2.37831e-06 kx=0.000208117 ky=4.11499e-05 kz=5.84786 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17386e-09 l2=1.59197e-05 x=4.93623e-05 y=0.000108596 z=-7.96141e-06 kx=6.01534e-05 ky=7.49123e-05 kz=3.14122 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09906e-09 l2=3.4372e-05 x=-4.69533e-05 y=-0.0003612 z=-1.71878e-05 kx=-0.000154867 ky=-6.58111e-05 kz=5.80323 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68664e-09 l2=1.71516e-05 x=4.9259e-05 y=-0.000100398 z=-8.57809e-06 kx=0.000185292 ky=-9.95105e-05 kz=6.33807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76505e-09 l2=1.98277e-05 x=-4.90077e-05 y=0.000318486 z=-9.91368e-06 kx=0.000143244 ky=0.000354445 kz=6.56897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21513e-09 l2=1.77771e-05 x=-4.92035e-05 y=0.000306613 z=-8.89205e-06 kx=-0.000251449 ky=0.000418839 kz=6.48803 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05198e-09 l2=1.332e-05 x=-4.95545e-05 y=-0.000204607 z=-6.6608e-06 kx=-3.69407e-05 ky=-0.00031953 kz=7.0218 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3387e-09 l2=1.54689e-05 x=-4.93979e-05 y=2.56887e-05 z=-7.73747e-06 kx=-0.000312427 ky=1.78139e-05 kz=6.53562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00887e-09 l2=3.12697e-05 x=-4.74922e-05 y=0.000168612 z=-1.56374e-05 kx=-0.000255392 ky=0.000373884 kz=5.9952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69771e-09 l2=1.58439e-05 x=4.93682e-05 y=4.21954e-06 z=-7.92544e-06 kx=0.000107171 ky=-9.53224e-05 kz=1.98498 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10299e-09 l2=1.94909e-05 x=4.90408e-05 y=-0.000337081 z=-9.74872e-06 kx=0.000226253 ky=4.17355e-05 kz=4.98496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17386e-09 l2=1.59197e-05 x=4.93623e-05 y=0.000108596 z=-7.96141e-06 kx=6.01534e-05 ky=7.49123e-05 kz=3.14122 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26021e-09 l2=1.29742e-05 x=-4.95771e-05 y=-0.00046414 z=-6.49019e-06 kx=-0.000319508 ky=-0.000268729 kz=6.43268 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.59343e-09 l2=1.13962e-05 x=4.96745e-05 y=4.48164e-05 z=-5.69837e-06 kx=-1.50507e-05 ky=-2.32952e-05 kz=0.715439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.26156e-09 l2=8.31574e-06 x=4.98267e-05 y=-0.000272225 z=-4.16131e-06 kx=3.74698e-05 ky=-2.70909e-05 kz=0.807665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.69159e-09 l2=1.04991e-06 x=-4.99973e-05 y=1.95228e-05 z=-5.25797e-07 kx=5.3071e-06 ky=-3.80683e-06 kz=0.132422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14251e-09 l2=1.86907e-05 x=-4.91191e-05 y=0.000385872 z=-9.34537e-06 kx=1.27905e-05 ky=-6.36263e-06 kz=1.1053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.85837e-09 l2=5.20024e-06 x=4.99324e-05 y=0.000305499 z=-2.60556e-06 kx=0.000273612 ky=0.00019047 kz=6.79381 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19079e-09 l2=1.57319e-05 x=4.93772e-05 y=-0.00020864 z=-7.86809e-06 kx=0.000208149 ky=-8.57418e-05 kz=6.63128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39345e-09 l2=1.74326e-05 x=4.92348e-05 y=4.51465e-05 z=-8.71539e-06 kx=-7.47571e-05 ky=-8.51125e-05 kz=2.25956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7767e-09 l2=1.8618e-05 x=-4.91255e-05 y=-0.000306218 z=-9.31201e-06 kx=-0.000250729 ky=-3.80821e-05 kz=5.76156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.2968e-09 l2=2.82286e-06 x=4.99801e-05 y=0.000398012 z=-1.41112e-06 kx=-9.11452e-05 ky=3.47658e-05 kz=3.12134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06892e-09 l2=1.48718e-05 x=-4.94443e-05 y=0.000422809 z=-7.43499e-06 kx=0.000120933 ky=6.30442e-06 kz=4.06654 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22974e-09 l2=2.96994e-05 x=-4.77446e-05 y=-0.00031655 z=-1.48488e-05 kx=0.000203252 ky=9.67596e-05 kz=6.56953 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0412e-09 l2=3.70315e-05 x=4.64455e-05 y=-0.00047685 z=-1.85164e-05 kx=1.9517e-06 ky=-2.96205e-05 kz=0.72283 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15349e-09 l2=4.71883e-05 x=4.40823e-05 y=-0.000135328 z=-2.35968e-05 kx=0.00030206 ky=-6.08714e-05 kz=6.55809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.06477e-09 l2=6.72629e-06 x=-4.9887e-05 y=-0.000221755 z=-3.3632e-06 kx=0.000119842 ky=-0.000104306 kz=4.05325 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45061e-09 l2=1.46984e-05 x=-4.94571e-05 y=-4.43304e-05 z=-7.34985e-06 kx=4.62938e-07 ky=9.1227e-06 kz=0.377335 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56839e-09 l2=2.41848e-05 x=4.8516e-05 y=-8.20303e-05 z=-1.20928e-05 kx=-2.28059e-06 ky=-1.4991e-05 kz=0.339997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.36292e-09 l2=5.31499e-06 x=-4.99294e-05 y=0.000251194 z=-2.66086e-06 kx=-5.63106e-05 ky=2.25632e-06 kz=4.12665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0702e-09 l2=2.18465e-05 x=4.87923e-05 y=-0.000409088 z=-1.09242e-05 kx=1.10017e-05 ky=-4.27996e-05 kz=1.24817 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09366e-09 l2=2.58687e-05 x=4.8298e-05 y=0.000121754 z=-1.29356e-05 kx=1.37692e-06 ky=2.17873e-06 kz=0.0915217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.51406e-09 l2=5.37713e-06 x=-4.99277e-05 y=4.2353e-05 z=-2.6923e-06 kx=-0.000185499 ky=-3.89734e-05 kz=4.67596 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13807e-09 l2=9.55604e-06 x=-4.97713e-05 y=-0.000155153 z=-4.77784e-06 kx=7.55845e-05 ky=9.5323e-05 kz=5.05277 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41724e-09 l2=1.33237e-05 x=-4.95545e-05 y=0.000390557 z=-6.66103e-06 kx=2.66839e-05 ky=1.7938e-05 kz=0.851721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25445e-09 l2=1.62787e-05 x=-4.93334e-05 y=0.000249095 z=-8.13866e-06 kx=0.000150164 ky=0.000258883 kz=5.5183 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04208e-09 l2=4.47788e-05 x=-4.47067e-05 y=0.000177218 z=-2.23911e-05 kx=-8.95223e-05 ky=-6.76781e-06 kz=3.46028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81541e-09 l2=1.51256e-05 x=4.94247e-05 y=0.000368013 z=-7.56462e-06 kx=8.33585e-06 ky=7.57021e-06 kz=0.453171 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49861e-09 l2=1.57123e-05 x=-4.93788e-05 y=-4.65877e-06 z=-7.85843e-06 kx=-0.000193017 ky=2.71657e-06 kz=6.30009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15581e-09 l2=2.97667e-05 x=-4.77337e-05 y=0.000443361 z=-1.4884e-05 kx=-1.65688e-06 ky=8.84039e-05 kz=1.68263 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84162e-09 l2=1.18279e-05 x=4.96492e-05 y=-0.000494456 z=-5.91401e-06 kx=-9.64164e-05 ky=-0.000331207 kz=5.65239 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80663e-09 l2=8.8276e-06 x=4.98048e-05 y=7.64248e-05 z=-4.41607e-06 kx=3.83187e-05 ky=3.24779e-05 kz=1.39894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01593e-09 l2=1.38304e-05 x=-4.95199e-05 y=0.000114898 z=-6.91361e-06 kx=0.00026343 ky=0.000339126 kz=6.19858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01356e-09 l2=2.55935e-05 x=-4.83347e-05 y=-0.000372453 z=-1.27978e-05 kx=-4.58412e-05 ky=-9.70782e-05 kz=4.03813 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.36164e-09 l2=7.72255e-06 x=4.98506e-05 y=0.000372903 z=-3.8651e-06 kx=0.000187191 ky=0.000210979 kz=3.53304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13615e-09 l2=1.59442e-05 x=-4.93602e-05 y=-0.000344586 z=-7.97402e-06 kx=-1.33268e-05 ky=-1.64787e-05 kz=0.486867 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0361e-09 l2=2.8201e-05 x=4.79712e-05 y=-0.000100848 z=-1.40996e-05 kx=-3.2549e-05 ky=-7.61374e-06 kz=1.05725 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05187e-09 l2=3.32489e-05 x=-4.71548e-05 y=-0.000340168 z=-1.66272e-05 kx=-0.000315528 ky=-0.000122048 kz=6.79005 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18132e-09 l2=1.62941e-05 x=4.93317e-05 y=-9.75097e-05 z=-8.14964e-06 kx=9.41068e-05 ky=9.01511e-05 kz=3.12827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06165e-09 l2=1.1394e-05 x=4.96743e-05 y=0.000406266 z=-5.69869e-06 kx=4.71802e-05 ky=9.42397e-05 kz=1.99505 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97497e-09 l2=1.26496e-05 x=4.95982e-05 y=-3.0575e-05 z=-6.32788e-06 kx=0.00016991 ky=-2.24245e-05 kz=4.03898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09444e-09 l2=3.32543e-06 x=-4.99724e-05 y=-0.000247033 z=-1.6639e-06 kx=-1.16498e-05 ky=-0.000246393 kz=4.18281 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93087e-09 l2=2.1786e-05 x=4.87987e-05 y=0.000424161 z=-1.08961e-05 kx=0.000291661 ky=0.000326211 kz=6.817 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10434e-09 l2=9.59375e-06 x=-4.97692e-05 y=0.000378152 z=-4.80056e-06 kx=-0.000103611 ky=7.79599e-05 kz=1.95701 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22821e-09 l2=2.17493e-05 x=4.88028e-05 y=-3.40532e-05 z=-1.0877e-05 kx=6.10927e-05 ky=1.81468e-05 kz=1.73011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16185e-09 l2=2.49474e-05 x=-4.84192e-05 y=-0.000219853 z=-1.24742e-05 kx=7.2507e-06 ky=0.000193428 kz=6.93181 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13624e-09 l2=1.08962e-05 x=4.97024e-05 y=0.000174486 z=-5.44957e-06 kx=5.76149e-05 ky=-0.000175029 kz=6.88584 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10411e-09 l2=2.96044e-05 x=-4.77595e-05 y=-0.000344953 z=-1.48009e-05 kx=0.000243808 ky=3.49699e-05 kz=6.44352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10892e-09 l2=3.61954e-05 x=4.661e-05 y=0.00049613 z=-1.80982e-05 kx=-4.26013e-06 ky=0.000651062 kz=6.80796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6298e-09 l2=7.65262e-06 x=4.98536e-05 y=0.000180113 z=-3.82499e-06 kx=-6.58192e-05 ky=-1.25416e-05 kz=1.54177 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33848e-09 l2=2.71259e-05 x=4.81258e-05 y=-0.000109715 z=-1.35626e-05 kx=-0.00015083 ky=-8.34155e-05 kz=6.87685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.20266e-09 l2=7.61167e-06 x=-4.9855e-05 y=-0.000252926 z=-3.80843e-06 kx=-0.000118709 ky=-5.01243e-05 kz=5.9643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1152e-09 l2=3.64023e-05 x=4.65699e-05 y=0.000316334 z=-1.82013e-05 kx=-3.21602e-05 ky=4.014e-05 kz=4.06414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11412e-09 l2=1.41922e-05 x=-4.94939e-05 y=6.62854e-05 z=-7.0981e-06 kx=-3.28919e-05 ky=6.48307e-05 kz=1.70601 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17959e-09 l2=5.8387e-06 x=4.99148e-05 y=-0.000189343 z=-2.92011e-06 kx=-2.96018e-05 ky=-7.48246e-05 kz=4.40239 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06384e-09 l2=3.93707e-05 x=-4.59615e-05 y=0.000146304 z=-1.9687e-05 kx=-2.14162e-05 ky=2.56496e-07 kz=0.842552 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23161e-09 l2=2.68703e-05 x=-4.81613e-05 y=0.000162458 z=-1.34358e-05 kx=8.95022e-07 ky=0.000133694 kz=6.32301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26118e-09 l2=1.50507e-05 x=-4.94308e-05 y=4.90707e-06 z=-7.5242e-06 kx=3.13421e-05 ky=-3.70226e-05 kz=0.87664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.02673e-09 l2=7.30272e-06 x=-4.98667e-05 y=-0.00048941 z=-3.65206e-06 kx=0.000102414 ky=-0.000163613 kz=6.30106 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.96727e-09 l2=1.2946e-06 x=-4.99958e-05 y=-0.000160061 z=-6.53218e-07 kx=-3.08893e-05 ky=-4.08985e-05 kz=0.634547 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.05838e-09 l2=1.4578e-05 x=4.9466e-05 y=-0.000200608 z=-7.29088e-06 kx=1.28491e-05 ky=1.10323e-05 kz=1.91107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.39186e-09 l2=9.454e-06 x=4.97763e-05 y=0.0001606 z=-4.72875e-06 kx=-8.01573e-06 ky=2.46429e-05 kz=0.885842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13532e-09 l2=3.25185e-05 x=4.72823e-05 y=-0.000362658 z=-1.6261e-05 kx=1.98775e-05 ky=-2.89938e-05 kz=0.767469 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49658e-09 l2=2.12348e-05 x=4.88596e-05 y=-0.000418362 z=-1.06193e-05 kx=0.000105407 ky=-3.2577e-05 kz=4.4642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75817e-09 l2=1.4011e-05 x=4.95066e-05 y=-0.000484429 z=-7.00869e-06 kx=4.90337e-05 ky=-1.92052e-05 kz=1.04911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63877e-09 l2=1.83968e-05 x=4.91464e-05 y=-0.000248294 z=-9.20105e-06 kx=0.000242202 ky=-9.88549e-05 kz=6.57541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.01205e-09 l2=5.11131e-06 x=4.99348e-05 y=0.000226159 z=-2.55621e-06 kx=-0.000129526 ky=-5.7933e-05 kz=6.82598 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49472e-09 l2=1.62385e-05 x=-4.93367e-05 y=-8.5181e-05 z=-8.11896e-06 kx=0.000139429 ky=-0.000171952 kz=6.54763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03005e-09 l2=2.77546e-05 x=4.80359e-05 y=0.000465025 z=-1.38774e-05 kx=-4.3197e-05 ky=0.000354104 kz=5.46243 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.27801e-09 l2=1.49995e-05 x=-4.94346e-05 y=-7.98228e-05 z=-7.50042e-06 kx=3.99472e-05 ky=-0.000143493 kz=4.05359 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00424e-09 l2=4.20704e-05 x=4.53598e-05 y=0.000147081 z=-2.10363e-05 kx=5.47313e-05 ky=3.70409e-05 kz=3.72522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96574e-09 l2=1.15299e-05 x=4.96666e-05 y=-0.000307283 z=-5.76634e-06 kx=3.43013e-05 ky=-0.000226731 kz=4.04551 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14125e-09 l2=3.65546e-05 x=-4.654e-05 y=-0.000128683 z=-1.82777e-05 kx=1.56801e-06 ky=6.44933e-07 kz=0.426422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.42221e-09 l2=1.18016e-05 x=4.96504e-05 y=-0.000341311 z=-5.90457e-06 kx=0.000145919 ky=-9.73634e-05 kz=2.83004 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33684e-09 l2=1.44076e-05 x=-4.94786e-05 y=0.000232474 z=-7.20443e-06 kx=1.80158e-05 ky=5.03678e-05 kz=1.63691 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.51898e-09 l2=9.69658e-06 x=-4.97646e-05 y=-0.00012048 z=-4.84838e-06 kx=0.000120786 ky=-3.97776e-05 kz=5.1356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38457e-09 l2=1.11708e-05 x=-4.96871e-05 y=0.000385945 z=-5.58708e-06 kx=-3.63715e-05 ky=-1.2412e-05 kz=3.76041 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08462e-09 l2=1.07005e-05 x=-4.97131e-05 y=-0.000168929 z=-5.34939e-06 kx=0.000123542 ky=-5.02059e-05 kz=4.41998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.26133e-09 l2=8.35517e-06 x=-4.98254e-05 y=0.000256738 z=-4.17754e-06 kx=0.000140039 ky=0.000276499 kz=5.97096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03863e-09 l2=2.34071e-05 x=4.86107e-05 y=0.000234659 z=-1.17057e-05 kx=7.52456e-05 ky=-1.80369e-05 kz=2.25645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07091e-09 l2=1.89236e-05 x=-4.90963e-05 y=-0.000206636 z=-9.46456e-06 kx=-0.000129093 ky=-6.12618e-05 kz=2.82068 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24591e-09 l2=2.25764e-05 x=4.87097e-05 y=0.000433578 z=-1.12867e-05 kx=-0.000159767 ky=0.000284513 kz=3.73171 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16901e-09 l2=2.30332e-05 x=4.86555e-05 y=-0.000281655 z=-1.15181e-05 kx=8.53822e-05 ky=-0.000220689 kz=4.85095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24545e-09 l2=2.67319e-05 x=4.818e-05 y=0.00046746 z=-1.33686e-05 kx=0.000239846 ky=0.000236011 kz=5.72562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07321e-09 l2=2.47722e-05 x=4.84411e-05 y=0.000171875 z=-1.23891e-05 kx=0.00015278 ky=9.5563e-05 kz=2.93469 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03351e-08 l2=1.92692e-06 x=4.99908e-05 y=0.000286488 z=-9.69041e-07 kx=4.96822e-06 ky=-1.2336e-05 kz=0.602918 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31202e-09 l2=2.84458e-05 x=-4.79352e-05 y=0.000322875 z=-1.42216e-05 kx=0.000168417 ky=0.000262346 kz=4.10534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32684e-09 l2=2.17705e-05 x=4.88005e-05 y=0.000319751 z=-1.08877e-05 kx=5.4051e-06 ky=1.00675e-05 kz=0.149436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13008e-09 l2=2.38598e-05 x=4.85562e-05 y=-0.000136611 z=-1.19299e-05 kx=-7.10341e-05 ky=0.000143944 kz=5.94948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39845e-08 l2=1.81832e-06 x=-4.99918e-05 y=-0.000381221 z=-9.18082e-07 kx=-0.000175038 ky=-0.000257252 kz=4.53742 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09322e-09 l2=2.41888e-05 x=-4.8515e-05 y=3.59039e-05 z=-1.20963e-05 kx=-0.00016037 ky=0.000214316 kz=5.58104 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24773e-09 l2=2.45457e-05 x=-4.84703e-05 y=-0.000490841 z=-1.22744e-05 kx=-0.000130249 ky=-0.000199268 kz=6.88662 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08064e-09 l2=3.28857e-05 x=4.72189e-05 y=-0.000122351 z=-1.64442e-05 kx=0.000115769 ky=-9.36561e-05 kz=6.84346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38625e-09 l2=3.20146e-05 x=4.73686e-05 y=-9.44611e-05 z=-1.60082e-05 kx=4.20573e-06 ky=-1.11732e-05 kz=1.05396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63995e-09 l2=3.12639e-05 x=4.74931e-05 y=-0.000337462 z=-1.5635e-05 kx=0.000162229 ky=-6.91058e-05 kz=3.39989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.11178e-09 l2=1.272e-05 x=-4.95942e-05 y=-0.000422882 z=-6.3606e-06 kx=7.4097e-05 ky=-0.000334782 kz=3.897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05385e-09 l2=3.60757e-05 x=4.66336e-05 y=-0.000150868 z=-1.80372e-05 kx=-4.46944e-05 ky=-6.38855e-05 kz=1.79712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35979e-09 l2=7.13391e-06 x=-4.98726e-05 y=0.000232093 z=-3.56939e-06 kx=-0.000169064 ky=0.000310035 kz=6.68189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05822e-09 l2=2.02335e-05 x=-4.89661e-05 y=-0.000459903 z=-1.01164e-05 kx=2.14429e-05 ky=-8.62991e-05 kz=1.22075 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29561e-09 l2=7.19739e-06 x=4.98704e-05 y=-3.8183e-05 z=-3.59862e-06 kx=-7.68276e-05 ky=0.000214394 kz=5.33875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06407e-09 l2=3.4948e-05 x=-4.68471e-05 y=-0.000236803 z=-1.74754e-05 kx=-7.06766e-05 ky=-2.99736e-05 kz=3.61959 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21016e-09 l2=3.28424e-05 x=4.7227e-05 y=0.000374412 z=-1.64211e-05 kx=-4.55647e-05 ky=-3.18418e-06 kz=2.88832 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47313e-09 l2=2.77694e-05 x=4.80332e-05 y=0.000209721 z=-1.38871e-05 kx=0.000144088 ky=2.34197e-05 kz=4.21903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.424e-09 l2=1.37669e-05 x=4.9524e-05 y=0.000220181 z=-6.88434e-06 kx=3.24211e-06 ky=4.04868e-05 kz=0.856947 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15441e-09 l2=6.41018e-06 x=4.98971e-05 y=-0.000460363 z=-3.20676e-06 kx=0.000151051 ky=-0.000159383 kz=6.88754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14563e-09 l2=1.05015e-05 x=-4.97234e-05 y=0.000384853 z=-5.25454e-06 kx=-0.000287439 ky=0.000201871 kz=5.3035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1149e-09 l2=3.12207e-05 x=-4.75013e-05 y=-0.00034149 z=-1.56096e-05 kx=0.000106233 ky=-4.25298e-05 kz=3.94092 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80606e-09 l2=1.76519e-05 x=4.9215e-05 y=-0.000426517 z=-8.82684e-06 kx=-4.54134e-06 ky=-0.00019788 kz=6.51665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29331e-09 l2=1.13674e-05 x=-4.96757e-05 y=-0.000331435 z=-5.68635e-06 kx=-7.34344e-05 ky=-0.000151841 kz=1.83161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14176e-09 l2=2.63871e-05 x=4.82274e-05 y=0.000443489 z=-1.31965e-05 kx=0.000195281 ky=0.000211579 kz=3.97591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07293e-09 l2=1.46532e-05 x=4.94601e-05 y=0.000355047 z=-7.32896e-06 kx=0.000180011 ky=0.000245657 kz=4.82898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5225e-09 l2=9.13803e-06 x=4.97906e-05 y=-8.47824e-05 z=-4.57221e-06 kx=0.000221721 ky=-0.000242333 kz=4.53874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13379e-09 l2=8.18206e-06 x=-4.98326e-05 y=0.000192474 z=-4.09054e-06 kx=0.000185888 ky=-0.000130247 kz=5.93255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11523e-09 l2=1.37385e-05 x=4.95256e-05 y=-0.000424144 z=-6.87225e-06 kx=0.000278268 ky=-0.000110905 kz=5.6908 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01446e-09 l2=2.60778e-05 x=4.82704e-05 y=0.000311916 z=-1.30384e-05 kx=-0.000118024 ky=0.000260458 kz=5.44643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70176e-09 l2=2.10537e-05 x=-4.88797e-05 y=-0.000262728 z=-1.05265e-05 kx=0.000160634 ky=-0.000487033 kz=6.74068 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76186e-09 l2=2.37447e-05 x=-4.85704e-05 y=-0.000413187 z=-1.18725e-05 kx=1.36906e-05 ky=-1.32884e-05 kz=0.873148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.97142e-09 l2=5.74504e-06 x=-4.99174e-05 y=-0.000230148 z=-2.87608e-06 kx=-0.000171927 ky=-5.45519e-05 kz=4.13788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26656e-09 l2=2.65378e-05 x=-4.82069e-05 y=9.50696e-05 z=-1.32714e-05 kx=-6.43426e-05 ky=7.48785e-05 kz=1.62682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.07894e-09 l2=2.83331e-05 x=-4.79517e-05 y=-9.57916e-05 z=-1.41666e-05 kx=1.60278e-05 ky=-3.58131e-05 kz=0.800103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57573e-09 l2=1.73586e-05 x=-4.9241e-05 y=0.000268368 z=-8.68071e-06 kx=-5.03968e-05 ky=5.20903e-07 kz=4.0106 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28807e-09 l2=1.73418e-05 x=4.92426e-05 y=-0.000147721 z=-8.67101e-06 kx=-5.40855e-05 ky=1.4087e-05 kz=5.14315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20037e-09 l2=3.10141e-05 x=-4.75352e-05 y=7.71542e-05 z=-1.55061e-05 kx=0.000220198 ky=0.000276539 kz=6.97877 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90705e-09 l2=2.41296e-05 x=-4.85225e-05 y=-8.06974e-05 z=-1.20672e-05 kx=-6.74704e-05 ky=6.06568e-05 kz=2.36311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00979e-09 l2=2.183e-05 x=-4.87941e-05 y=-0.000130763 z=-1.09169e-05 kx=-0.000115333 ky=-0.000248774 kz=6.74011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0694e-09 l2=6.41444e-05 x=3.83585e-05 y=-0.000461312 z=-3.20732e-05 kx=4.15142e-05 ky=-0.000173128 kz=3.23402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1185e-09 l2=2.05114e-05 x=4.89374e-05 y=0.000447737 z=-1.02544e-05 kx=-4.5747e-05 ky=3.35082e-05 kz=1.20466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45418e-09 l2=1.29081e-05 x=-4.95815e-05 y=-7.12774e-05 z=-6.45734e-06 kx=-0.000132833 ky=2.38641e-05 kz=2.55372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18926e-09 l2=1.18344e-05 x=-4.96485e-05 y=0.00044301 z=-5.9209e-06 kx=-4.8525e-05 ky=5.40594e-05 kz=0.9182 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10054e-09 l2=2.94442e-05 x=4.77832e-05 y=-0.000218345 z=-1.47242e-05 kx=4.55582e-05 ky=-2.68962e-05 kz=1.39828 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69184e-08 l2=1.51424e-06 x=-4.99944e-05 y=0.000357415 z=-7.66925e-07 kx=-7.10506e-05 ky=4.15438e-05 kz=2.6425 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00881e-09 l2=6.0104e-05 x=3.9961e-05 y=0.000101091 z=-3.0053e-05 kx=1.92565e-05 ky=4.70412e-05 kz=1.65734 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45019e-09 l2=1.55811e-05 x=-4.93892e-05 y=-5.07424e-05 z=-7.79281e-06 kx=-0.000174222 ky=0.000135484 kz=5.54474 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19506e-09 l2=2.40333e-05 x=-4.85347e-05 y=0.000154151 z=-1.20171e-05 kx=1.42947e-05 ky=0.000178616 kz=6.45592 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.54232e-09 l2=9.29455e-06 x=-4.97835e-05 y=-7.24373e-05 z=-4.6507e-06 kx=-9.39074e-05 ky=-9.86193e-05 kz=2.1657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.14222e-09 l2=6.51605e-06 x=4.98938e-05 y=0.000365504 z=-3.25971e-06 kx=1.46303e-05 ky=0.000493838 kz=6.42999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.59852e-09 l2=6.84832e-06 x=-4.98825e-05 y=-0.000342335 z=-3.42806e-06 kx=-4.37022e-05 ky=-1.2784e-05 kz=0.838841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22124e-09 l2=3.14179e-05 x=4.74691e-05 y=0.000464451 z=-1.57074e-05 kx=-0.000167137 ky=2.57257e-05 kz=3.70062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66919e-09 l2=9.64489e-06 x=-4.97669e-05 y=-0.000170767 z=-4.82452e-06 kx=-4.39516e-05 ky=-4.67224e-05 kz=1.76434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5194e-09 l2=1.49834e-05 x=-4.94354e-05 y=0.000351014 z=-7.49432e-06 kx=-0.000107205 ky=0.000216371 kz=2.85788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.4787e-09 l2=7.18103e-06 x=-4.98711e-05 y=0.000469074 z=-3.5918e-06 kx=1.93884e-05 ky=5.00597e-05 kz=2.14449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72297e-09 l2=2.49321e-05 x=-4.84215e-05 y=1.39644e-05 z=-1.2466e-05 kx=3.99297e-05 ky=-1.3225e-05 kz=2.07477 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42022e-09 l2=1.07701e-05 x=4.97092e-05 y=0.000124902 z=-5.38659e-06 kx=4.7612e-05 ky=0.000141379 kz=2.83594 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01125e-09 l2=2.45621e-05 x=-4.84681e-05 y=-0.000167854 z=-1.22828e-05 kx=-0.000152805 ky=7.73934e-06 kz=5.87022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16325e-09 l2=1.31893e-05 x=-4.95636e-05 y=0.000129104 z=-6.59393e-06 kx=0.000201465 ky=-0.000121391 kz=5.55025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15836e-09 l2=2.23137e-05 x=-4.87391e-05 y=0.000449232 z=-1.11591e-05 kx=-7.05433e-05 ky=0.000169865 kz=2.04738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26865e-09 l2=3.21167e-05 x=4.73519e-05 y=-4.41214e-05 z=-1.60572e-05 kx=-0.000246482 ky=-0.000128235 kz=6.55102 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15602e-09 l2=1.36152e-05 x=-4.95342e-05 y=0.00017396 z=-6.81007e-06 kx=-9.1438e-05 ky=8.20328e-05 kz=2.38339 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18928e-09 l2=1.88688e-05 x=-4.9102e-05 y=0.000129687 z=-9.4358e-06 kx=-2.43435e-06 ky=-9.34287e-06 kz=0.401717 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05993e-09 l2=3.08276e-05 x=4.75649e-05 y=0.000284285 z=-1.54147e-05 kx=9.11846e-06 ky=-1.37841e-05 kz=1.19374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1809e-09 l2=1.3544e-05 x=-4.95396e-05 y=0.00044455 z=-6.77109e-06 kx=4.99911e-05 ky=0.000125569 kz=1.65044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06038e-09 l2=3.35552e-05 x=-4.71007e-05 y=-0.000232088 z=-1.67799e-05 kx=-0.000221066 ky=-6.76472e-05 kz=5.96932 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1326e-09 l2=1.49219e-05 x=4.94403e-05 y=-0.000115601 z=-7.4612e-06 kx=-3.91459e-05 ky=-1.41254e-05 kz=5.74515 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.43267e-09 l2=6.74271e-06 x=-4.98864e-05 y=-0.000128533 z=-3.3755e-06 kx=-5.75127e-05 ky=1.8301e-05 kz=6.63274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1326e-09 l2=1.49219e-05 x=4.94403e-05 y=-0.000115601 z=-7.4612e-06 kx=-3.91459e-05 ky=-1.41254e-05 kz=5.74515 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.86031e-09 l2=2.96534e-06 x=4.99781e-05 y=0.00014031 z=-1.4859e-06 kx=-1.81985e-05 ky=2.71107e-05 kz=1.29301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.67786e-09 l2=7.86071e-06 x=-4.98455e-05 y=-0.000182885 z=-3.93172e-06 kx=2.85349e-06 ky=4.54121e-06 kz=0.146063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35309e-09 l2=2.38175e-05 x=4.85608e-05 y=0.000200901 z=-1.19113e-05 kx=0.000122353 ky=0.000133628 kz=3.16178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35247e-09 l2=2.86061e-05 x=-4.79105e-05 y=-0.000483521 z=-1.43047e-05 kx=-9.35647e-05 ky=-0.000129736 kz=4.58374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.46627e-09 l2=3.14432e-06 x=-4.99753e-05 y=6.82461e-05 z=-1.57585e-06 kx=-1.99091e-05 ky=3.3358e-05 kz=1.03509 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3814e-09 l2=1.36446e-05 x=4.95325e-05 y=-2.7839e-05 z=-6.82257e-06 kx=-5.71179e-05 ky=-0.000226612 kz=6.65504 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2354e-09 l2=5.34661e-05 x=-4.22524e-05 y=0.000171344 z=-2.67358e-05 kx=-0.000330443 ky=-0.000111962 kz=6.51355 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36941e-09 l2=3.81427e-05 x=-4.62204e-05 y=0.000348737 z=-1.90717e-05 kx=2.40148e-05 ky=0.000161697 kz=3.29874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15119e-09 l2=1.72259e-05 x=4.92527e-05 y=0.000207571 z=-8.6142e-06 kx=1.63762e-05 ky=0.000146058 kz=5.2005 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52243e-09 l2=1.87606e-05 x=4.9112e-05 y=-0.000108607 z=-9.38315e-06 kx=0.000274295 ky=0.000149453 kz=6.40859 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08822e-09 l2=2.3516e-05 x=-4.85981e-05 y=0.000117606 z=-1.17578e-05 kx=5.84241e-06 ky=2.15291e-05 kz=0.404637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01408e-09 l2=1.62276e-05 x=-4.9337e-05 y=0.000354625 z=-8.11657e-06 kx=-0.000102348 ky=3.26084e-05 kz=2.22455 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08967e-09 l2=3.02526e-05 x=4.76572e-05 y=-0.000395492 z=-1.5127e-05 kx=5.51189e-07 ky=-1.9698e-05 kz=0.260456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01146e-09 l2=2.21168e-05 x=-4.87623e-05 y=-0.00040032 z=-1.10572e-05 kx=0.000194669 ky=-0.000386108 kz=5.47886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87129e-09 l2=2.60192e-05 x=-4.82778e-05 y=0.000162171 z=-1.30118e-05 kx=-0.000157032 ky=0.000337794 kz=6.19938 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16826e-09 l2=2.04035e-05 x=-4.89482e-05 y=-0.000354417 z=-1.02029e-05 kx=-7.87904e-05 ky=-9.54297e-05 kz=6.236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06282e-09 l2=4.92025e-05 x=-4.35288e-05 y=0.000439098 z=-2.46027e-05 kx=-7.1129e-05 ky=0.000114739 kz=3.28721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89616e-09 l2=1.72357e-05 x=4.9252e-05 y=-0.000448074 z=-8.61825e-06 kx=-1.63222e-05 ky=-6.41687e-05 kz=1.50158 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00749e-09 l2=3.92272e-05 x=4.59916e-05 y=0.000441732 z=-1.96166e-05 kx=0.000347888 ky=4.32856e-05 kz=6.50952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90177e-09 l2=1.16302e-05 x=-4.96608e-05 y=-0.000379464 z=-5.81639e-06 kx=-8.57462e-06 ky=-5.40557e-05 kz=1.3105 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28196e-09 l2=2.3656e-05 x=-4.85815e-05 y=-6.67712e-05 z=-1.18276e-05 kx=0.000212876 ky=-0.0002462 kz=6.70994 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12078e-09 l2=3.11608e-05 x=-4.75105e-05 y=-2.13523e-05 z=-1.55816e-05 kx=-1.02898e-05 ky=2.55187e-06 kz=0.715191 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78641e-08 l2=1.73144e-06 x=-4.99927e-05 y=-7.07589e-05 z=-8.73121e-07 kx=0.000203112 ky=-0.00022693 kz=6.63232 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.895e-09 l2=1.70301e-05 x=-4.92695e-05 y=0.000215847 z=-8.51757e-06 kx=-4.35804e-05 ky=2.54002e-05 kz=1.36208 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49658e-09 l2=9.87935e-06 x=-4.97553e-05 y=0.000342975 z=-4.94184e-06 kx=-8.82417e-05 ky=0.000209631 kz=3.09609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16424e-09 l2=2.33365e-05 x=-4.86198e-05 y=0.000432971 z=-1.1668e-05 kx=8.75983e-05 ky=0.000196328 kz=4.8489 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0498e-09 l2=1.91187e-05 x=-4.90776e-05 y=0.000228413 z=-9.56098e-06 kx=-0.000106333 ky=-4.21006e-05 kz=4.75135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34797e-09 l2=4.33623e-05 x=4.50545e-05 y=0.000353879 z=-2.16829e-05 kx=9.9434e-05 ky=0.000125784 kz=4.30895 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.44355e-09 l2=9.45442e-06 x=-4.97761e-05 y=0.000412544 z=-4.73026e-06 kx=-0.000116345 ky=0.000226675 kz=4.36158 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27957e-09 l2=1.5624e-05 x=-4.93858e-05 y=-0.000142124 z=-7.8143e-06 kx=-1.65144e-05 ky=-1.93889e-05 kz=0.489463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.40908e-09 l2=1.35863e-05 x=4.95366e-05 y=-0.000259845 z=-6.79394e-06 kx=-3.07126e-05 ky=-6.4359e-05 kz=3.54398 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06683e-09 l2=1.82283e-05 x=-4.91627e-05 y=0.00032475 z=-9.11291e-06 kx=0.000228904 ky=0.000444543 kz=6.27913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.39798e-09 l2=4.2456e-06 x=4.9955e-05 y=8.9935e-05 z=-2.12482e-06 kx=-1.73855e-05 ky=7.11213e-06 kz=4.8957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53838e-09 l2=2.36005e-05 x=4.8588e-05 y=0.000336835 z=-1.18e-05 kx=-9.97738e-06 ky=-5.37617e-06 kz=0.503639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44281e-09 l2=1.86317e-05 x=4.91246e-05 y=-0.000413344 z=-9.31646e-06 kx=-6.90338e-06 ky=-0.000241142 kz=2.82521 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04984e-09 l2=1.35322e-05 x=4.95398e-05 y=0.000470211 z=-6.76929e-06 kx=0.00033674 ky=0.000562141 kz=6.30134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83076e-09 l2=1.81958e-05 x=-4.91651e-05 y=-0.00037578 z=-9.10081e-06 kx=-7.58224e-05 ky=-0.000137441 kz=1.88098 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02721e-09 l2=2.34347e-05 x=4.86079e-05 y=0.000308484 z=-1.17174e-05 kx=-5.9851e-05 ky=-7.57297e-05 kz=6.11481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20582e-09 l2=3.35338e-05 x=4.71051e-05 y=-0.000190336 z=-1.67675e-05 kx=-8.03392e-06 ky=-0.000432446 kz=6.42979 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32298e-09 l2=1.33501e-05 x=4.95527e-05 y=-5.22964e-06 z=-6.67534e-06 kx=-4.26443e-05 ky=-8.60054e-05 kz=2.46696 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13881e-09 l2=2.6612e-05 x=4.81965e-05 y=1.44217e-05 z=-1.33088e-05 kx=0.000203216 ky=-0.000104123 kz=4.39396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55198e-09 l2=2.48647e-05 x=4.84301e-05 y=0.000276671 z=-1.24322e-05 kx=-6.75274e-06 ky=1.41973e-05 kz=0.363066 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37799e-09 l2=2.23948e-05 x=-4.87303e-05 y=-0.000494257 z=-1.11976e-05 kx=6.68762e-05 ky=-0.000176771 kz=6.49707 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.17373e-09 l2=1.18438e-05 x=-4.96484e-05 y=0.000157608 z=-5.92227e-06 kx=0.000134514 ky=-9.32462e-05 kz=5.43593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.64493e-09 l2=4.6891e-06 x=-4.99451e-05 y=0.000289809 z=-2.35013e-06 kx=-9.71019e-05 ky=0.000139699 kz=2.76178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03148e-09 l2=2.17209e-05 x=4.88065e-05 y=0.000307473 z=-1.08603e-05 kx=-3.86374e-05 ky=8.34067e-05 kz=2.98207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27969e-09 l2=3.6225e-05 x=-4.66035e-05 y=0.000253191 z=-1.81151e-05 kx=-0.000277823 ky=-9.40719e-07 kz=6.50427 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.06639e-09 l2=2.43046e-05 x=4.85013e-05 y=-0.000422093 z=-1.21523e-05 kx=-1.97228e-05 ky=-6.10704e-05 kz=0.920877 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.8864e-09 l2=1.35057e-05 x=-4.95422e-05 y=-4.83607e-05 z=-6.7534e-06 kx=6.00516e-05 ky=0.00012608 kz=3.33606 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06094e-09 l2=1.91285e-05 x=4.90771e-05 y=0.0003728 z=-9.56339e-06 kx=-2.28892e-05 ky=3.60294e-05 kz=0.805985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3465e-09 l2=3.94331e-05 x=-4.59492e-05 y=-0.00034333 z=-1.97162e-05 kx=1.65929e-05 ky=-6.14385e-05 kz=0.734725 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10627e-09 l2=1.44217e-05 x=-4.94772e-05 y=7.66449e-05 z=-7.21233e-06 kx=-2.61672e-05 ky=-1.3109e-05 kz=1.41566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.424e-09 l2=2.10894e-05 x=4.88758e-05 y=-0.000232966 z=-1.05446e-05 kx=-5.18828e-05 ky=7.30489e-05 kz=3.0738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41588e-09 l2=1.29926e-05 x=4.95762e-05 y=0.000223109 z=-6.49736e-06 kx=3.62292e-05 ky=5.99382e-05 kz=5.0241 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05052e-09 l2=5.51133e-05 x=-4.17224e-05 y=0.000328955 z=-2.75554e-05 kx=0.000187812 ky=0.0002069 kz=4.53426 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1167e-09 l2=2.18688e-05 x=4.879e-05 y=-0.000244731 z=-1.09342e-05 kx=-2.63527e-05 ky=-5.40281e-05 kz=1.79874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06333e-09 l2=1.8626e-05 x=4.91254e-05 y=0.000182899 z=-9.31227e-06 kx=-9.61126e-05 ky=7.86893e-05 kz=3.79836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.58618e-09 l2=6.6258e-06 x=-4.98904e-05 y=0.000154321 z=-3.3158e-06 kx=5.68264e-06 ky=3.40879e-05 kz=0.724325 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6665e-09 l2=2.01866e-05 x=-4.89708e-05 y=-0.000106947 z=-1.00943e-05 kx=-3.42762e-06 ky=3.01098e-05 kz=1.03731 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22388e-09 l2=3.97243e-05 x=-4.58868e-05 y=4.79037e-05 z=-1.98609e-05 kx=0.000288091 ky=-0.000211182 kz=6.99973 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71708e-09 l2=1.27435e-05 x=4.95926e-05 y=-0.000487514 z=-6.3712e-06 kx=-0.000103483 ky=-0.000117091 kz=3.68477 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60337e-09 l2=1.37438e-05 x=4.95258e-05 y=8.00098e-05 z=-6.87148e-06 kx=-0.000102785 ky=0.000206212 kz=4.17212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.36918e-09 l2=6.64683e-06 x=4.98898e-05 y=0.00017419 z=-3.32488e-06 kx=-0.000149119 ky=-5.76626e-06 kz=3.34582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37523e-09 l2=2.93015e-05 x=-4.78059e-05 y=0.000114086 z=-1.46504e-05 kx=0.000105565 ky=0.000272698 kz=4.94926 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09108e-09 l2=2.70792e-05 x=-4.8132e-05 y=0.000131058 z=-1.35404e-05 kx=-1.16786e-05 ky=-4.92125e-05 kz=2.33295 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2793e-09 l2=2.38868e-05 x=-4.85532e-05 y=-2.01482e-05 z=-1.19424e-05 kx=0.000196177 ky=-0.000120471 kz=5.97374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.04384e-09 l2=8.2856e-06 x=4.98283e-05 y=-7.74525e-06 z=-4.14372e-06 kx=-5.18209e-05 ky=-6.16124e-05 kz=4.27267 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.56801e-09 l2=9.54934e-06 x=4.97716e-05 y=0.00040776 z=-4.77574e-06 kx=-2.29295e-05 ky=0.000168443 kz=5.39327 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2526e-09 l2=2.69249e-05 x=4.81536e-05 y=0.00024782 z=-1.34635e-05 kx=4.21021e-05 ky=0.000146988 kz=4.83065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13222e-09 l2=2.99491e-05 x=4.77056e-05 y=0.000482105 z=-1.49736e-05 kx=-0.000193422 ky=0.000449222 kz=6.167 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59036e-09 l2=1.25774e-05 x=-4.96033e-05 y=-0.000126354 z=-6.28737e-06 kx=8.10538e-05 ky=-5.9774e-06 kz=1.9101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40228e-09 l2=1.53831e-05 x=-4.94048e-05 y=-0.000247277 z=-7.69336e-06 kx=-0.000139124 ky=-4.93453e-05 kz=6.25384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0703e-09 l2=4.36832e-05 x=4.49763e-05 y=-0.000406633 z=-2.18445e-05 kx=4.4581e-05 ky=-7.53535e-05 kz=0.871073 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.783e-09 l2=2.08425e-05 x=-4.89019e-05 y=0.000107997 z=-1.04231e-05 kx=-0.000117259 ky=0.000121595 kz=5.75971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.78308e-09 l2=5.87793e-06 x=4.99137e-05 y=0.000444499 z=-2.94229e-06 kx=1.97511e-05 ky=5.07325e-05 kz=2.25616 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02496e-09 l2=9.37413e-06 x=4.978e-05 y=-1.82633e-05 z=-4.68734e-06 kx=-5.03916e-05 ky=7.44239e-05 kz=3.38567 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23328e-09 l2=3.17641e-05 x=-4.74112e-05 y=0.000284572 z=-1.58814e-05 kx=3.95487e-05 ky=5.14692e-05 kz=1.44564 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07844e-09 l2=2.02778e-05 x=4.89608e-05 y=-0.000260848 z=-1.01421e-05 kx=0.000359497 ky=-0.000406853 kz=6.57316 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49123e-09 l2=1.67829e-05 x=4.92909e-05 y=-0.000262726 z=-8.39215e-06 kx=-2.641e-06 ky=-4.15372e-05 kz=2.14957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75662e-09 l2=1.967e-05 x=-4.90234e-05 y=-0.000184585 z=-9.83557e-06 kx=1.25817e-05 ky=-0.000127803 kz=2.11456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14493e-09 l2=2.06168e-05 x=-4.89258e-05 y=-0.000259535 z=-1.03107e-05 kx=-0.000179345 ky=0.000133928 kz=7.00963 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11228e-09 l2=1.06982e-05 x=-4.97133e-05 y=-0.000426665 z=-5.34769e-06 kx=7.75556e-06 ky=-1.08142e-05 kz=0.19506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19242e-09 l2=3.2932e-05 x=4.72113e-05 y=0.000315133 z=-1.64661e-05 kx=-6.00603e-05 ky=0.000444455 kz=5.80589 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23027e-09 l2=1.04251e-05 x=-4.97274e-05 y=-0.000205001 z=-5.21488e-06 kx=-5.42002e-05 ky=-9.66439e-05 kz=1.56434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.40418e-09 l2=1.03014e-05 x=-4.97342e-05 y=-0.000324572 z=-5.15076e-06 kx=9.23293e-05 ky=-0.000332693 kz=4.07771 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.17942e-09 l2=1.69901e-05 x=4.92736e-05 y=0.000326808 z=-8.49526e-06 kx=-0.000112606 ky=0.00017645 kz=4.09221 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.39759e-09 l2=1.078e-05 x=4.9709e-05 y=-9.6529e-07 z=-5.39086e-06 kx=-0.000179453 ky=-0.000132129 kz=6.70678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13341e-09 l2=2.52472e-05 x=-4.83798e-05 y=0.000321588 z=-1.26263e-05 kx=-0.000246753 ky=0.000190864 kz=5.63774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86744e-09 l2=8.3208e-06 x=4.98265e-05 y=8.10758e-05 z=-4.16384e-06 kx=0.000353951 ky=-0.000241591 kz=7.03012 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96127e-09 l2=1.68256e-05 x=-4.92875e-05 y=-0.000234382 z=-8.41272e-06 kx=0.000138032 ky=-6.93695e-05 kz=6.55357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01865e-09 l2=1.38406e-05 x=4.95185e-05 y=8.44353e-06 z=-6.92303e-06 kx=0.000304677 ky=-0.000333368 kz=6.8109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40535e-09 l2=7.86225e-06 x=-4.98454e-05 y=6.76946e-05 z=-3.92993e-06 kx=8.8033e-05 ky=-5.51317e-05 kz=2.30425 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21846e-09 l2=5.84049e-06 x=4.99148e-05 y=0.00035808 z=-2.92043e-06 kx=-0.000154334 ky=-4.75925e-05 kz=5.38302 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21935e-09 l2=2.97591e-05 x=4.77354e-05 y=-0.000493126 z=-1.48785e-05 kx=-0.000210365 ky=-0.000132586 kz=6.21312 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.59355e-09 l2=3.07099e-06 x=4.99765e-05 y=0.000112082 z=-1.53643e-06 kx=-2.87869e-05 ky=0.000113735 kz=3.98563 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00904e-09 l2=1.3564e-05 x=-4.95382e-05 y=-0.000486873 z=-6.78152e-06 kx=0.000110485 ky=-0.000338009 kz=3.66228 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23919e-09 l2=2.01976e-05 x=-4.89696e-05 y=0.000471531 z=-1.00996e-05 kx=-2.26944e-05 ky=9.28674e-05 kz=5.57728 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16827e-09 l2=1.35943e-05 x=4.9536e-05 y=0.000319762 z=-6.79695e-06 kx=-7.00623e-06 ky=1.85663e-06 kz=0.445116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0872e-09 l2=1.02872e-05 x=4.97349e-05 y=-0.000315874 z=-5.14378e-06 kx=-2.70414e-05 ky=-9.55776e-05 kz=1.55197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35932e-09 l2=3.58196e-05 x=-4.66818e-05 y=-0.000207645 z=-1.79126e-05 kx=-9.08264e-05 ky=1.15125e-05 kz=2.01244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13968e-09 l2=9.81554e-06 x=-4.97585e-05 y=-0.000409642 z=-4.90918e-06 kx=-8.39421e-05 ky=-0.000307291 kz=4.97832 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00968e-09 l2=9.99541e-06 x=4.97499e-05 y=0.000117093 z=-4.9961e-06 kx=-0.000144955 ky=5.65555e-05 kz=3.40919 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25303e-09 l2=1.84803e-05 x=-4.91384e-05 y=0.000150697 z=-9.24329e-06 kx=-2.17133e-05 ky=-1.25817e-05 kz=0.422967 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35654e-09 l2=1.46085e-05 x=-4.94635e-05 y=-0.00044833 z=-7.30661e-06 kx=-0.000130785 ky=-0.000307247 kz=3.87554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07235e-09 l2=3.29696e-05 x=-4.72052e-05 y=7.94513e-05 z=-1.64834e-05 kx=4.15101e-05 ky=-1.46525e-05 kz=1.01436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87136e-09 l2=1.37528e-05 x=-4.9525e-05 y=4.98745e-05 z=-6.87771e-06 kx=-5.82385e-06 ky=8.71778e-06 kz=0.77402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22168e-09 l2=2.42224e-05 x=4.85105e-05 y=-0.000129999 z=-1.21145e-05 kx=0.000218191 ky=7.76726e-05 kz=4.00642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16979e-09 l2=2.75861e-05 x=4.80605e-05 y=0.000362098 z=-1.37921e-05 kx=-8.98604e-05 ky=5.86318e-05 kz=2.81353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4522e-09 l2=7.81782e-06 x=4.98472e-05 y=0.000231435 z=-3.90837e-06 kx=-0.000138139 ky=1.58961e-05 kz=3.89092 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27489e-09 l2=1.04167e-05 x=4.9728e-05 y=0.000148901 z=-5.20912e-06 kx=1.35013e-05 ky=0.000144466 kz=5.79679 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79618e-09 l2=1.7725e-05 x=-4.9208e-05 y=-0.000473325 z=-8.86586e-06 kx=-0.000143881 ky=-8.9403e-05 kz=2.88763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06316e-09 l2=4.1138e-05 x=4.55724e-05 y=0.000230808 z=-2.05718e-05 kx=0.000187411 ky=0.000138983 kz=3.76758 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.45498e-09 l2=1.97442e-05 x=4.90163e-05 y=-6.43835e-05 z=-9.87147e-06 kx=-0.0001542 ky=0.000140012 kz=4.0352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3471e-09 l2=1.65132e-05 x=-4.93133e-05 y=0.000110428 z=-8.25973e-06 kx=-5.02572e-05 ky=-9.8667e-06 kz=1.00645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.47965e-09 l2=8.51981e-06 x=4.98184e-05 y=0.000190165 z=-4.2612e-06 kx=-1.67745e-05 ky=0.000127798 kz=1.86978 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.21986e-09 l2=5.55361e-06 x=4.99229e-05 y=-0.000445067 z=-2.78073e-06 kx=0.00014735 ky=-7.74368e-06 kz=5.59613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36585e-09 l2=1.69284e-05 x=4.92783e-05 y=-1.39604e-05 z=-8.46598e-06 kx=8.11728e-05 ky=1.50527e-05 kz=3.57027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.81027e-09 l2=1.14109e-05 x=-4.96739e-05 y=-1.54511e-05 z=-5.70701e-06 kx=2.87655e-06 ky=5.00425e-07 kz=0.10763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.14193e-09 l2=2.62576e-06 x=-4.99829e-05 y=-0.000380267 z=-1.31747e-06 kx=-4.32172e-05 ky=-0.000133644 kz=4.17566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.85606e-09 l2=2.67877e-05 x=-4.81724e-05 y=-0.000295128 z=-1.33967e-05 kx=-0.000165852 ky=-0.000218248 kz=4.10375 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30401e-09 l2=1.69523e-05 x=4.92766e-05 y=-0.000247868 z=-8.47668e-06 kx=-5.11644e-05 ky=-3.2978e-05 kz=4.02797 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.51148e-09 l2=7.40264e-06 x=-4.9863e-05 y=0.000258485 z=-3.70201e-06 kx=8.70551e-05 ky=-8.39478e-05 kz=4.07403 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87136e-09 l2=1.37528e-05 x=-4.9525e-05 y=4.98745e-05 z=-6.87771e-06 kx=-5.82385e-06 ky=8.71778e-06 kz=0.77402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02089e-09 l2=4.08692e-05 x=-4.56334e-05 y=-0.000305668 z=-2.0436e-05 kx=-9.77362e-05 ky=2.1726e-06 kz=4.68722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69659e-09 l2=2.19929e-05 x=-4.87764e-05 y=-1.11284e-05 z=-1.09955e-05 kx=2.29492e-05 ky=1.69006e-05 kz=0.60645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12267e-09 l2=1.26366e-05 x=4.95989e-05 y=-5.1859e-06 z=-6.32134e-06 kx=0.000275855 ky=-8.67543e-05 kz=5.47612 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04127e-09 l2=1.28754e-05 x=-4.95838e-05 y=-0.000461612 z=-6.4396e-06 kx=-5.64893e-05 ky=-0.000168196 kz=3.15029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27921e-09 l2=9.17912e-06 x=-4.97888e-05 y=0.000224816 z=-4.59255e-06 kx=-5.25219e-05 ky=6.17131e-05 kz=1.11431 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26129e-09 l2=3.16789e-05 x=-4.74244e-05 y=-0.000242157 z=-1.5842e-05 kx=-0.000278754 ky=-0.000488735 kz=6.79052 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02679e-09 l2=2.35511e-05 x=4.85935e-05 y=0.000194126 z=-1.17771e-05 kx=8.43334e-05 ky=6.68304e-05 kz=4.06235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32033e-09 l2=1.93306e-05 x=-4.90568e-05 y=-0.000499831 z=-9.66836e-06 kx=-0.000155629 ky=-0.000301069 kz=4.05068 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51503e-09 l2=1.35701e-05 x=-4.95379e-05 y=-3.47892e-05 z=-6.7837e-06 kx=7.35874e-05 ky=-7.64146e-05 kz=1.72519 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56846e-09 l2=7.92579e-06 x=-4.98426e-05 y=-6.33693e-05 z=-3.96568e-06 kx=-5.47666e-05 ky=3.23723e-05 kz=1.36835 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24103e-09 l2=3.97627e-05 x=4.58781e-05 y=0.000233526 z=-1.98809e-05 kx=-4.90163e-05 ky=0.00011191 kz=2.06338 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15014e-09 l2=1.46276e-05 x=4.94621e-05 y=-0.000278759 z=-7.31651e-06 kx=0.000106724 ky=-0.000173109 kz=3.25936 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.066e-09 l2=1.98543e-05 x=4.90043e-05 y=0.000336614 z=-9.92982e-06 kx=0.000279336 ky=0.000471887 kz=6.47047 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34385e-09 l2=9.93804e-06 x=-4.97527e-05 y=-4.51229e-05 z=-4.9681e-06 kx=0.000108414 ky=0.000106638 kz=3.38824 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04425e-09 l2=1.12043e-05 x=-4.96855e-05 y=-0.000173294 z=-5.6011e-06 kx=0.000171471 ky=-0.000215632 kz=4.09194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15462e-09 l2=4.62334e-05 x=4.43363e-05 y=4.61529e-06 z=-2.3116e-05 kx=-9.45427e-05 ky=-5.22939e-05 kz=3.21541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05115e-09 l2=3.63202e-05 x=-4.65864e-05 y=-0.000330797 z=-1.81589e-05 kx=8.43982e-05 ky=2.31492e-05 kz=2.27215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09239e-09 l2=1.55276e-05 x=4.93935e-05 y=0.000375143 z=-7.76539e-06 kx=0.000115551 ky=0.000468461 kz=5.5279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.07754e-09 l2=8.43975e-06 x=-4.98216e-05 y=-0.000275718 z=-4.22206e-06 kx=-0.000113138 ky=-0.00036675 kz=4.92166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08888e-09 l2=1.65976e-05 x=-4.93063e-05 y=0.000389142 z=-8.30086e-06 kx=-9.67882e-05 ky=0.000206566 kz=3.11981 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05773e-09 l2=2.64114e-05 x=-4.82241e-05 y=-0.000332992 z=-1.32086e-05 kx=-8.09984e-06 ky=-9.94017e-06 kz=0.167482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33833e-09 l2=2.7355e-06 x=-4.99813e-05 y=0.000183751 z=-1.36838e-06 kx=5.99322e-05 ky=0.000172137 kz=5.55149 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.41739e-09 l2=7.37155e-06 x=-4.98642e-05 y=0.000415245 z=-3.68501e-06 kx=3.84266e-05 ky=3.64835e-06 kz=0.972127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07189e-09 l2=2.89132e-05 x=4.78651e-05 y=-0.000152451 z=-1.44556e-05 kx=-0.000178059 ky=-0.000315514 kz=5.44446 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.79065e-09 l2=1.71515e-05 x=4.92595e-05 y=-7.13161e-05 z=-8.57607e-06 kx=-8.12299e-05 ky=-0.000118162 kz=3.66033 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31473e-09 l2=2.81819e-05 x=4.79741e-05 y=-0.000172166 z=-1.40899e-05 kx=-1.94357e-05 ky=9.37916e-06 kz=0.555958 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32912e-09 l2=3.03668e-05 x=4.76387e-05 y=-0.000444844 z=-1.51854e-05 kx=0.000141773 ky=-0.000131202 kz=4.9311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07464e-09 l2=1.99057e-05 x=-4.89994e-05 y=-0.000132349 z=-9.95398e-06 kx=-5.87088e-05 ky=9.38905e-05 kz=4.88699 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38091e-09 l2=1.67592e-05 x=-4.92929e-05 y=-0.000471997 z=-8.38073e-06 kx=-3.42273e-05 ky=-0.000345116 kz=3.68754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.34084e-09 l2=3.84993e-06 x=-4.9963e-05 y=2.85642e-05 z=-1.92582e-06 kx=3.53847e-05 ky=-9.16543e-05 kz=2.16825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03878e-09 l2=5.09621e-05 x=4.30211e-05 y=0.000181602 z=-2.54802e-05 kx=-3.13006e-05 ky=4.47396e-05 kz=0.994238 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00693e-09 l2=2.65187e-05 x=4.82093e-05 y=-0.000340867 z=-1.32625e-05 kx=0.000377227 ky=-0.000427816 kz=6.91312 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22478e-09 l2=1.7834e-05 x=-4.91982e-05 y=0.00021203 z=-8.91978e-06 kx=-6.76266e-05 ky=6.84596e-05 kz=1.54038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0005e-09 l2=5.22981e-05 x=-4.26168e-05 y=-1.87578e-05 z=-2.61508e-05 kx=-0.000189025 ky=0.000120582 kz=6.47196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23218e-09 l2=3.01147e-05 x=4.76788e-05 y=-0.000458049 z=-1.5059e-05 kx=3.6193e-05 ky=-0.000141555 kz=1.66447 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50652e-09 l2=1.18525e-05 x=4.96474e-05 y=-0.000219965 z=-5.92924e-06 kx=0.000129727 ky=-5.78087e-05 kz=2.90127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90038e-09 l2=2.52919e-05 x=4.83749e-05 y=-0.000456408 z=-1.26458e-05 kx=-5.59875e-05 ky=-0.000243498 kz=2.57755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45202e-09 l2=3.21197e-05 x=-4.73509e-05 y=0.000197422 z=-1.60604e-05 kx=1.06218e-05 ky=-3.45323e-05 kz=2.71131 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90527e-09 l2=7.70796e-06 x=-4.98513e-05 y=7.24564e-05 z=-3.85456e-06 kx=1.77222e-05 ky=-2.32471e-05 kz=2.39695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37659e-09 l2=9.72145e-06 x=-4.97631e-05 y=-0.000193395 z=-4.86335e-06 kx=-0.000110888 ky=-0.000159826 kz=2.84872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21016e-09 l2=2.29341e-05 x=4.86672e-05 y=-0.000479393 z=-1.14686e-05 kx=9.65262e-05 ky=-0.000246111 kz=4.82733 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06585e-09 l2=2.73095e-05 x=4.8099e-05 y=5.94791e-05 z=-1.3657e-05 kx=0.000239591 ky=-0.000160471 kz=6.63766 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82772e-09 l2=1.82885e-05 x=-4.91569e-05 y=0.000120012 z=-9.14506e-06 kx=2.95234e-06 ky=6.24199e-05 kz=1.51624 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98628e-09 l2=1.96991e-05 x=-4.90202e-05 y=0.000251449 z=-9.85171e-06 kx=-0.000127311 ky=-7.65853e-05 kz=5.47877 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.49923e-09 l2=1.91177e-05 x=4.90776e-05 y=-0.00040829 z=-9.5624e-06 kx=7.50248e-05 ky=-3.33616e-05 kz=1.61718 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52021e-09 l2=1.63876e-05 x=4.93244e-05 y=-6.23876e-05 z=-8.19338e-06 kx=-9.40291e-05 ky=6.39217e-05 kz=3.88346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1299e-09 l2=2.85706e-05 x=-4.79162e-05 y=-0.000471353 z=-1.42854e-05 kx=2.27719e-05 ky=-0.000158982 kz=2.37138 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05725e-09 l2=2.1183e-05 x=-4.88653e-05 y=-0.000302843 z=-1.05926e-05 kx=-5.32179e-05 ky=1.71076e-05 kz=4.54396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69013e-08 l2=1.91744e-06 x=-4.9991e-05 y=-0.000356254 z=-9.6596e-07 kx=0.000158682 ky=-1.04771e-05 kz=6.54067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05572e-09 l2=1.94321e-05 x=4.90471e-05 y=-0.000457365 z=-9.71591e-06 kx=-7.16125e-05 ky=-0.000431285 kz=5.32273 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05098e-09 l2=4.64405e-05 x=-4.42802e-05 y=0.000130395 z=-2.32232e-05 kx=-4.41179e-05 ky=2.8932e-05 kz=0.817328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45691e-09 l2=4.04342e-05 x=4.57304e-05 y=0.000373008 z=-2.02186e-05 kx=0.000104324 ky=0.000131478 kz=5.88955 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39245e-09 l2=4.54939e-06 x=-4.99483e-05 y=-0.000243912 z=-2.2735e-06 kx=0.000200731 ky=-0.000394028 kz=5.30156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12645e-09 l2=4.14415e-05 x=4.55045e-05 y=0.000182717 z=-2.07216e-05 kx=3.88549e-05 ky=-0.000188024 kz=5.94741 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3822e-09 l2=1.90746e-05 x=-4.90821e-05 y=-0.000410179 z=-9.53816e-06 kx=-1.59587e-05 ky=-0.000439712 kz=4.83775 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.77831e-09 l2=6.27218e-06 x=4.99018e-05 y=-0.000468999 z=-3.13614e-06 kx=-0.000100472 ky=-3.68887e-05 kz=2.73311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58936e-09 l2=1.47726e-05 x=-4.94519e-05 y=-0.000327223 z=-7.38595e-06 kx=0.000117628 ky=-0.000262471 kz=3.50096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30743e-09 l2=1.28912e-05 x=4.95829e-05 y=-1.72626e-05 z=-6.44601e-06 kx=-3.41499e-06 ky=-2.60309e-05 kz=0.721932 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74403e-09 l2=7.73433e-06 x=-4.98503e-05 y=-7.48438e-05 z=-3.86742e-06 kx=4.85491e-05 ky=-0.000140489 kz=3.93906 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29414e-09 l2=7.08374e-06 x=4.98745e-05 y=-0.000402663 z=-3.54136e-06 kx=-0.000139059 ky=-0.000121881 kz=5.97132 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.87525e-09 l2=1.15992e-05 x=-4.96629e-05 y=-0.0001049 z=-5.79921e-06 kx=6.87311e-05 ky=-0.000105848 kz=1.88655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09925e-09 l2=2.26989e-05 x=-4.86948e-05 y=0.000272253 z=-1.13507e-05 kx=-9.78016e-05 ky=0.000385725 kz=6.44362 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03295e-09 l2=2.63446e-05 x=-4.82335e-05 y=0.000357242 z=-1.3174e-05 kx=-3.51886e-06 ky=-1.64162e-06 kz=0.15249 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28744e-09 l2=1.49533e-05 x=-4.94376e-05 y=-0.000194123 z=-7.47939e-06 kx=-6.81154e-05 ky=-8.27611e-05 kz=1.62053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19795e-09 l2=3.05938e-05 x=4.76026e-05 y=1.04864e-05 z=-1.5298e-05 kx=4.58337e-05 ky=0.000104707 kz=4.40823 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9771e-09 l2=1.97544e-05 x=4.90149e-05 y=0.000341722 z=-9.87841e-06 kx=3.32796e-05 ky=0.000417827 kz=6.86343 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07715e-09 l2=1.22148e-05 x=4.96254e-05 y=-0.00045096 z=-6.10998e-06 kx=8.47774e-05 ky=-9.80088e-06 kz=2.06807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.87525e-09 l2=1.15992e-05 x=-4.96629e-05 y=-0.0001049 z=-5.79921e-06 kx=6.87311e-05 ky=-0.000105848 kz=1.88655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.37584e-09 l2=2.36218e-05 x=-4.85858e-05 y=0.000417365 z=-1.18101e-05 kx=0.000269501 ky=0.000213736 kz=6.42406 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.25929e-09 l2=4.86746e-06 x=-4.99409e-05 y=-0.000454215 z=-2.43397e-06 kx=0.000113351 ky=-0.000213764 kz=2.99451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04275e-09 l2=1.50754e-05 x=-4.94283e-05 y=0.000289402 z=-7.54137e-06 kx=-0.00036801 ky=0.000220192 kz=6.83822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54793e-09 l2=1.75512e-05 x=-4.92236e-05 y=-0.000374678 z=-8.77873e-06 kx=-1.53182e-05 ky=-1.00359e-05 kz=0.318875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91218e-09 l2=2.43563e-05 x=-4.84946e-05 y=-0.000468588 z=-1.21787e-05 kx=1.37339e-05 ky=-1.68535e-05 kz=1.61582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62332e-09 l2=1.53475e-05 x=4.9408e-05 y=-0.000131519 z=-7.67267e-06 kx=-0.00017304 ky=0.000151368 kz=4.57676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69218e-09 l2=3.25335e-05 x=-4.728e-05 y=0.000459466 z=-1.62681e-05 kx=-4.01255e-05 ky=0.000324482 kz=3.40715 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02415e-09 l2=4.59106e-05 x=-4.44201e-05 y=0.00042846 z=-2.29544e-05 kx=4.15456e-05 ky=-4.31655e-06 kz=1.32465 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02642e-09 l2=2.20333e-05 x=-4.87712e-05 y=1.28699e-05 z=-1.1018e-05 kx=-0.00011314 ky=0.00028663 kz=6.912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9771e-09 l2=1.97544e-05 x=4.90149e-05 y=0.000341722 z=-9.87841e-06 kx=3.32796e-05 ky=0.000417827 kz=6.86343 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04495e-09 l2=6.64652e-05 x=3.73567e-05 y=-0.000172862 z=-3.32348e-05 kx=0.000287934 ky=-0.000351173 kz=6.5251 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19612e-09 l2=2.76854e-05 x=-4.80451e-05 y=0.000218128 z=-1.38458e-05 kx=-0.000157429 ky=1.25958e-05 kz=3.04125 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16178e-08 l2=8.37715e-07 x=-4.99984e-05 y=0.000152214 z=-4.27469e-07 kx=0.000114392 ky=0.000115233 kz=2.60267 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28128e-09 l2=2.28401e-05 x=-4.8678e-05 y=-0.000471725 z=-1.14228e-05 kx=-0.000260576 ky=-5.06113e-06 kz=6.13229 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12749e-09 l2=3.76504e-05 x=4.63207e-05 y=-0.000346831 z=-1.88265e-05 kx=1.31729e-05 ky=8.88275e-06 kz=0.834993 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53317e-09 l2=1.29851e-05 x=-4.95768e-05 y=0.000485043 z=-6.49276e-06 kx=7.156e-06 ky=6.34606e-05 kz=0.66028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61332e-09 l2=2.86231e-05 x=-4.79077e-05 y=0.000375414 z=-1.43144e-05 kx=-0.000140816 ky=-3.69696e-08 kz=3.34809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05205e-09 l2=3.04377e-05 x=4.76273e-05 y=-0.000127639 z=-1.52207e-05 kx=0.000118293 ky=0.000137548 kz=4.09657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88333e-09 l2=1.13008e-05 x=4.968e-05 y=-0.000175446 z=-5.64946e-06 kx=-0.000157005 ky=-7.04962e-05 kz=4.08852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.43491e-09 l2=6.26543e-06 x=4.99019e-05 y=0.000157725 z=-3.13457e-06 kx=-2.91341e-05 ky=0.000231023 kz=3.99256 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.59335e-09 l2=2.63403e-06 x=-4.99827e-05 y=0.000335853 z=-1.32384e-06 kx=-0.000120527 ky=-1.79028e-05 kz=2.38018 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0735e-09 l2=9.43867e-06 x=-4.97767e-05 y=-0.000374044 z=-4.72153e-06 kx=-0.000227547 ky=-0.00051152 kz=6.81618 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11544e-09 l2=1.53203e-05 x=-4.94095e-05 y=3.1003e-05 z=-7.66271e-06 kx=-2.13619e-05 ky=-1.85539e-05 kz=0.533123 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26791e-09 l2=2.01323e-05 x=4.89767e-05 y=-3.75447e-05 z=-1.00654e-05 kx=-0.000126912 ky=3.30549e-05 kz=4.51384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24125e-09 l2=2.13016e-05 x=-4.88525e-05 y=-0.000311841 z=-1.06516e-05 kx=-9.00685e-06 ky=-0.00012692 kz=2.18571 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20941e-09 l2=3.06251e-05 x=-4.75977e-05 y=0.000308895 z=-1.53134e-05 kx=-2.42391e-05 ky=0.000182645 kz=4.99061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.38568e-09 l2=1.96258e-06 x=-4.99904e-05 y=-5.77738e-05 z=-9.83805e-07 kx=-3.08135e-05 ky=6.95552e-05 kz=4.79972 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31392e-09 l2=2.81126e-05 x=4.79838e-05 y=1.61579e-05 z=-1.40567e-05 kx=-1.35044e-05 ky=-2.27067e-05 kz=3.48901 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14567e-09 l2=1.17433e-05 x=-4.96543e-05 y=-0.000301839 z=-5.87044e-06 kx=9.56413e-06 ky=-8.40645e-06 kz=0.269031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23125e-09 l2=2.1638e-05 x=-4.8816e-05 y=0.000373725 z=-1.08177e-05 kx=0.000242486 ky=-6.65867e-05 kz=6.26652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.85971e-09 l2=1.93258e-05 x=-4.90574e-05 y=0.000205778 z=-9.66488e-06 kx=-6.93299e-05 ky=0.000139411 kz=3.28562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.6323e-09 l2=2.94303e-06 x=-4.99784e-05 y=-0.000341256 z=-1.47448e-06 kx=-6.14897e-07 ky=-1.0059e-07 kz=0.210072 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47217e-09 l2=9.94518e-06 x=4.97521e-05 y=0.000355009 z=-4.97406e-06 kx=8.55591e-05 ky=0.000392944 kz=5.77506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02102e-09 l2=3.30172e-05 x=4.71963e-05 y=-0.000388743 z=-1.6509e-05 kx=-7.67327e-06 ky=-0.000274319 kz=4.04717 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.88022e-09 l2=6.26937e-06 x=4.99017e-05 y=-0.000281862 z=-3.13667e-06 kx=6.78995e-05 ky=-0.000270327 kz=6.21349 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.38151e-09 l2=8.46408e-06 x=-4.98206e-05 y=-0.000222246 z=-4.23499e-06 kx=-0.000122284 ky=-0.000194342 kz=4.83383 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13542e-09 l2=4.3199e-05 x=4.5094e-05 y=1.33079e-05 z=-2.16004e-05 kx=3.42875e-07 ky=-5.62572e-07 kz=0.0508481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18569e-09 l2=2.82853e-05 x=-4.79587e-05 y=0.000286882 z=-1.41421e-05 kx=0.000134309 ky=-7.53231e-06 kz=5.72755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.27767e-09 l2=8.31333e-06 x=-4.98272e-05 y=-0.000444147 z=-4.1583e-06 kx=0.000140014 ky=-0.00054082 kz=6.97726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3563e-09 l2=1.34704e-05 x=-4.95446e-05 y=-3.77204e-05 z=-6.73454e-06 kx=0.000140495 ky=-2.40903e-07 kz=5.16819 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.61811e-09 l2=9.50596e-06 x=4.97739e-05 y=0.00015885 z=-4.75487e-06 kx=-3.30504e-05 ky=2.22928e-05 kz=1.79359 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43113e-09 l2=1.87164e-05 x=-4.91163e-05 y=0.000457888 z=-9.36018e-06 kx=-7.71885e-06 ky=1.55363e-05 kz=0.298042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20233e-09 l2=1.62635e-05 x=-4.93342e-05 y=0.000363231 z=-8.13366e-06 kx=-0.000126246 ky=0.000295547 kz=4.68198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57285e-09 l2=1.54763e-05 x=4.9398e-05 y=-0.000394139 z=-7.73701e-06 kx=-9.32937e-05 ky=1.69129e-06 kz=2.36236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13001e-09 l2=1.14307e-06 x=-4.99967e-05 y=7.41639e-05 z=-5.74261e-07 kx=-0.000269426 ky=0.000140692 kz=6.23723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.0852e-09 l2=1.49322e-05 x=-4.94396e-05 y=3.35401e-05 z=-7.46819e-06 kx=-8.88949e-06 ky=-2.46735e-05 kz=0.827022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00319e-09 l2=3.99824e-05 x=4.583e-05 y=-0.000316635 z=-1.99913e-05 kx=-7.2596e-06 ky=-8.60619e-06 kz=0.847011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33023e-09 l2=1.81404e-05 x=-4.91703e-05 y=0.00041805 z=-9.07224e-06 kx=-0.000100743 ky=0.000128231 kz=3.65904 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50845e-09 l2=1.73255e-05 x=4.92436e-05 y=-7.90693e-05 z=-8.66559e-06 kx=0.000283518 ky=0.000222614 kz=6.61579 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46455e-09 l2=1.57604e-06 x=-4.99938e-05 y=0.000356624 z=-7.91361e-07 kx=-0.000154901 ky=2.3424e-05 kz=3.67498 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0484e-09 l2=2.54967e-05 x=4.83479e-05 y=0.000124856 z=-1.2748e-05 kx=-0.000126595 ky=-0.00015297 kz=6.92135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39154e-09 l2=1.47172e-05 x=-4.94556e-05 y=6.88944e-05 z=-7.35935e-06 kx=-6.8651e-06 ky=6.34132e-05 kz=6.36762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.96015e-09 l2=4.17952e-06 x=4.99563e-05 y=-0.000212617 z=-2.09395e-06 kx=0.000125844 ky=-0.000261914 kz=3.68196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07201e-09 l2=2.86199e-05 x=-4.79084e-05 y=0.000190298 z=-1.43114e-05 kx=-0.000130357 ky=-4.48193e-05 kz=6.68412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14058e-09 l2=4.51453e-05 x=4.46148e-05 y=-4.93662e-05 z=-2.25737e-05 kx=6.75892e-05 ky=-0.000227167 kz=6.84809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17023e-09 l2=3.4457e-05 x=-4.6938e-05 y=-0.00036935 z=-1.72299e-05 kx=-4.23621e-06 ky=-2.01348e-05 kz=0.250423 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25704e-09 l2=7.19472e-06 x=4.98705e-05 y=0.000283547 z=-3.59805e-06 kx=-4.62211e-05 ky=-6.38576e-05 kz=5.31034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09536e-09 l2=1.18231e-05 x=4.96493e-05 y=0.000238283 z=-5.91282e-06 kx=9.01888e-05 ky=-3.01845e-05 kz=6.00323 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81e-09 l2=1.00268e-05 x=-4.9748e-05 y=0.000496858 z=-5.01559e-06 kx=-0.00011281 ky=7.64742e-05 kz=4.40015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06234e-09 l2=1.50741e-05 x=4.94286e-05 y=-0.000461043 z=-7.53864e-06 kx=0.000133122 ky=-0.000556702 kz=6.1184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06694e-09 l2=4.88546e-05 x=4.36266e-05 y=-0.000379407 z=-2.4429e-05 kx=5.84715e-05 ky=-0.000103775 kz=2.15953 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10731e-08 l2=2.20362e-06 x=-4.9988e-05 y=0.000263364 z=-1.10721e-06 kx=9.54199e-06 ky=0.000174455 kz=3.4449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36352e-09 l2=2.95541e-05 x=-4.7766e-05 y=-0.00047952 z=-1.47799e-05 kx=-0.000160151 ky=-0.000153152 kz=3.45953 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19102e-09 l2=4.0978e-05 x=-4.56098e-05 y=0.000163675 z=-2.0489e-05 kx=2.64395e-05 ky=8.78751e-05 kz=1.86928 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41365e-09 l2=2.07988e-05 x=4.89064e-05 y=-4.96485e-06 z=-1.04015e-05 kx=1.81784e-05 ky=3.15963e-05 kz=0.648762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06568e-09 l2=2.75971e-05 x=4.80581e-05 y=-0.000468667 z=-1.38004e-05 kx=0.000107787 ky=-0.0002155 kz=3.88641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06691e-09 l2=2.54974e-05 x=4.83472e-05 y=0.000136147 z=-1.27505e-05 kx=1.76925e-05 ky=2.72747e-05 kz=0.662982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37032e-09 l2=1.14269e-05 x=4.96723e-05 y=0.000385307 z=-5.71611e-06 kx=1.50421e-05 ky=1.42838e-05 kz=0.373778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74437e-09 l2=1.51932e-05 x=4.942e-05 y=0.00023876 z=-7.59531e-06 kx=-0.000101511 ky=-3.28856e-05 kz=2.31712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39217e-09 l2=1.91259e-05 x=-4.90772e-05 y=0.000486317 z=-9.5632e-06 kx=6.6417e-05 ky=0.000374291 kz=6.91086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09069e-09 l2=3.83032e-05 x=-4.61863e-05 y=-0.000222927 z=-1.91538e-05 kx=-8.78948e-05 ky=-0.0001308 kz=2.39778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11413e-09 l2=3.41274e-05 x=-4.69976e-05 y=0.000195279 z=-1.70664e-05 kx=-0.000323982 ky=0.00040289 kz=7.00912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.66763e-09 l2=9.89922e-06 x=4.97547e-05 y=-0.000364709 z=-4.94942e-06 kx=-1.27588e-05 ky=-3.14921e-05 kz=0.416001 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.80798e-09 l2=5.31671e-06 x=-4.99292e-05 y=-6.31282e-06 z=-2.66237e-06 kx=-0.000110081 ky=-1.26097e-05 kz=2.10414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27506e-09 l2=3.07114e-05 x=4.75844e-05 y=9.08824e-05 z=-1.53545e-05 kx=-0.000260666 ky=0.000230436 kz=6.80559 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10004e-09 l2=1.39499e-05 x=4.9511e-05 y=-0.00034426 z=-6.97777e-06 kx=5.051e-05 ky=-1.18074e-06 kz=1.40334 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05608e-09 l2=3.4985e-05 x=-4.68408e-05 y=0.000144175 z=-1.74922e-05 kx=6.37106e-05 ky=-2.70252e-06 kz=3.83816 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0758e-09 l2=2.51178e-05 x=4.83971e-05 y=0.000209365 z=-1.25597e-05 kx=7.91685e-06 ky=3.8288e-05 kz=1.30184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07715e-09 l2=1.83743e-05 x=-4.9149e-05 y=0.000328022 z=-9.18678e-06 kx=8.96421e-06 ky=2.68784e-05 kz=0.492449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80708e-09 l2=9.6364e-06 x=-4.97673e-05 y=-5.67034e-05 z=-4.81987e-06 kx=-1.21729e-05 ky=2.01641e-05 kz=0.791191 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28906e-09 l2=2.00368e-05 x=4.89865e-05 y=0.000226165 z=-1.00174e-05 kx=-9.42461e-05 ky=3.93561e-05 kz=2.73691 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35451e-09 l2=2.95955e-05 x=-4.776e-05 y=-0.00047891 z=-1.47995e-05 kx=-4.91602e-06 ky=-1.08753e-05 kz=0.22384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00006e-09 l2=1.05095e-05 x=-4.97232e-05 y=0.000367593 z=-5.25534e-06 kx=-4.73891e-06 ky=9.84991e-05 kz=3.14577 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42205e-09 l2=7.99002e-06 x=4.98403e-05 y=-0.00033534 z=-3.99505e-06 kx=-3.63099e-05 ky=-0.00022415 kz=2.70424 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65759e-09 l2=9.39938e-06 x=-4.97785e-05 y=-0.000148748 z=-4.70261e-06 kx=-1.39871e-05 ky=1.07839e-05 kz=0.332121 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52846e-09 l2=1.31257e-05 x=-4.95673e-05 y=0.00035286 z=-6.56506e-06 kx=-0.000197771 ky=0.000354801 kz=6.81658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47973e-09 l2=2.75144e-05 x=-4.80702e-05 y=0.000301384 z=-1.37584e-05 kx=-1.66061e-05 ky=-2.30703e-05 kz=1.5993 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13945e-09 l2=3.18381e-05 x=4.73981e-05 y=-0.00025841 z=-1.59204e-05 kx=0.00010122 ky=1.08263e-05 kz=6.10963 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0098e-09 l2=2.30705e-05 x=-4.86512e-05 y=-0.000404657 z=-1.15362e-05 kx=-5.56323e-05 ky=-0.000347535 kz=5.98352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89775e-09 l2=3.26167e-05 x=-4.72657e-05 y=-0.000222153 z=-1.63101e-05 kx=-0.000121931 ky=0.000140881 kz=6.921 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08138e-09 l2=2.18424e-05 x=4.87929e-05 y=-0.000449417 z=-1.09213e-05 kx=-1.31442e-05 ky=-7.03611e-06 kz=1.47726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74927e-09 l2=1.37826e-05 x=-4.9523e-05 y=-0.000449001 z=-6.89184e-06 kx=2.10839e-05 ky=-0.000302333 kz=3.30284 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12142e-09 l2=1.72082e-05 x=4.92538e-05 y=-0.000409703 z=-8.60733e-06 kx=0.000288965 ky=-0.000284713 kz=5.33206 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39409e-09 l2=1.69538e-05 x=-4.92759e-05 y=-0.000137429 z=-8.47973e-06 kx=-0.000244477 ky=0.000179708 kz=5.64601 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08875e-09 l2=2.33298e-05 x=4.86207e-05 y=-0.000220121 z=-1.1664e-05 kx=-5.94057e-05 ky=-2.38852e-05 kz=1.99278 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20044e-09 l2=1.37623e-05 x=-4.95246e-05 y=0.000319129 z=-6.87956e-06 kx=0.000242139 ky=0.000207356 kz=5.51543 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39997e-09 l2=1.04451e-05 x=4.97267e-05 y=-0.000211072 z=-5.22184e-06 kx=-0.000114645 ky=1.58889e-05 kz=4.09695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.48699e-09 l2=1.5043e-05 x=-4.94309e-05 y=8.9542e-05 z=-7.52489e-06 kx=-0.000138732 ky=7.16733e-05 kz=3.22085 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27596e-09 l2=1.81637e-05 x=-4.91682e-05 y=0.000425787 z=-9.08346e-06 kx=-7.36494e-05 ky=0.000159403 kz=3.7257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11597e-09 l2=1.94477e-05 x=-4.90451e-05 y=0.000189504 z=-9.7262e-06 kx=-0.000254067 ky=0.000398222 kz=6.89846 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.33144e-09 l2=4.28308e-06 x=4.99542e-05 y=-0.000342899 z=-2.14218e-06 kx=-5.81954e-05 ky=-0.000108886 kz=2.84054 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5005e-09 l2=1.72093e-05 x=-4.9254e-05 y=0.000154891 z=-8.60618e-06 kx=-5.74763e-05 ky=-8.32811e-05 kz=3.64622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83349e-09 l2=1.72807e-05 x=4.92479e-05 y=-0.000425175 z=-8.64135e-06 kx=2.26255e-06 ky=-0.000109838 kz=1.55942 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13727e-09 l2=2.43951e-05 x=-4.84895e-05 y=0.000342081 z=-1.2198e-05 kx=1.67798e-06 ky=4.35306e-05 kz=0.784838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15922e-09 l2=2.40897e-05 x=-4.85276e-05 y=-0.000360467 z=-1.20458e-05 kx=-3.23107e-05 ky=-0.000224138 kz=3.99668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18695e-09 l2=1.86486e-05 x=4.91227e-05 y=-0.000491803 z=-9.32662e-06 kx=0.000161907 ky=-0.000335791 kz=4.54104 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29655e-09 l2=1.73115e-05 x=4.9245e-05 y=-0.000364576 z=-8.65778e-06 kx=0.000151716 ky=-4.40417e-05 kz=5.35714 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.40484e-09 l2=1.17402e-05 x=4.96545e-05 y=0.000249498 z=-5.87082e-06 kx=-7.02336e-05 ky=6.26472e-05 kz=3.64353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44736e-09 l2=1.69171e-05 x=4.92794e-05 y=0.000113054 z=-8.46034e-06 kx=1.9023e-05 ky=5.76764e-06 kz=1.71335 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20109e-09 l2=3.53502e-05 x=-4.67714e-05 y=0.000355532 z=-1.7677e-05 kx=-5.78094e-05 ky=9.20632e-05 kz=2.01945 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0598e-09 l2=2.63464e-05 x=4.82329e-05 y=-9.636e-05 z=-1.31762e-05 kx=4.1188e-05 ky=-3.60375e-05 kz=0.805209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.16817e-09 l2=8.89662e-06 x=4.9802e-05 y=0.000207226 z=-4.44947e-06 kx=-3.91982e-05 ky=5.53706e-05 kz=2.12069 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04821e-09 l2=1.37119e-05 x=-4.95279e-05 y=-7.99136e-05 z=-6.8557e-06 kx=4.01281e-05 ky=-3.71827e-05 kz=2.57694 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6143e-09 l2=2.52586e-05 x=4.83785e-05 y=0.000377902 z=-1.26317e-05 kx=0.000228539 ky=0.000412953 kz=6.83253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89e-09 l2=1.29254e-05 x=-4.95805e-05 y=-0.000361233 z=-6.46518e-06 kx=-0.00019855 ky=-7.64233e-05 kz=6.43976 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5757e-09 l2=2.08573e-05 x=-4.89002e-05 y=0.00036362 z=-1.04309e-05 kx=-0.000171644 ky=0.000105982 kz=5.88781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33127e-09 l2=1.67102e-05 x=4.92973e-05 y=-0.000465574 z=-8.35467e-06 kx=-0.000126808 ky=-0.00026995 kz=5.83201 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42832e-09 l2=1.7993e-05 x=4.91836e-05 y=6.21066e-06 z=-8.99985e-06 kx=0.000343344 ky=-0.00027642 kz=6.45535 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13614e-09 l2=2.56653e-05 x=4.83256e-05 y=0.000304993 z=-1.28322e-05 kx=-0.000137368 ky=-5.81328e-05 kz=6.71823 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55694e-09 l2=2.18908e-05 x=-4.87874e-05 y=-0.000292842 z=-1.09464e-05 kx=-3.16887e-05 ky=-0.00041685 kz=6.95683 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09774e-09 l2=1.87058e-05 x=-4.91176e-05 y=0.000450034 z=-9.35327e-06 kx=2.16155e-05 ky=0.000164303 kz=5.25215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.90298e-09 l2=9.96435e-06 x=-4.97514e-05 y=0.000442058 z=-4.98261e-06 kx=0.00011699 ky=0.000165961 kz=5.74244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01997e-09 l2=1.00501e-05 x=4.97469e-05 y=-0.000299981 z=-5.02539e-06 kx=-9.59664e-07 ky=-1.55144e-05 kz=0.323942 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09409e-09 l2=1.03471e-05 x=-4.97315e-05 y=0.000471153 z=-5.17581e-06 kx=-0.000232593 ky=0.000610216 kz=6.80225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.69633e-09 l2=8.94609e-06 x=4.97997e-05 y=0.000434124 z=-4.47407e-06 kx=-5.85561e-06 ky=4.40651e-05 kz=0.894809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36418e-09 l2=1.26573e-05 x=4.95979e-05 y=0.000195655 z=-6.32978e-06 kx=2.52134e-05 ky=2.4659e-05 kz=2.83243 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58558e-09 l2=1.22013e-05 x=4.96266e-05 y=0.000474071 z=-6.10149e-06 kx=-5.88552e-05 ky=0.000367625 kz=6.19665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29642e-09 l2=3.20088e-05 x=4.73687e-05 y=0.000334814 z=-1.60077e-05 kx=2.53522e-05 ky=5.16e-06 kz=0.463663 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10982e-09 l2=9.1036e-06 x=4.97922e-05 y=0.000319904 z=-4.55543e-06 kx=4.97128e-05 ky=2.23438e-05 kz=0.960613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.08007e-09 l2=7.7369e-06 x=4.98502e-05 y=0.000338429 z=-3.87e-06 kx=5.33446e-05 ky=0.000195397 kz=5.21658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17096e-09 l2=1.82377e-05 x=-4.91612e-05 y=-3.02253e-05 z=-9.12126e-06 kx=-8.70265e-05 ky=3.15645e-05 kz=2.34306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1656e-09 l2=2.02899e-05 x=4.89602e-05 y=0.000355112 z=-1.01452e-05 kx=-2.32638e-05 ky=0.000118723 kz=3.36795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.20134e-09 l2=1.73202e-05 x=-4.92449e-05 y=0.000312462 z=-8.65917e-06 kx=7.56936e-05 ky=2.9982e-05 kz=1.82158 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.98888e-09 l2=8.54626e-06 x=4.98172e-05 y=0.000271656 z=-4.27546e-06 kx=2.44774e-05 ky=0.000129734 kz=3.6553 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.00073e-09 l2=9.89831e-06 x=4.97545e-05 y=0.000324065 z=-4.95153e-06 kx=3.88936e-05 ky=5.55324e-06 kz=2.19903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49541e-09 l2=2.85616e-05 x=4.7917e-05 y=7.10136e-05 z=-1.42831e-05 kx=0.000205296 ky=0.000123235 kz=6.51646 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3728e-09 l2=2.8431e-05 x=4.79372e-05 y=-9.98465e-06 z=-1.42148e-05 kx=-1.3741e-05 ky=-1.69578e-05 kz=0.479385 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38996e-09 l2=1.06616e-05 x=4.97152e-05 y=-0.000198905 z=-5.33027e-06 kx=-8.83252e-05 ky=-0.000108283 kz=3.6109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00928e-09 l2=1.78261e-05 x=4.91993e-05 y=0.000193434 z=-8.91335e-06 kx=-2.86946e-06 ky=3.29406e-05 kz=0.731239 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1885e-09 l2=4.3725e-05 x=4.49666e-05 y=-0.000116159 z=-2.18645e-05 kx=0.000221362 ky=6.93702e-05 kz=6.85741 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47035e-09 l2=2.12394e-05 x=-4.8859e-05 y=-0.000155155 z=-1.06221e-05 kx=-8.38829e-05 ky=-0.000147735 kz=2.42013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75739e-09 l2=1.2157e-05 x=-4.96294e-05 y=-0.000204322 z=-6.07816e-06 kx=3.14251e-05 ky=-7.34399e-05 kz=1.27894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16809e-09 l2=1.96967e-05 x=-4.90203e-05 y=0.00045243 z=-9.85052e-06 kx=-6.71681e-05 ky=6.10982e-05 kz=2.10271 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96725e-09 l2=2.45385e-05 x=-4.84709e-05 y=0.000337337 z=-1.22728e-05 kx=-3.0493e-05 ky=2.43873e-05 kz=0.565704 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.29671e-09 l2=1.40682e-05 x=4.95032e-05 y=0.000106617 z=-7.03451e-06 kx=-8.64755e-05 ky=1.87609e-05 kz=3.50397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07744e-09 l2=1.05528e-05 x=-4.97207e-05 y=-0.000187554 z=-5.27876e-06 kx=-9.24359e-05 ky=-9.83572e-05 kz=2.50665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69319e-09 l2=2.40212e-05 x=4.85366e-05 y=-0.000455165 z=-1.20099e-05 kx=-1.36155e-05 ky=-1.94044e-05 kz=0.422614 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10443e-09 l2=5.56716e-05 x=4.15347e-05 y=-0.000478982 z=-2.78376e-05 kx=0.000202276 ky=-0.000387961 kz=6.59112 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38847e-09 l2=1.21078e-05 x=4.96319e-05 y=-6.77317e-05 z=-6.05726e-06 kx=0.000275333 ky=0.000114136 kz=5.12702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58019e-09 l2=1.35225e-05 x=4.95407e-05 y=0.00032528 z=-6.763e-06 kx=6.3125e-05 ky=2.36862e-05 kz=3.24913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09152e-09 l2=3.35537e-05 x=4.71007e-05 y=3.29254e-05 z=-1.67797e-05 kx=5.02312e-06 ky=2.83594e-06 kz=0.10159 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58235e-09 l2=1.87219e-05 x=4.91158e-05 y=-0.000251627 z=-9.36328e-06 kx=5.29556e-05 ky=1.03788e-05 kz=1.71162 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14931e-09 l2=3.26252e-05 x=-4.72647e-05 y=-7.89976e-05 z=-1.6312e-05 kx=3.26523e-05 ky=-5.63265e-05 kz=1.33562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83407e-09 l2=1.84266e-05 x=4.9144e-05 y=-0.000358747 z=-9.21426e-06 kx=1.14936e-06 ky=-0.000145328 kz=3.11318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73333e-09 l2=7.06343e-06 x=4.98753e-05 y=0.000290606 z=-3.53102e-06 kx=-4.75931e-05 ky=8.30983e-05 kz=1.51593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.56762e-09 l2=1.31621e-05 x=-4.95651e-05 y=0.000321415 z=-6.58392e-06 kx=-8.05367e-05 ky=-4.79191e-06 kz=3.61386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38879e-09 l2=3.18688e-05 x=-4.73938e-05 y=0.00023017 z=-1.59334e-05 kx=1.40006e-05 ky=1.53684e-05 kz=0.401207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57048e-09 l2=9.23937e-06 x=-4.97864e-05 y=-0.000339872 z=-4.6188e-06 kx=0.000192286 ky=-0.000305338 kz=5.71812 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72742e-09 l2=2.1104e-05 x=-4.88742e-05 y=0.000361029 z=-1.05524e-05 kx=3.97077e-05 ky=7.80103e-05 kz=4.15487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60445e-09 l2=1.60331e-05 x=-4.9353e-05 y=-6.09515e-05 z=-8.01907e-06 kx=-0.000127274 ky=-0.000138922 kz=3.63386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34051e-09 l2=2.23402e-05 x=-4.87368e-05 y=0.000357501 z=-1.11692e-05 kx=3.52989e-05 ky=5.92438e-05 kz=1.12061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16008e-09 l2=4.9472e-05 x=-4.34536e-05 y=0.000106293 z=-2.47355e-05 kx=0.000163554 ky=0.000124387 kz=6.44103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.33611e-09 l2=6.859e-06 x=4.98823e-05 y=-0.000195284 z=-3.43461e-06 kx=5.20937e-06 ky=-6.15229e-06 kz=0.106347 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59323e-09 l2=1.89689e-05 x=-4.90925e-05 y=-0.00014419 z=-9.48454e-06 kx=1.61057e-05 ky=-4.85543e-05 kz=1.09131 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57568e-09 l2=9.92085e-06 x=-4.97536e-05 y=6.74223e-05 z=-4.95903e-06 kx=0.000238192 ky=-0.00013994 kz=5.43527 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04808e-09 l2=2.36423e-05 x=-4.85829e-05 y=0.000140045 z=-1.18207e-05 kx=7.94737e-06 ky=-1.61029e-06 kz=0.411285 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39914e-09 l2=2.24697e-05 x=4.87216e-05 y=4.61585e-05 z=-1.12355e-05 kx=8.23537e-08 ky=-8.27526e-06 kz=2.64051 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38524e-09 l2=4.01467e-05 x=-4.57942e-05 y=-0.00019481 z=-2.00735e-05 kx=4.85828e-05 ky=6.64062e-05 kz=3.79669 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65059e-09 l2=2.86286e-05 x=-4.79077e-05 y=0.000164274 z=-1.43142e-05 kx=6.03464e-06 ky=5.01282e-06 kz=0.302482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55462e-09 l2=2.72715e-05 x=4.81055e-05 y=-0.000478528 z=-1.36348e-05 kx=-0.000229928 ky=-7.26124e-05 kz=6.48253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49493e-09 l2=2.82839e-05 x=-4.7958e-05 y=9.20247e-05 z=-1.41446e-05 kx=-0.000168212 ky=-8.39015e-05 kz=4.15448 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31932e-09 l2=3.6142e-05 x=4.66212e-05 y=0.000278477 z=-1.80696e-05 kx=-8.43019e-05 ky=3.68049e-05 kz=1.9138 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.5517e-09 l2=1.22231e-05 x=-4.96251e-05 y=0.000382663 z=-6.11398e-06 kx=-8.10211e-05 ky=0.000107478 kz=3.5499 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32871e-09 l2=2.01191e-05 x=-4.8978e-05 y=0.000406195 z=-1.00588e-05 kx=8.49708e-05 ky=0.000255699 kz=2.88858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47255e-09 l2=1.2681e-05 x=4.95963e-05 y=0.00032954 z=-6.34264e-06 kx=0.000168697 ky=0.000110085 kz=5.93241 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03501e-09 l2=3.07191e-05 x=4.75821e-05 y=-0.000293179 z=-1.53614e-05 kx=1.22208e-05 ky=-3.21345e-05 kz=0.424803 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12543e-09 l2=1.84755e-05 x=4.91393e-05 y=-0.000186047 z=-9.23867e-06 kx=4.87844e-05 ky=-0.000110673 kz=6.8956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03828e-09 l2=1.68507e-05 x=4.92851e-05 y=-8.4062e-05 z=-8.42584e-06 kx=-1.24111e-06 ky=-0.000104606 kz=2.31336 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46713e-09 l2=1.15188e-05 x=4.96673e-05 y=6.47027e-05 z=-5.76012e-06 kx=-4.24898e-06 ky=-0.00025423 kz=5.90834 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22943e-09 l2=2.52843e-05 x=4.83757e-05 y=0.000199796 z=-1.26423e-05 kx=-7.03206e-05 ky=0.00019537 kz=6.9676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21625e-09 l2=3.30676e-05 x=4.71876e-05 y=-0.000417228 z=-1.65339e-05 kx=-7.08234e-05 ky=-0.000280074 kz=6.55427 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21505e-09 l2=3.3869e-05 x=4.70458e-05 y=0.000131378 z=-1.69332e-05 kx=-7.66836e-05 ky=8.08176e-05 kz=1.85348 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34652e-09 l2=1.37073e-05 x=-4.95285e-05 y=-0.000143068 z=-6.85288e-06 kx=7.2573e-05 ky=-1.34598e-05 kz=1.86104 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09234e-09 l2=7.72832e-06 x=4.98506e-05 y=-5.17852e-05 z=-3.86419e-06 kx=-0.00011208 ky=-6.30319e-06 kz=5.50331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46183e-09 l2=7.4221e-06 x=4.98623e-05 y=-9.40964e-06 z=-3.71034e-06 kx=-0.000113701 ky=-0.000142201 kz=2.9192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.36853e-09 l2=2.92663e-05 x=4.78108e-05 y=0.000361498 z=-1.46355e-05 kx=0.000169238 ky=0.000249468 kz=6.96708 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04047e-09 l2=2.76058e-05 x=-4.8057e-05 y=0.000268243 z=-1.3804e-05 kx=-7.76792e-05 ky=9.15993e-05 kz=6.43277 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01097e-09 l2=1.65651e-05 x=4.9309e-05 y=-0.000232487 z=-8.28587e-06 kx=0.000166161 ky=-6.2502e-05 kz=3.5457 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4493e-09 l2=1.15472e-05 x=4.96654e-05 y=-0.000217525 z=-5.7763e-06 kx=0.000104128 ky=6.64148e-05 kz=2.61724 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96964e-09 l2=1.33725e-05 x=4.95507e-05 y=7.35978e-05 z=-6.68967e-06 kx=0.000257164 ky=-4.1575e-05 kz=5.20776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.96059e-09 l2=7.82277e-06 x=-4.98468e-05 y=0.000156094 z=-3.91644e-06 kx=-3.13221e-05 ky=2.21154e-05 kz=0.606875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10987e-09 l2=1.32741e-05 x=-4.95573e-05 y=-0.000359439 z=-6.63999e-06 kx=-0.000261208 ky=-0.00029869 kz=5.44933 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02097e-09 l2=1.19464e-05 x=-4.96423e-05 y=-0.000292916 z=-5.97253e-06 kx=0.000235677 ky=-0.000114171 kz=7.03107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01567e-09 l2=1.70093e-05 x=4.92713e-05 y=-5.69047e-05 z=-8.50708e-06 kx=0.000184359 ky=-4.91833e-05 kz=6.4057 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67701e-09 l2=1.29592e-05 x=-4.95782e-05 y=-6.38896e-05 z=-6.48365e-06 kx=-0.000123376 ky=4.90632e-06 kz=2.27845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.13796e-09 l2=4.92401e-06 x=-4.99395e-05 y=-0.000249045 z=-2.46363e-06 kx=1.34105e-06 ky=-1.30168e-06 kz=0.151063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.29206e-09 l2=1.02289e-05 x=4.97378e-05 y=-0.000134447 z=-5.11713e-06 kx=0.000130558 ky=9.0119e-05 kz=6.13872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76277e-09 l2=1.13168e-05 x=-4.96789e-05 y=-0.000211066 z=-5.65884e-06 kx=3.04992e-06 ky=8.22813e-06 kz=0.331972 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.85014e-09 l2=8.58674e-06 x=-4.98156e-05 y=0.000386467 z=-4.29365e-06 kx=5.38042e-05 ky=7.88554e-05 kz=1.63062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1726e-09 l2=3.87246e-05 x=4.60993e-05 y=0.000163482 z=-1.93624e-05 kx=-7.27516e-05 ky=-0.00014267 kz=7.00566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42938e-09 l2=2.64658e-05 x=-4.82173e-05 y=-8.51003e-05 z=-1.32337e-05 kx=-8.13668e-06 ky=6.16631e-06 kz=4.23621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31344e-09 l2=1.63391e-05 x=4.93284e-05 y=9.94349e-06 z=-8.16884e-06 kx=-2.80869e-05 ky=-1.90111e-05 kz=1.03141 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76149e-09 l2=2.35822e-05 x=-4.85899e-05 y=-2.10824e-05 z=-1.17925e-05 kx=-2.23025e-05 ky=4.58831e-05 kz=2.02298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21385e-09 l2=3.22128e-05 x=-4.73348e-05 y=-0.000301465 z=-1.61077e-05 kx=-6.84156e-05 ky=-7.48152e-05 kz=4.36601 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15291e-09 l2=3.37016e-05 x=-4.70756e-05 y=-0.000408256 z=-1.68503e-05 kx=0.000153106 ky=-1.41703e-05 kz=6.30131 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04174e-09 l2=1.32749e-05 x=4.95574e-05 y=0.000308654 z=-6.63926e-06 kx=7.44376e-05 ky=0.00013807 kz=2.86124 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5987e-09 l2=2.95728e-06 x=-4.99782e-05 y=-0.000365229 z=-1.47994e-06 kx=5.03309e-06 ky=-2.04102e-05 kz=0.507678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05706e-09 l2=2.66346e-05 x=-4.81938e-05 y=-0.000261718 z=-1.33188e-05 kx=-6.79741e-05 ky=-0.000119822 kz=3.29907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12573e-09 l2=1.38801e-05 x=4.95162e-05 y=-0.000106867 z=-6.94088e-06 kx=-2.43959e-06 ky=-8.4636e-06 kz=0.478652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22959e-09 l2=2.4866e-05 x=-4.84299e-05 y=-0.000114355 z=-1.24328e-05 kx=1.92028e-06 ky=-1.19566e-06 kz=0.120402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49864e-09 l2=9.58362e-06 x=-4.97699e-05 y=1.52604e-05 z=-4.79244e-06 kx=1.57409e-05 ky=0.000175892 kz=6.81815 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.08314e-09 l2=3.9877e-06 x=-4.99602e-05 y=-0.000268176 z=-1.99858e-06 kx=-8.44741e-05 ky=1.54323e-05 kz=1.56664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0482e-09 l2=2.60191e-05 x=-4.8278e-05 y=-0.000469049 z=-1.301e-05 kx=6.45532e-06 ky=-0.000363806 kz=5.17447 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17902e-09 l2=1.96987e-05 x=-4.902e-05 y=7.96876e-05 z=-9.85182e-06 kx=-6.53452e-05 ky=7.73854e-05 kz=1.71583 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38955e-09 l2=3.35615e-06 x=4.99718e-05 y=-0.000288261 z=-1.68188e-06 kx=0.000120528 ky=-9.21658e-05 kz=2.30686 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76454e-09 l2=9.42575e-06 x=-4.97774e-05 y=-0.00035977 z=-4.71431e-06 kx=-7.50411e-05 ky=-0.000466048 kz=6.72838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36743e-09 l2=1.12966e-05 x=-4.96798e-05 y=9.22037e-05 z=-5.65114e-06 kx=-0.000184454 ky=0.000249178 kz=4.24916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05827e-09 l2=1.39399e-05 x=-4.95122e-05 y=0.000156094 z=-6.96959e-06 kx=4.0864e-05 ky=1.68781e-05 kz=1.43402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38174e-09 l2=1.58193e-05 x=4.93708e-05 y=0.000150838 z=-7.90884e-06 kx=-6.83161e-05 ky=9.22624e-05 kz=2.23179 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16719e-09 l2=2.42836e-05 x=4.85039e-05 y=-2.73011e-05 z=-1.2141e-05 kx=-2.6285e-05 ky=-2.06463e-05 kz=0.899585 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28556e-09 l2=1.16325e-05 x=4.96607e-05 y=-6.36716e-05 z=-5.81676e-06 kx=-4.38531e-06 ky=-5.20933e-05 kz=1.86751 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10109e-09 l2=2.82118e-05 x=-4.79697e-05 y=-0.000108805 z=-1.41047e-05 kx=3.72184e-05 ky=-2.99831e-05 kz=1.04246 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14127e-09 l2=3.84451e-05 x=4.61578e-05 y=0.000301735 z=-1.92225e-05 kx=-6.52764e-05 ky=-7.73196e-05 kz=5.09315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23822e-09 l2=1.81459e-05 x=-4.91702e-05 y=-0.000257563 z=-9.07294e-06 kx=5.74895e-05 ky=0.000104962 kz=4.59405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84674e-09 l2=1.49778e-05 x=4.94359e-05 y=-0.000370826 z=-7.49162e-06 kx=2.45999e-05 ky=-4.36783e-05 kz=0.679193 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10932e-09 l2=2.04704e-05 x=4.89408e-05 y=-0.000297036 z=-1.02383e-05 kx=0.000260123 ky=-0.000149655 kz=4.97353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07421e-09 l2=3.21991e-05 x=4.73378e-05 y=0.000151454 z=-1.60987e-05 kx=-4.77683e-05 ky=6.13962e-05 kz=1.60862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47262e-09 l2=2.89276e-05 x=4.78623e-05 y=-0.000414406 z=-1.44653e-05 kx=3.11491e-05 ky=-0.000133294 kz=1.98372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25658e-09 l2=7.30487e-06 x=4.98663e-05 y=-0.000133496 z=-3.6553e-06 kx=0.000299294 ky=4.69946e-05 kz=6.65067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23924e-09 l2=3.10175e-06 x=-4.9976e-05 y=0.000216644 z=-1.55188e-06 kx=1.07516e-05 ky=1.20707e-05 kz=4.89662 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38237e-09 l2=3.18025e-05 x=-4.74046e-05 y=0.000244076 z=-1.59011e-05 kx=5.63886e-05 ky=2.43811e-05 kz=3.32954 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.06384e-09 l2=1.61377e-05 x=4.93445e-05 y=-7.90567e-05 z=-8.07205e-06 kx=0.000138405 ky=6.49179e-05 kz=3.17706 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01835e-09 l2=5.01884e-06 x=4.99371e-05 y=-4.79686e-05 z=-2.51006e-06 kx=-4.79079e-05 ky=-7.3751e-05 kz=6.36236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53533e-09 l2=1.88043e-05 x=-4.91079e-05 y=-0.000401749 z=-9.40432e-06 kx=-0.000199411 ky=-0.000360202 kz=6.88933 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5762e-09 l2=1.2492e-05 x=-4.96087e-05 y=4.37309e-05 z=-6.24494e-06 kx=3.78534e-05 ky=5.98452e-06 kz=1.01626 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01371e-09 l2=1.80902e-05 x=4.9175e-05 y=-0.000328964 z=-9.04631e-06 kx=7.47279e-05 ky=-0.000384497 kz=5.30458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15745e-09 l2=1.28957e-05 x=-4.95826e-05 y=-9.28637e-05 z=-6.44905e-06 kx=-1.26048e-05 ky=-0.000237152 kz=5.99144 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02007e-09 l2=3.6524e-05 x=4.65466e-05 y=-7.59949e-05 z=-1.82607e-05 kx=-9.892e-05 ky=-5.16466e-05 kz=2.48136 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67407e-09 l2=4.79478e-06 x=-4.99425e-05 y=-0.000288631 z=-2.39969e-06 kx=-0.000122523 ky=-0.000328975 kz=6.35499 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2013e-09 l2=2.4828e-05 x=4.84339e-05 y=0.000246956 z=-1.24172e-05 kx=0.000191065 ky=0.000163837 kz=3.50306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58495e-09 l2=9.2039e-06 x=4.97881e-05 y=0.00028543 z=-4.60113e-06 kx=-8.2368e-05 ky=5.98666e-06 kz=1.94692 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09596e-09 l2=2.73832e-05 x=-4.80886e-05 y=9.29744e-05 z=-1.36938e-05 kx=-0.000164522 ky=0.0001409 kz=4.70416 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65088e-09 l2=2.54517e-05 x=4.83541e-05 y=5.05173e-05 z=-1.27251e-05 kx=-4.77314e-05 ky=1.25171e-05 kz=1.44402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97423e-09 l2=1.64215e-05 x=4.93211e-05 y=-0.000449998 z=-8.21344e-06 kx=0.000180794 ky=-0.000346999 kz=5.29213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4191e-09 l2=3.5576e-05 x=4.67289e-05 y=6.99202e-05 z=-1.77892e-05 kx=4.73305e-05 ky=0.000132378 kz=4.11028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28581e-09 l2=3.57781e-05 x=4.66905e-05 y=0.000136238 z=-1.78899e-05 kx=2.25404e-05 ky=-0.000153801 kz=6.78674 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90871e-09 l2=2.2009e-05 x=4.87741e-05 y=-0.000322857 z=-1.10059e-05 kx=2.75352e-05 ky=-0.000203544 kz=3.04296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7817e-09 l2=2.68136e-05 x=4.81693e-05 y=-0.000339625 z=-1.34076e-05 kx=-7.36849e-07 ky=-7.14692e-06 kz=0.336117 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15166e-09 l2=1.64063e-05 x=-4.93223e-05 y=-8.87249e-05 z=-8.20518e-06 kx=-0.000166243 ky=-0.000181937 kz=5.72753 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24146e-09 l2=3.14659e-05 x=4.74603e-05 y=0.000272637 z=-1.57341e-05 kx=7.19592e-05 ky=0.000394579 kz=6.71448 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06606e-09 l2=1.33857e-05 x=4.955e-05 y=-0.000404453 z=-6.69398e-06 kx=9.92198e-06 ky=-4.13526e-05 kz=0.821581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01077e-09 l2=3.97305e-06 x=-4.99604e-05 y=-0.000265767 z=-1.9895e-06 kx=-4.31127e-05 ky=-5.65772e-07 kz=0.87352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22925e-09 l2=1.55422e-05 x=-4.93924e-05 y=4.4796e-05 z=-7.77327e-06 kx=-7.82746e-05 ky=9.40101e-05 kz=3.73236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01608e-09 l2=2.40832e-05 x=-4.85285e-05 y=-5.44788e-05 z=-1.20419e-05 kx=1.15158e-05 ky=5.60979e-05 kz=3.0294 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79682e-09 l2=9.25755e-06 x=-4.97855e-05 y=0.000472801 z=-4.62855e-06 kx=8.09922e-05 ky=8.76537e-05 kz=3.58568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82449e-09 l2=9.04054e-06 x=4.97954e-05 y=-0.000371089 z=-4.52068e-06 kx=-6.18229e-05 ky=-0.000462943 kz=6.11711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72281e-09 l2=1.35022e-05 x=-4.95419e-05 y=0.000246698 z=-6.7543e-06 kx=-0.000319551 ky=-7.51079e-06 kz=6.8193 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.06558e-09 l2=1.42652e-05 x=-4.94886e-05 y=-0.000188342 z=-7.1353e-06 kx=-0.00022806 ky=-0.000129576 kz=6.70039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2754e-09 l2=3.10201e-05 x=4.75333e-05 y=0.000131493 z=-1.55119e-05 kx=4.59634e-05 ky=-3.03719e-05 kz=1.73865 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03345e-09 l2=3.66754e-05 x=-4.65152e-05 y=-7.35065e-05 z=-1.83405e-05 kx=-0.000179014 ky=-0.000106446 kz=3.66218 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17456e-09 l2=1.97482e-05 x=4.90155e-05 y=0.000421189 z=-9.87442e-06 kx=-2.87724e-05 ky=-1.64633e-05 kz=5.12408 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37426e-09 l2=1.31979e-05 x=-4.95624e-05 y=0.000192898 z=-6.60225e-06 kx=-0.000225063 ky=0.000291805 kz=4.26777 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26227e-09 l2=2.59987e-05 x=-4.82808e-05 y=-0.000201183 z=-1.3e-05 kx=-1.87258e-06 ky=-8.34123e-05 kz=2.81958 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20812e-09 l2=4.13547e-05 x=-4.55245e-05 y=-0.000297978 z=-2.06778e-05 kx=2.4385e-05 ky=-0.000344363 kz=6.5377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.72628e-09 l2=4.74776e-06 x=-4.99436e-05 y=0.000301045 z=-2.37921e-06 kx=-8.59447e-05 ky=0.000125954 kz=1.74037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34322e-09 l2=1.2581e-05 x=4.96026e-05 y=-0.000339998 z=-6.29375e-06 kx=7.23284e-05 ky=-7.31999e-06 kz=1.71532 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25488e-09 l2=3.86673e-05 x=-4.61115e-05 y=5.44906e-05 z=-1.93333e-05 kx=3.70718e-05 ky=6.70429e-05 kz=1.71375 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42186e-09 l2=2.22649e-05 x=4.87452e-05 y=0.000424467 z=-1.11327e-05 kx=-5.23627e-05 ky=0.000500272 kz=5.50331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01192e-09 l2=1.76519e-05 x=4.92147e-05 y=0.000330627 z=-8.82783e-06 kx=0.000137615 ky=-4.25344e-05 kz=4.99652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26158e-09 l2=3.17527e-05 x=4.7412e-05 y=0.000367266 z=-1.5879e-05 kx=0.000116615 ky=0.000133878 kz=2.73657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.28675e-09 l2=2.60056e-06 x=-4.99832e-05 y=-0.000301043 z=-1.30419e-06 kx=1.01439e-05 ky=-8.07202e-05 kz=2.17804 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38459e-09 l2=1.91435e-05 x=4.90757e-05 y=-0.000160758 z=-9.57081e-06 kx=-5.95673e-05 ky=4.39008e-05 kz=1.81187 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00081e-09 l2=2.30612e-05 x=4.86529e-05 y=-0.000310313 z=-1.1529e-05 kx=-9.49709e-05 ky=-6.16538e-05 kz=2.22765 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49437e-09 l2=1.62401e-05 x=4.93367e-05 y=-6.05945e-05 z=-8.11878e-06 kx=-0.000208244 ky=0.000135658 kz=5.14111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1024e-09 l2=2.29036e-05 x=-4.86713e-05 y=6.7266e-05 z=-1.14512e-05 kx=7.67675e-06 ky=1.72363e-05 kz=0.319732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7728e-09 l2=2.70453e-05 x=-4.81367e-05 y=-9.52392e-05 z=-1.35244e-05 kx=-1.95757e-05 ky=-3.98867e-05 kz=1.13182 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.31522e-09 l2=5.03485e-06 x=4.99365e-05 y=0.000410138 z=-2.5213e-06 kx=7.43553e-05 ky=5.49433e-05 kz=1.3669 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90334e-09 l2=3.35919e-06 x=4.99718e-05 y=-0.000394325 z=-1.68035e-06 kx=-1.12646e-05 ky=-1.403e-05 kz=2.91438 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04487e-09 l2=6.89807e-06 x=4.98809e-05 y=0.000321362 z=-3.4501e-06 kx=3.28005e-05 ky=0.000134203 kz=3.03165 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90817e-09 l2=2.18613e-05 x=4.87905e-05 y=0.000119876 z=-1.09331e-05 kx=0.000212313 ky=0.000339262 kz=6.76491 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.01471e-09 l2=3.08544e-06 x=-4.99763e-05 y=0.000218078 z=-1.54493e-06 kx=7.14795e-05 ky=0.000144353 kz=2.7583 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1756e-09 l2=3.00464e-05 x=-4.76895e-05 y=0.00049277 z=-1.50248e-05 kx=-7.33073e-06 ky=3.01519e-05 kz=0.352805 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08688e-09 l2=3.265e-05 x=4.72592e-05 y=-0.000369639 z=-1.63279e-05 kx=0.000299749 ky=-0.000176503 kz=5.89091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43966e-09 l2=1.47117e-05 x=-4.94563e-05 y=-0.00034509 z=-7.35614e-06 kx=2.57642e-05 ky=-8.08636e-05 kz=1.38574 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.21719e-09 l2=3.8266e-06 x=4.99635e-05 y=-0.000467075 z=-1.91649e-06 kx=1.45925e-07 ky=-5.47284e-06 kz=0.0837455 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.609e-09 l2=2.99509e-05 x=4.77044e-05 y=8.52886e-05 z=-1.49779e-05 kx=3.57564e-05 ky=3.53199e-05 kz=1.00538 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24022e-09 l2=1.74608e-05 x=4.92316e-05 y=-0.000425408 z=-8.73323e-06 kx=0.00022999 ky=-0.000275938 kz=5.16211 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.63777e-09 l2=5.05381e-06 x=-4.99362e-05 y=-0.000423463 z=-2.52917e-06 kx=-1.92588e-05 ky=-0.000159247 kz=2.16649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70227e-09 l2=1.0037e-05 x=4.97475e-05 y=-4.82436e-06 z=-5.02077e-06 kx=5.84683e-05 ky=9.82469e-05 kz=2.01973 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10451e-09 l2=1.58816e-05 x=4.93655e-05 y=9.12596e-05 z=-7.94145e-06 kx=1.46952e-05 ky=-6.86348e-05 kz=6.79542 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02634e-09 l2=3.2553e-05 x=4.72773e-05 y=0.000245764 z=-1.62755e-05 kx=-0.000185636 ky=0.000267976 kz=5.85786 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10147e-09 l2=3.3324e-05 x=4.71424e-05 y=0.000460665 z=-1.66621e-05 kx=-3.50496e-06 ky=1.62564e-05 kz=0.413391 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.19063e-09 l2=7.27813e-06 x=4.98676e-05 y=2.81013e-05 z=-3.63862e-06 kx=-8.66251e-05 ky=-7.33448e-05 kz=2.81712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35183e-09 l2=1.05099e-05 x=4.97234e-05 y=0.000134336 z=-5.25374e-06 kx=-9.60574e-05 ky=0.000152154 kz=2.51762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.08364e-09 l2=1.56269e-06 x=-4.99939e-05 y=-0.000243629 z=-7.84281e-07 kx=-2.38906e-06 ky=-1.06905e-06 kz=0.304148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44127e-09 l2=3.84032e-06 x=-4.99632e-05 y=-0.000307461 z=-1.92089e-06 kx=1.46834e-05 ky=1.66056e-05 kz=1.49163 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04092e-09 l2=9.89927e-06 x=4.97546e-05 y=-0.000333143 z=-4.94913e-06 kx=-1.08905e-05 ky=-1.65173e-05 kz=0.527059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07937e-09 l2=4.23201e-05 x=-4.53021e-05 y=0.000176213 z=-2.11605e-05 kx=3.11893e-06 ky=0.000219339 kz=3.42935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02984e-09 l2=3.81608e-05 x=4.62157e-05 y=0.000273726 z=-1.90826e-05 kx=0.000237599 ky=0.000233807 kz=6.61747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48061e-09 l2=1.4035e-05 x=4.95051e-05 y=-0.000367146 z=-7.01899e-06 kx=9.36007e-05 ky=-0.000519781 kz=6.12012 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68485e-09 l2=1.88553e-05 x=-4.91033e-05 y=-0.000419878 z=-9.42866e-06 kx=-9.04166e-06 ky=-8.54942e-06 kz=2.63762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59311e-09 l2=1.93239e-05 x=4.90577e-05 y=0.00010424 z=-9.66301e-06 kx=3.37869e-05 ky=3.29473e-05 kz=6.83428 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02687e-09 l2=2.8563e-05 x=-4.79168e-05 y=-6.63673e-05 z=-1.42833e-05 kx=-2.59911e-05 ky=2.69961e-05 kz=0.991726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28544e-09 l2=2.24898e-05 x=-4.87194e-05 y=0.000232124 z=-1.12459e-05 kx=1.35839e-05 ky=-4.79387e-05 kz=4.02067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4727e-09 l2=2.25385e-05 x=4.87135e-05 y=-0.000300447 z=-1.12708e-05 kx=1.98391e-05 ky=-8.43326e-05 kz=1.20268 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.09754e-09 l2=9.08972e-06 x=4.97933e-05 y=0.000380632 z=-4.54567e-06 kx=-1.93451e-06 ky=3.87507e-06 kz=0.0775875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18599e-09 l2=2.77798e-05 x=4.80317e-05 y=3.45969e-06 z=-1.38919e-05 kx=0.000197502 ky=-3.88731e-05 kz=6.55986 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20947e-09 l2=1.79341e-05 x=4.91891e-05 y=-0.000233446 z=-8.96973e-06 kx=4.40556e-05 ky=-4.09079e-05 kz=1.04197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10801e-09 l2=3.5468e-05 x=-4.67504e-05 y=0.00035975 z=-1.77325e-05 kx=0.000103852 ky=0.000117631 kz=2.32153 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10658e-09 l2=2.46945e-05 x=-4.84518e-05 y=-0.000363531 z=-1.23469e-05 kx=1.34334e-05 ky=-4.27853e-05 kz=0.737243 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15424e-09 l2=1.54097e-05 x=-4.94031e-05 y=5.35895e-05 z=-7.70376e-06 kx=8.69581e-06 ky=1.09663e-05 kz=0.258935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43846e-09 l2=7.5112e-06 x=-4.98587e-05 y=0.000440719 z=-3.75922e-06 kx=-0.000127571 ky=3.65951e-05 kz=2.64725 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7406e-09 l2=1.2233e-05 x=-4.96244e-05 y=-0.000184162 z=-6.11847e-06 kx=-4.80423e-05 ky=-0.000132799 kz=2.19365 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48599e-09 l2=1.78653e-05 x=4.91958e-05 y=0.000432424 z=-8.93327e-06 kx=-1.89152e-06 ky=7.58548e-05 kz=0.956887 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52466e-09 l2=1.71018e-05 x=4.92637e-05 y=-1.46047e-05 z=-8.55039e-06 kx=-0.000144353 ky=5.69174e-05 kz=5.6071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30394e-09 l2=2.30258e-05 x=4.86567e-05 y=0.000438895 z=-1.15132e-05 kx=-3.77983e-05 ky=0.000110498 kz=4.85672 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52487e-09 l2=2.26458e-05 x=-4.87011e-05 y=-0.000291445 z=-1.13244e-05 kx=-5.67181e-05 ky=-0.000143147 kz=4.00641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0432e-09 l2=1.09423e-05 x=4.96998e-05 y=-0.000160494 z=-5.47302e-06 kx=5.33865e-05 ky=-0.000144411 kz=3.09373 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.74818e-09 l2=3.43771e-06 x=-4.99705e-05 y=0.000465462 z=-1.72493e-06 kx=-0.00010921 ky=0.000136288 kz=2.4757 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61226e-09 l2=2.94532e-05 x=-4.77823e-05 y=3.41018e-05 z=-1.47275e-05 kx=-1.13228e-07 ky=-2.90311e-08 kz=0.106619 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06128e-09 l2=3.24134e-05 x=4.73011e-05 y=-1.24133e-05 z=-1.62062e-05 kx=-9.43108e-05 ky=6.07959e-05 kz=4.26304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19445e-09 l2=3.31303e-05 x=4.71757e-05 y=0.000472102 z=-1.65678e-05 kx=2.30949e-05 ky=2.73836e-05 kz=0.541924 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87196e-09 l2=1.65805e-05 x=4.93081e-05 y=-0.000188567 z=-8.29125e-06 kx=1.09168e-05 ky=-2.9342e-05 kz=6.73056 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.7725e-09 l2=3.6636e-06 x=4.99664e-05 y=0.000310498 z=-1.83522e-06 kx=0.000155295 ky=4.37659e-05 kz=5.05582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53803e-09 l2=2.68356e-05 x=-4.81663e-05 y=0.000396965 z=-1.34182e-05 kx=6.31992e-06 ky=6.86658e-06 kz=0.81063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17173e-09 l2=2.15402e-05 x=-4.88263e-05 y=0.00044197 z=-1.07714e-05 kx=-6.87933e-05 ky=2.14916e-06 kz=4.85216 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4258e-09 l2=1.86701e-05 x=4.91212e-05 y=0.000420833 z=-9.33569e-06 kx=-7.79806e-05 ky=0.000180752 kz=6.4304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.23707e-09 l2=1.42796e-05 x=4.9488e-05 y=-0.000481157 z=-7.14032e-06 kx=-5.57034e-05 ky=-1.05728e-05 kz=2.50501 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97192e-09 l2=9.79378e-06 x=-4.97596e-05 y=-0.000102219 z=-4.89881e-06 kx=-2.40691e-05 ky=4.66039e-05 kz=1.28652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46659e-09 l2=1.09947e-05 x=-4.96968e-05 y=-0.000302857 z=-5.49948e-06 kx=-3.93531e-05 ky=1.35202e-05 kz=1.41714 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29668e-09 l2=2.39761e-05 x=4.85422e-05 y=-0.000369291 z=-1.1987e-05 kx=-0.000139481 ky=-0.000310528 kz=4.07231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16141e-09 l2=4.99465e-05 x=4.33158e-05 y=-0.000187861 z=-2.4976e-05 kx=0.000333104 ky=-0.000270975 kz=6.75574 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42757e-09 l2=1.3927e-05 x=4.95126e-05 y=-0.000139056 z=-6.96574e-06 kx=0.000105223 ky=2.49631e-05 kz=3.42622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58062e-09 l2=2.22913e-05 x=-4.87424e-05 y=0.000336759 z=-1.11453e-05 kx=0.000119866 ky=1.75787e-05 kz=4.92055 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71653e-09 l2=1.30395e-05 x=4.95732e-05 y=-0.000255321 z=-6.52069e-06 kx=1.05995e-05 ky=6.63782e-05 kz=5.00272 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.25547e-09 l2=3.60425e-06 x=-4.99677e-05 y=0.000173742 z=-1.80395e-06 kx=7.87125e-05 ky=6.39814e-05 kz=3.01743 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05058e-09 l2=8.91266e-06 x=4.98011e-05 y=-0.000405712 z=-4.45788e-06 kx=4.83199e-05 ky=-6.84164e-05 kz=4.62608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.53858e-09 l2=9.04922e-06 x=4.97951e-05 y=-0.000376143 z=-4.52433e-06 kx=-7.71886e-05 ky=-0.000173617 kz=2.47983 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10922e-09 l2=2.02917e-05 x=4.89595e-05 y=0.000196612 z=-1.01482e-05 kx=7.4568e-05 ky=-5.74241e-05 kz=2.02218 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.85744e-09 l2=9.69879e-07 x=-4.99977e-05 y=0.000394548 z=-4.88372e-07 kx=-6.22278e-05 ky=1.10361e-05 kz=6.18155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.61059e-09 l2=1.61483e-05 x=-4.93441e-05 y=-0.000253979 z=-8.07477e-06 kx=2.3904e-05 ky=2.33381e-06 kz=1.67038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18278e-09 l2=1.54293e-05 x=4.94016e-05 y=-0.000274838 z=-7.71365e-06 kx=-0.000125179 ky=5.48217e-05 kz=3.8468 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25474e-09 l2=4.31332e-05 x=-4.51103e-05 y=-6.73517e-05 z=-2.15666e-05 kx=2.28494e-05 ky=1.42612e-05 kz=1.69277 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7253e-09 l2=1.22085e-05 x=4.96258e-05 y=0.000495083 z=-6.10715e-06 kx=0.000272429 ky=0.000311027 kz=6.63659 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.29899e-09 l2=5.90817e-06 x=4.99126e-05 y=-8.41772e-05 z=-2.95771e-06 kx=0.000225616 ky=4.8781e-05 kz=5.69003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.188e-09 l2=2.17052e-05 x=4.88083e-05 y=7.01458e-06 z=-1.08536e-05 kx=-6.48381e-06 ky=-8.63746e-05 kz=3.20712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89326e-09 l2=1.69932e-05 x=4.92728e-05 y=-6.68409e-05 z=-8.49831e-06 kx=9.90967e-05 ky=-0.000221741 kz=6.59387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57557e-09 l2=1.08462e-05 x=4.97051e-05 y=-0.000353522 z=-5.42402e-06 kx=1.70127e-05 ky=-0.000361172 kz=6.36271 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79105e-09 l2=2.56365e-05 x=-4.83292e-05 y=1.18492e-05 z=-1.28193e-05 kx=-8.42793e-06 ky=6.8196e-05 kz=3.21257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12775e-09 l2=1.86283e-05 x=-4.9125e-05 y=0.000486511 z=-9.31416e-06 kx=1.24529e-05 ky=4.4463e-05 kz=1.15905 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12015e-09 l2=2.90587e-05 x=4.7843e-05 y=0.000221728 z=-1.45287e-05 kx=-2.22579e-05 ky=-2.19601e-05 kz=0.877448 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28061e-09 l2=1.64602e-05 x=4.93185e-05 y=-0.000125093 z=-8.22941e-06 kx=-0.000136436 ky=-0.000176586 kz=3.66382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29398e-09 l2=3.27329e-05 x=4.72452e-05 y=2.13484e-07 z=-1.63685e-05 kx=0.000207917 ky=8.87057e-05 kz=6.74096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38341e-09 l2=1.9374e-05 x=4.90527e-05 y=0.00024422 z=-9.68797e-06 kx=3.27492e-05 ky=0.000255903 kz=6.06476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48514e-09 l2=1.22424e-05 x=4.96242e-05 y=-0.00045317 z=-6.12061e-06 kx=-8.31739e-05 ky=-9.08033e-05 kz=3.04965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36402e-09 l2=2.22796e-05 x=-4.87433e-05 y=0.00031491 z=-1.1141e-05 kx=-3.30212e-05 ky=1.53381e-06 kz=3.21159 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19682e-09 l2=2.73028e-05 x=4.81002e-05 y=-5.66906e-05 z=-1.3653e-05 kx=7.83468e-05 ky=-0.000183029 kz=3.54154 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16092e-09 l2=2.33593e-05 x=4.86171e-05 y=0.000410139 z=-1.16793e-05 kx=-7.97729e-05 ky=0.000378069 kz=4.20689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49737e-09 l2=1.3363e-05 x=4.95517e-05 y=-0.000428165 z=-6.68221e-06 kx=-6.41468e-07 ky=-8.77702e-05 kz=1.57597 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6333e-09 l2=2.38607e-05 x=4.8556e-05 y=-9.83921e-06 z=-1.19313e-05 kx=8.47895e-06 ky=7.77283e-05 kz=3.36282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81043e-09 l2=2.42463e-05 x=4.85085e-05 y=-0.000217605 z=-1.2123e-05 kx=-4.77938e-06 ky=5.532e-07 kz=0.23212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7022e-09 l2=1.81721e-05 x=4.91674e-05 y=-0.000357697 z=-9.0884e-06 kx=0.000107516 ky=-8.65112e-05 kz=3.50251 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29057e-09 l2=1.17546e-05 x=4.96533e-05 y=-0.000380727 z=-5.87925e-06 kx=4.0765e-05 ky=-4.37862e-05 kz=1.57094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15456e-09 l2=2.96125e-05 x=-4.77573e-05 y=0.000204866 z=-1.4808e-05 kx=-5.2822e-05 ky=8.31008e-05 kz=2.21371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86725e-09 l2=2.77125e-05 x=-4.80422e-05 y=-0.000487908 z=-1.38562e-05 kx=0.000133725 ky=-0.000131148 kz=6.7382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.56307e-09 l2=1.45817e-05 x=4.94654e-05 y=-0.000490572 z=-7.29438e-06 kx=0.000229431 ky=-0.000496154 kz=5.06766 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30494e-09 l2=1.2852e-05 x=-4.95851e-05 y=-0.000388251 z=-6.42923e-06 kx=-1.5928e-05 ky=-1.62027e-06 kz=0.307114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.56343e-09 l2=8.63614e-06 x=4.98133e-05 y=-0.000240803 z=-4.32232e-06 kx=7.37409e-05 ky=-0.000121697 kz=2.50562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78746e-09 l2=1.59535e-05 x=-4.93596e-05 y=-6.9847e-05 z=-7.97885e-06 kx=-3.90429e-06 ky=-2.87114e-06 kz=0.162429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79286e-09 l2=1.95972e-05 x=4.90308e-05 y=0.000158259 z=-9.79877e-06 kx=-1.95578e-05 ky=-3.44377e-05 kz=1.35637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96964e-09 l2=2.30981e-06 x=4.99867e-05 y=0.000230171 z=-1.15469e-06 kx=-5.1511e-05 ky=-4.93405e-05 kz=2.14356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28094e-09 l2=2.37083e-05 x=4.85747e-05 y=0.000116557 z=-1.18544e-05 kx=-3.92294e-06 ky=-5.69714e-06 kz=0.498244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.277e-09 l2=1.31601e-05 x=4.95653e-05 y=2.3937e-05 z=-6.58011e-06 kx=-3.72391e-05 ky=-8.08004e-05 kz=3.07549 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14109e-09 l2=3.65377e-05 x=-4.65422e-05 y=-0.000141844 z=-1.82719e-05 kx=-0.000345304 ky=-0.00034116 kz=6.58493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05386e-09 l2=3.61974e-05 x=4.66099e-05 y=0.00046191 z=-1.80985e-05 kx=-7.00677e-05 ky=0.000301544 kz=4.39279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70528e-09 l2=7.10976e-06 x=4.98736e-05 y=0.000428916 z=-3.55582e-06 kx=-6.90001e-06 ky=6.05887e-06 kz=0.821783 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68908e-09 l2=2.06476e-05 x=-4.89231e-05 y=3.28967e-05 z=-1.03232e-05 kx=0.000196807 ky=-0.000210084 kz=6.91966 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70052e-09 l2=2.80135e-05 x=-4.79979e-05 y=-6.95792e-07 z=-1.40089e-05 kx=-0.000123064 ky=0.000209047 kz=4.5694 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41373e-09 l2=1.41675e-05 x=4.94955e-05 y=0.000124462 z=-7.08655e-06 kx=2.36816e-05 ky=-1.52833e-05 kz=0.56464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28551e-09 l2=1.52193e-05 x=4.94179e-05 y=0.000144348 z=-7.60842e-06 kx=-0.000215562 ky=0.000152955 kz=5.67797 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.55115e-09 l2=1.21958e-05 x=-4.96272e-05 y=-0.000308747 z=-6.09694e-06 kx=0.000151433 ky=-0.000240849 kz=3.38533 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0823e-09 l2=5.28714e-05 x=4.24398e-05 y=0.00019515 z=-2.64371e-05 kx=3.51202e-05 ky=4.41499e-05 kz=1.66234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.44023e-09 l2=8.26179e-06 x=4.9829e-05 y=6.41024e-05 z=-4.13477e-06 kx=0.000198746 ky=1.47166e-05 kz=4.60091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07006e-09 l2=1.24109e-05 x=-4.96134e-05 y=-0.000249585 z=-6.20705e-06 kx=-8.25508e-05 ky=-0.000133763 kz=3.80392 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69894e-09 l2=1.55229e-05 x=-4.93938e-05 y=-0.000398833 z=-7.76418e-06 kx=-6.16997e-05 ky=-0.000143427 kz=1.62063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54815e-09 l2=1.38244e-05 x=4.95198e-05 y=-0.000142981 z=-6.91454e-06 kx=9.17994e-05 ky=-0.000154792 kz=2.94629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27808e-09 l2=1.94164e-05 x=-4.90489e-05 y=-0.000406002 z=-9.70741e-06 kx=0.000123675 ky=-0.000307043 kz=4.2192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.48086e-09 l2=7.28186e-06 x=4.98675e-05 y=0.000473091 z=-3.64039e-06 kx=-0.000218405 ky=9.78537e-05 kz=6.11838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79286e-09 l2=1.95972e-05 x=4.90308e-05 y=0.000158259 z=-9.79877e-06 kx=-1.95578e-05 ky=-3.44377e-05 kz=1.35637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22592e-09 l2=2.51494e-05 x=-4.83925e-05 y=-0.000132191 z=-1.25777e-05 kx=-0.000179362 ky=-8.54119e-05 kz=3.67046 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39589e-09 l2=2.5315e-05 x=4.83716e-05 y=0.000155895 z=-1.26578e-05 kx=-4.48722e-05 ky=0.000314471 kz=5.0792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01172e-09 l2=3.18552e-05 x=-4.73953e-05 y=-8.8056e-05 z=-1.59284e-05 kx=-2.43262e-05 ky=0.000136603 kz=4.22449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02417e-09 l2=3.36458e-05 x=-4.70844e-05 y=-0.000402362 z=-1.68253e-05 kx=-0.000160744 ky=-0.000181515 kz=3.95584 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05481e-09 l2=3.05798e-05 x=-4.76045e-05 y=-0.00022455 z=-1.5292e-05 kx=-3.39265e-05 ky=2.53035e-05 kz=1.04555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4142e-09 l2=9.29072e-06 x=4.97836e-05 y=-0.000435755 z=-4.64777e-06 kx=0.000100319 ky=-0.000181349 kz=2.94253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1714e-09 l2=2.20683e-05 x=-4.87676e-05 y=-3.71411e-05 z=-1.1034e-05 kx=9.41782e-05 ky=-0.00010416 kz=5.7756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29188e-09 l2=3.08202e-05 x=4.75661e-05 y=-0.000248527 z=-1.54113e-05 kx=1.44542e-05 ky=1.37223e-05 kz=1.15323 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36225e-08 l2=2.06064e-06 x=-4.99895e-05 y=0.000289586 z=-1.03979e-06 kx=-0.000140442 ky=7.85669e-05 kz=2.64115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1277e-09 l2=3.24204e-05 x=-4.73001e-05 y=-8.25922e-05 z=-1.62091e-05 kx=3.17689e-05 ky=-4.46787e-06 kz=0.917036 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15933e-09 l2=2.12217e-05 x=-4.88615e-05 y=0.000427752 z=-1.06102e-05 kx=7.50185e-05 ky=0.000182326 kz=2.92552 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4312e-09 l2=2.61262e-05 x=-4.8264e-05 y=-0.000135638 z=-1.30622e-05 kx=0.000173467 ky=-3.54928e-05 kz=5.14127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70632e-09 l2=4.54397e-06 x=4.99484e-05 y=-0.000432452 z=-2.27241e-06 kx=-2.44305e-05 ky=-0.000194365 kz=2.82644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04572e-09 l2=2.35754e-05 x=4.85911e-05 y=-0.000352455 z=-1.17867e-05 kx=-1.48477e-05 ky=-3.24068e-05 kz=0.465947 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83361e-09 l2=1.7304e-05 x=-4.92457e-05 y=-0.000358673 z=-8.65397e-06 kx=-9.96726e-05 ky=-0.000365824 kz=4.64406 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01612e-09 l2=3.34391e-05 x=4.71211e-05 y=-0.000136661 z=-1.67222e-05 kx=1.74489e-05 ky=-9.92745e-06 kz=0.383658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11841e-09 l2=2.68843e-05 x=4.81591e-05 y=0.000242953 z=-1.34438e-05 kx=6.68157e-05 ky=0.000185176 kz=2.9868 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04516e-09 l2=3.99455e-05 x=-4.58371e-05 y=0.000344516 z=-1.9975e-05 kx=-4.1206e-05 ky=6.88207e-05 kz=1.08404 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08718e-09 l2=4.34183e-05 x=4.50425e-05 y=-0.000460394 z=-2.17076e-05 kx=-0.000315571 ky=-0.000303715 kz=7.0056 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05023e-09 l2=3.52294e-05 x=4.67943e-05 y=0.000476223 z=-1.76163e-05 kx=0.00012008 ky=0.000433684 kz=5.29762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24032e-09 l2=1.2206e-05 x=4.96265e-05 y=0.000246638 z=-6.10195e-06 kx=-0.000275245 ky=2.96552e-05 kz=6.30576 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10183e-09 l2=2.13817e-05 x=-4.88432e-05 y=0.00017735 z=-1.06941e-05 kx=-0.000269615 ky=0.000106065 kz=4.91896 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00626e-09 l2=2.17741e-05 x=-4.88005e-05 y=0.000465157 z=-1.08874e-05 kx=7.43102e-07 ky=2.13318e-05 kz=0.249244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02367e-09 l2=8.43369e-06 x=4.98219e-05 y=-0.000366943 z=-4.21885e-06 kx=1.81152e-05 ky=-5.31954e-05 kz=0.9097 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10035e-09 l2=5.58114e-05 x=-4.14895e-05 y=-0.000100148 z=-2.79049e-05 kx=0.000106763 ky=9.7015e-05 kz=3.20291 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03222e-09 l2=3.54479e-05 x=4.6754e-05 y=0.000417072 z=-1.77229e-05 kx=-0.000237536 ky=0.000205715 kz=6.93716 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.93272e-09 l2=7.31136e-06 x=-4.98663e-05 y=-0.000330622 z=-3.65844e-06 kx=-3.8837e-05 ky=-4.0112e-05 kz=6.51226 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.26649e-09 l2=1.07265e-05 x=4.97119e-05 y=-0.000407937 z=-5.36237e-06 kx=-0.000149158 ky=2.66231e-05 kz=3.70682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45671e-09 l2=3.97256e-05 x=-4.58862e-05 y=0.000183038 z=-1.98624e-05 kx=4.47711e-05 ky=7.87169e-05 kz=1.75155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00364e-09 l2=1.86447e-05 x=-4.91233e-05 y=0.000303047 z=-9.32318e-06 kx=-7.46547e-06 ky=7.01404e-05 kz=1.19609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0922e-09 l2=1.63742e-05 x=-4.93254e-05 y=0.000295165 z=-8.18677e-06 kx=4.94436e-05 ky=0.000115381 kz=2.72666 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22615e-09 l2=8.6708e-06 x=4.98117e-05 y=0.000132128 z=-4.33776e-06 kx=0.000109846 ky=2.55132e-05 kz=4.368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12858e-09 l2=3.70097e-05 x=4.6449e-05 y=0.000491893 z=-1.85077e-05 kx=0.000111654 ky=0.000209179 kz=2.28322 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13192e-09 l2=2.15037e-05 x=-4.88299e-05 y=0.000419267 z=-1.07546e-05 kx=-0.000270185 ky=0.000351425 kz=5.96629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44657e-09 l2=9.13974e-06 x=4.9791e-05 y=0.000304489 z=-4.56871e-06 kx=-9.07391e-05 ky=0.000162012 kz=2.39726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11731e-09 l2=1.65813e-05 x=4.93078e-05 y=-0.000321433 z=-8.29228e-06 kx=0.00011716 ky=-0.000141753 kz=5.32655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08666e-09 l2=5.1967e-05 x=4.27193e-05 y=-0.000422598 z=-2.5983e-05 kx=-8.03152e-05 ky=2.02564e-05 kz=3.31369 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41984e-09 l2=2.1492e-05 x=-4.88319e-05 y=-0.000466135 z=-1.07459e-05 kx=3.12036e-05 ky=-0.000151751 kz=1.78091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48849e-09 l2=1.94062e-05 x=4.905e-05 y=0.000458413 z=-9.7021e-06 kx=-9.3556e-05 ky=3.83862e-05 kz=2.60204 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15783e-09 l2=2.72611e-05 x=-4.81064e-05 y=-0.000186971 z=-1.3631e-05 kx=5.72534e-06 ky=-5.7374e-06 kz=3.42426 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52781e-09 l2=2.47626e-05 x=4.84425e-05 y=6.60409e-05 z=-1.23838e-05 kx=0.000227889 ky=-0.000194416 kz=6.48439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20974e-09 l2=1.79237e-05 x=-4.919e-05 y=0.000484408 z=-8.96475e-06 kx=-1.19622e-05 ky=9.9898e-06 kz=0.257786 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05482e-09 l2=1.91053e-05 x=-4.90794e-05 y=0.000173439 z=-9.55137e-06 kx=0.000151424 ky=0.000280466 kz=4.17641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.62271e-09 l2=5.6467e-06 x=4.99202e-05 y=-0.000227548 z=-2.82762e-06 kx=0.000137818 ky=-0.000164028 kz=3.50339 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05088e-09 l2=7.89313e-06 x=-4.98441e-05 y=-3.03896e-05 z=-3.94692e-06 kx=5.74756e-05 ky=-0.000113085 kz=4.24322 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24714e-09 l2=1.50416e-05 x=-4.94312e-05 y=0.000338965 z=-7.52249e-06 kx=-3.7352e-05 ky=2.4787e-05 kz=3.27687 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17122e-09 l2=2.23144e-05 x=-4.87397e-05 y=8.43381e-05 z=-1.11566e-05 kx=2.90755e-05 ky=-4.05791e-05 kz=1.1825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02674e-09 l2=1.33857e-05 x=-4.95501e-05 y=0.000180988 z=-6.69413e-06 kx=-1.39434e-05 ky=0.000101667 kz=2.38399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.93015e-09 l2=1.6642e-06 x=-4.99931e-05 y=-0.000129037 z=-8.39317e-07 kx=-1.65201e-05 ky=-1.27425e-05 kz=0.36656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06105e-09 l2=3.67101e-05 x=-4.6509e-05 y=-0.000186403 z=-1.83562e-05 kx=-4.45363e-05 ky=-0.000129764 kz=3.30224 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08293e-09 l2=4.03845e-05 x=-4.57409e-05 y=-0.000436253 z=-2.01945e-05 kx=-0.000165767 ky=-0.000144861 kz=4.58347 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61537e-09 l2=1.15503e-05 x=-4.96654e-05 y=-0.000458967 z=-5.77676e-06 kx=-5.4165e-05 ky=-3.4433e-05 kz=3.29086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04255e-09 l2=2.15964e-05 x=4.88199e-05 y=-0.000279831 z=-1.08001e-05 kx=8.42165e-05 ky=-9.15626e-05 kz=2.97592 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.57672e-09 l2=1.11088e-05 x=-4.96908e-05 y=-0.000295278 z=-5.55499e-06 kx=2.49169e-05 ky=2.15444e-05 kz=1.74582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.00107e-09 l2=5.69783e-06 x=4.99189e-05 y=-0.000119849 z=-2.85142e-06 kx=1.90271e-05 ky=2.86594e-05 kz=1.8849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14939e-09 l2=1.38081e-05 x=-4.95215e-05 y=-0.000353565 z=-6.90293e-06 kx=0.000131345 ky=3.88185e-05 kz=2.93952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32414e-09 l2=2.17959e-05 x=4.87983e-05 y=-0.00020876 z=-1.08984e-05 kx=-7.91135e-05 ky=0.000143405 kz=5.69021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55782e-09 l2=2.95358e-05 x=-4.77698e-05 y=0.000274912 z=-1.47681e-05 kx=2.15018e-05 ky=-2.98632e-06 kz=1.74895 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.36271e-09 l2=9.21247e-06 x=4.97877e-05 y=-9.23118e-05 z=-4.60532e-06 kx=-0.000163813 ky=0.000109024 kz=3.89581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76563e-09 l2=1.90671e-05 x=-4.90827e-05 y=0.000128066 z=-9.53537e-06 kx=-0.000100504 ky=0.000107678 kz=5.12424 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71523e-09 l2=2.46717e-05 x=-4.8454e-05 y=0.000393886 z=-1.23389e-05 kx=-0.000161686 ky=0.00015917 kz=3.62937 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30902e-09 l2=1.14639e-05 x=4.96702e-05 y=0.000317034 z=-5.73567e-06 kx=0.000346367 ky=0.000207201 kz=6.77535 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.42682e-09 l2=9.42648e-06 x=-4.97777e-05 y=-0.000156359 z=-4.71423e-06 kx=5.00504e-06 ky=-5.30503e-06 kz=0.204698 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71196e-09 l2=2.83497e-05 x=4.79483e-05 y=0.000310211 z=-1.41777e-05 kx=9.20347e-05 ky=-9.95601e-06 kz=2.2181 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04837e-09 l2=1.58576e-05 x=4.93675e-05 y=4.24006e-05 z=-7.92911e-06 kx=-2.6955e-05 ky=-9.39423e-05 kz=6.87447 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70542e-09 l2=1.58278e-05 x=-4.93697e-05 y=-1.00255e-05 z=-7.91676e-06 kx=-9.88112e-05 ky=-5.68177e-05 kz=3.21778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26864e-09 l2=3.99057e-05 x=4.58457e-05 y=-0.000120151 z=-1.99555e-05 kx=0.000205751 ky=8.86403e-05 kz=4.63696 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25542e-09 l2=2.35817e-05 x=-4.85903e-05 y=0.000199001 z=-1.17905e-05 kx=0.000114616 ky=0.000254388 kz=5.88303 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02599e-09 l2=1.19606e-05 x=-4.96409e-05 y=0.000322581 z=-5.98264e-06 kx=-0.000250443 ky=0.000106753 kz=6.76702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12221e-09 l2=3.44458e-05 x=4.69399e-05 y=0.000147708 z=-1.72244e-05 kx=4.08161e-05 ky=0.000111379 kz=2.01704 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.97833e-09 l2=6.54952e-06 x=-4.98927e-05 y=-0.000174876 z=-3.27768e-06 kx=-3.27644e-05 ky=2.63744e-05 kz=1.75834 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78055e-09 l2=1.54798e-05 x=-4.93971e-05 y=-0.000235759 z=-7.74304e-06 kx=-0.000292961 ky=-4.49966e-05 kz=6.46776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25151e-09 l2=3.05093e-05 x=-4.76157e-05 y=7.42608e-06 z=-1.52574e-05 kx=-0.000190862 ky=2.98151e-05 kz=4.26796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28757e-09 l2=1.78065e-05 x=4.92013e-05 y=-1.17475e-05 z=-8.90256e-06 kx=-0.00010045 ky=-0.000148648 kz=3.64283 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.06e-09 l2=6.13333e-06 x=4.99058e-05 y=7.61229e-05 z=-3.07083e-06 kx=0.000235159 ky=5.44945e-05 kz=4.44492 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17127e-09 l2=2.30414e-05 x=4.86544e-05 y=-0.00015742 z=-1.15229e-05 kx=0.000103489 ky=8.83085e-05 kz=3.16702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71826e-09 l2=1.34919e-05 x=4.95432e-05 y=0.000450984 z=-6.7452e-06 kx=-1.10577e-05 ky=2.42876e-05 kz=0.338719 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7014e-09 l2=1.6045e-05 x=4.93523e-05 y=-0.000155377 z=-8.02336e-06 kx=2.01754e-06 ky=5.08009e-05 kz=2.87859 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58461e-09 l2=1.5097e-05 x=-4.94267e-05 y=0.000449008 z=-7.5516e-06 kx=-0.000130021 ky=3.4659e-05 kz=2.80667 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21049e-09 l2=2.39294e-05 x=-4.85478e-05 y=-0.00042414 z=-1.19641e-05 kx=4.07958e-05 ky=-9.00509e-05 kz=1.61017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19945e-09 l2=3.88275e-05 x=-4.60781e-05 y=-6.89585e-05 z=-1.94128e-05 kx=5.40937e-05 ky=-5.31795e-05 kz=1.59124 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36865e-09 l2=1.34693e-05 x=-4.95442e-05 y=-0.000459151 z=-6.73692e-06 kx=-0.000116345 ky=-8.6089e-05 kz=3.61894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.23103e-09 l2=1.19512e-05 x=4.96421e-05 y=7.46419e-05 z=-5.97515e-06 kx=-0.000157913 ky=8.17819e-05 kz=3.76554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48898e-09 l2=1.49411e-05 x=-4.94388e-05 y=-3.6138e-05 z=-7.47184e-06 kx=-4.31166e-05 ky=-0.000116432 kz=3.89265 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97595e-09 l2=1.74891e-05 x=-4.92295e-05 y=0.000286855 z=-8.74602e-06 kx=-2.37211e-05 ky=0.000188344 kz=2.4012 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03534e-09 l2=2.06218e-05 x=-4.89251e-05 y=-0.000258074 z=-1.03131e-05 kx=-0.000174617 ky=3.70954e-05 kz=4.95434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61738e-09 l2=2.41128e-05 x=4.85245e-05 y=0.000448207 z=-1.20587e-05 kx=0.000194556 ky=0.0004615 kz=6.25382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15588e-09 l2=1.00853e-05 x=-4.97451e-05 y=-0.000436358 z=-5.04347e-06 kx=-2.65971e-05 ky=-0.000510582 kz=5.82843 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05818e-09 l2=1.50375e-05 x=-4.94313e-05 y=-0.000180378 z=-7.52113e-06 kx=-0.000178063 ky=-0.000230553 kz=4.69788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01738e-09 l2=4.74057e-05 x=-4.40244e-05 y=-5.70223e-05 z=-2.37044e-05 kx=-0.000157477 ky=0.000137535 kz=6.55526 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46171e-09 l2=1.40534e-05 x=4.95042e-05 y=-0.000245945 z=-7.02545e-06 kx=-0.000168579 ky=-0.000188681 kz=4.18333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03049e-09 l2=1.17952e-05 x=4.96513e-05 y=-0.000495667 z=-5.89645e-06 kx=-0.000210345 ky=-0.000477614 kz=4.83955 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0181e-09 l2=3.43384e-05 x=-4.69604e-05 y=0.000299865 z=-1.71685e-05 kx=1.75208e-05 ky=4.81046e-05 kz=0.704997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.26926e-09 l2=1.19514e-05 x=-4.96419e-05 y=-6.97572e-05 z=-5.97755e-06 kx=9.34654e-06 ky=4.06244e-05 kz=1.62548 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30747e-09 l2=3.79517e-05 x=4.626e-05 y=0.000346292 z=-1.89753e-05 kx=-0.000188931 ky=0.000282225 kz=6.9743 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21145e-09 l2=8.08832e-06 x=-4.98362e-05 y=-0.000326704 z=-4.04478e-06 kx=-1.35542e-06 ky=-0.000146666 kz=3.71868 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10084e-09 l2=3.75819e-05 x=-4.63355e-05 y=-0.000485397 z=-1.879e-05 kx=0.000227002 ky=-9.19225e-06 kz=6.92105 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41304e-09 l2=1.34692e-05 x=4.95447e-05 y=5.73314e-05 z=-6.73362e-06 kx=-0.000151909 ky=0.000166018 kz=4.5166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08206e-09 l2=2.79928e-05 x=4.80007e-05 y=-0.000274993 z=-1.39986e-05 kx=0.00014554 ky=-0.000101744 kz=4.22584 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15871e-09 l2=2.9576e-05 x=4.77638e-05 y=-4.36766e-05 z=-1.4787e-05 kx=-0.000162032 ky=0.00016062 kz=4.92874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.97908e-09 l2=2.58754e-06 x=4.99834e-05 y=0.000404313 z=-1.29615e-06 kx=-6.08456e-05 ky=7.28205e-05 kz=4.96073 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03066e-09 l2=3.13317e-05 x=-4.74825e-05 y=-0.000460521 z=-1.56666e-05 kx=-2.13513e-05 ky=-0.000116555 kz=3.99282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.345e-09 l2=6.76129e-06 x=4.98856e-05 y=0.000135587 z=-3.385e-06 kx=5.78934e-05 ky=-1.30985e-05 kz=1.32419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11182e-09 l2=4.19644e-05 x=4.53838e-05 y=0.000141229 z=-2.09847e-05 kx=2.58204e-05 ky=3.68678e-05 kz=0.620172 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76329e-09 l2=2.40912e-05 x=4.85271e-05 y=9.39918e-05 z=-1.20482e-05 kx=0.000164353 ky=0.000212807 kz=4.68487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.1602e-09 l2=1.15248e-05 x=-4.96669e-05 y=-0.000229514 z=-5.76506e-06 kx=-4.49338e-05 ky=-0.000120333 kz=2.05739 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38724e-09 l2=2.72681e-05 x=4.81058e-05 y=-0.000313568 z=-1.36333e-05 kx=-5.51819e-05 ky=-1.3868e-05 kz=1.86439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31029e-09 l2=1.9194e-05 x=-4.90699e-05 y=0.000275388 z=-9.60029e-06 kx=-0.000156351 ky=-5.49539e-05 kz=2.91672 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34786e-09 l2=1.16144e-05 x=4.96616e-05 y=0.000374114 z=-5.80929e-06 kx=3.7311e-05 ky=1.03826e-05 kz=2.03008 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26425e-09 l2=1.63356e-05 x=-4.93287e-05 y=0.000260692 z=-8.16701e-06 kx=0.000119917 ky=0.000285291 kz=4.10666 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.1602e-09 l2=5.68658e-06 x=-4.99193e-05 y=0.000445787 z=-2.84359e-06 kx=0.000149627 ky=0.000201482 kz=4.19628 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.23399e-09 l2=5.69357e-06 x=-4.9919e-05 y=-0.000445169 z=-2.85079e-06 kx=-8.74944e-06 ky=-2.31956e-05 kz=0.489152 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66571e-09 l2=1.23868e-05 x=4.96151e-05 y=-0.000384984 z=-6.19414e-06 kx=-3.41989e-06 ky=-3.36306e-05 kz=1.68437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46624e-09 l2=8.55471e-06 x=4.98169e-05 y=0.000442367 z=-4.27688e-06 kx=-1.29762e-05 ky=3.14219e-05 kz=0.534364 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20279e-09 l2=1.6774e-05 x=4.92916e-05 y=-0.000199239 z=-8.38807e-06 kx=2.7765e-05 ky=-6.29309e-05 kz=2.84223 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47755e-09 l2=6.78863e-06 x=4.98847e-05 y=-0.000409827 z=-3.39603e-06 kx=5.79206e-05 ky=-0.000175375 kz=5.99094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7177e-09 l2=1.45595e-05 x=-4.94673e-05 y=0.000412623 z=-7.28097e-06 kx=-9.44978e-06 ky=3.57558e-05 kz=1.2784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00191e-09 l2=3.0979e-05 x=4.75396e-05 y=-2.4573e-05 z=-1.54924e-05 kx=0.000272977 ky=-0.000205718 kz=5.51016 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6933e-09 l2=2.21371e-05 x=-4.87594e-05 y=-0.000329425 z=-1.10707e-05 kx=-0.000175335 ky=-0.000147309 kz=6.52101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54085e-09 l2=3.01555e-05 x=4.76722e-05 y=0.000362091 z=-1.50801e-05 kx=6.78046e-05 ky=8.64891e-05 kz=2.00324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3012e-09 l2=1.43917e-05 x=4.94798e-05 y=0.000496645 z=-7.19524e-06 kx=-6.5609e-05 ky=0.000235514 kz=2.58667 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0071e-09 l2=3.44709e-05 x=4.69352e-05 y=-5.55125e-05 z=-1.72372e-05 kx=0.000130442 ky=0.000106471 kz=5.00932 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08536e-09 l2=1.06176e-05 x=4.97173e-05 y=-1.61067e-05 z=-5.31024e-06 kx=2.81553e-05 ky=-4.35094e-05 kz=1.53207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2343e-09 l2=3.86247e-05 x=-4.61196e-05 y=-2.24496e-06 z=-1.9314e-05 kx=-4.25897e-05 ky=6.12037e-05 kz=1.95695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06515e-09 l2=3.45355e-05 x=4.69233e-05 y=-0.000303186 z=-1.72696e-05 kx=2.75985e-05 ky=-2.98441e-05 kz=0.953866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06624e-09 l2=2.08708e-05 x=4.88991e-05 y=0.000310265 z=-1.04357e-05 kx=-2.00581e-05 ky=9.86628e-05 kz=3.62496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.35761e-09 l2=1.06615e-05 x=-4.97149e-05 y=-0.000225145 z=-5.33517e-06 kx=-0.000125212 ky=-0.000119437 kz=2.28682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59255e-09 l2=1.1031e-05 x=-4.96947e-05 y=0.000171063 z=-5.51862e-06 kx=-0.000157923 ky=-9.66928e-05 kz=3.4021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2349e-09 l2=3.001e-05 x=-4.76959e-05 y=-0.000400569 z=-1.50045e-05 kx=1.09631e-05 ky=-2.28943e-05 kz=0.469605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85458e-09 l2=1.38339e-05 x=4.95196e-05 y=0.000265543 z=-6.91697e-06 kx=-0.000148381 ky=5.96637e-05 kz=5.22 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05943e-09 l2=1.89349e-05 x=-4.90957e-05 y=0.000270352 z=-9.46868e-06 kx=-2.51475e-05 ky=0.000403892 kz=5.64802 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34994e-09 l2=1.45888e-05 x=-4.94652e-05 y=0.000128529 z=-7.29548e-06 kx=9.50435e-06 ky=0.000122574 kz=4.78244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.38288e-09 l2=7.09543e-06 x=4.9874e-05 y=0.000435091 z=-3.5508e-06 kx=0.000109478 ky=0.00035377 kz=3.91212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38774e-09 l2=2.95248e-05 x=4.77718e-05 y=4.04364e-05 z=-1.47613e-05 kx=-4.65608e-05 ky=4.70143e-05 kz=1.23363 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23164e-09 l2=3.14351e-05 x=-4.74657e-05 y=0.000246937 z=-1.57178e-05 kx=1.99748e-05 ky=3.38062e-05 kz=2.79608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58974e-09 l2=8.90757e-06 x=4.98015e-05 y=-4.87229e-05 z=-4.45237e-06 kx=-0.000291792 ky=-0.000256768 kz=6.57778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87426e-09 l2=2.64204e-05 x=4.8224e-05 y=0.000408963 z=-1.32097e-05 kx=-0.000106678 ky=0.000191316 kz=3.52666 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09584e-09 l2=1.35443e-05 x=4.95396e-05 y=-0.000187772 z=-6.77093e-06 kx=-0.000215919 ky=-0.000334868 kz=6.01546 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27684e-09 l2=2.47868e-05 x=-4.84402e-05 y=-0.000134844 z=-1.23926e-05 kx=7.89972e-05 ky=-8.52238e-05 kz=2.61872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9388e-09 l2=1.80714e-05 x=4.91773e-05 y=-0.000495926 z=-9.03497e-06 kx=-0.000121143 ky=-0.000298257 kz=3.53696 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4425e-09 l2=9.77006e-06 x=4.97611e-05 y=0.000476116 z=-4.8837e-06 kx=-4.2809e-05 ky=6.53526e-05 kz=1.03719 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.13853e-09 l2=2.68529e-06 x=4.99821e-05 y=-0.000221907 z=-1.34568e-06 kx=-0.000153612 ky=-0.000116028 kz=5.00551 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13578e-09 l2=2.84331e-05 x=4.79368e-05 y=-0.000493866 z=-1.42161e-05 kx=-7.03933e-05 ky=-2.71992e-05 kz=3.23758 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3006e-09 l2=1.23773e-05 x=4.96159e-05 y=-0.000403129 z=-6.1878e-06 kx=-0.000177887 ky=-5.41533e-05 kz=4.38631 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01088e-09 l2=1.91371e-05 x=-4.9076e-05 y=0.000260834 z=-9.57023e-06 kx=-5.62834e-06 ky=3.80527e-06 kz=0.405049 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.45081e-09 l2=8.29779e-06 x=-4.98276e-05 y=1.85002e-05 z=-4.15169e-06 kx=-5.99306e-05 ky=2.37719e-05 kz=2.79641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19743e-09 l2=3.1546e-05 x=4.74477e-05 y=-0.000118416 z=-1.57718e-05 kx=-5.94871e-05 ky=-2.13931e-06 kz=1.57215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13713e-09 l2=1.88655e-05 x=4.91025e-05 y=0.000467581 z=-9.43205e-06 kx=-2.33022e-05 ky=3.42595e-05 kz=0.885674 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11822e-09 l2=1.92342e-05 x=4.90667e-05 y=0.000470905 z=-9.61656e-06 kx=-1.43221e-05 ky=1.58998e-05 kz=0.656635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36676e-09 l2=1.75133e-05 x=4.92271e-05 y=-0.000174622 z=-8.75866e-06 kx=1.3753e-05 ky=-2.2427e-05 kz=0.514716 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12526e-09 l2=3.33403e-05 x=4.71389e-05 y=-0.000444788 z=-1.66721e-05 kx=0.000132729 ky=-0.000123667 kz=4.52836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4002e-09 l2=3.34987e-05 x=-4.71114e-05 y=-0.000473628 z=-1.67501e-05 kx=-7.51995e-06 ky=-0.000281 kz=5.02842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.03091e-09 l2=6.24232e-06 x=-4.99026e-05 y=2.47739e-05 z=-3.12259e-06 kx=1.04855e-05 ky=0.00028993 kz=6.07744 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05897e-09 l2=4.88247e-05 x=-4.36344e-05 y=-0.000458242 z=-2.4415e-05 kx=-0.000327615 ky=-0.000607736 kz=6.55841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15633e-09 l2=2.24115e-05 x=-4.87288e-05 y=-0.000331254 z=-1.12042e-05 kx=0.000304072 ky=1.60854e-05 kz=6.94554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79799e-09 l2=1.1816e-05 x=-4.96495e-05 y=0.000226272 z=-5.9115e-06 kx=-0.000318353 ky=0.000243589 kz=6.09044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23062e-09 l2=1.20546e-05 x=4.96355e-05 y=1.13768e-05 z=-6.02725e-06 kx=-4.58425e-05 ky=-3.21486e-05 kz=3.30634 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26502e-09 l2=2.88233e-05 x=-4.78775e-05 y=-0.000412428 z=-1.44148e-05 kx=-9.68994e-05 ky=-0.000142094 kz=1.8892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87493e-09 l2=5.10226e-06 x=4.9935e-05 y=0.000333101 z=-2.55108e-06 kx=-8.00768e-05 ky=1.37624e-05 kz=4.04636 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0277e-09 l2=4.6865e-05 x=-4.41696e-05 y=-0.000478798 z=-2.34327e-05 kx=2.85234e-05 ky=-0.000227724 kz=4.12301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01088e-09 l2=1.91371e-05 x=-4.9076e-05 y=0.000260834 z=-9.57023e-06 kx=-5.62834e-06 ky=3.80527e-06 kz=0.405049 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15846e-09 l2=2.0918e-05 x=-4.88935e-05 y=9.40315e-05 z=-1.04618e-05 kx=-0.000218047 ky=0.000196025 kz=4.797 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.27106e-09 l2=8.60902e-06 x=4.98143e-05 y=8.8007e-05 z=-4.30782e-06 kx=5.16235e-05 ky=-4.01837e-05 kz=1.18181 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31847e-09 l2=3.72533e-05 x=4.64002e-05 y=0.000450789 z=-1.86298e-05 kx=0.000230642 ky=4.65134e-05 kz=4.37747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33078e-09 l2=2.74437e-05 x=-4.808e-05 y=-0.000370727 z=-1.37241e-05 kx=-4.59762e-05 ky=6.25744e-06 kz=1.35836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20121e-09 l2=1.88765e-05 x=-4.91009e-05 y=3.88689e-05 z=-9.44072e-06 kx=-6.40863e-05 ky=-6.02229e-05 kz=1.68387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.79304e-09 l2=9.16619e-06 x=4.97896e-05 y=-0.000297466 z=-4.58712e-06 kx=3.39007e-05 ky=9.57167e-06 kz=1.04086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31116e-09 l2=2.88074e-05 x=4.7881e-05 y=-0.000378875 z=-1.44032e-05 kx=-6.36231e-05 ky=-0.000207888 kz=2.52088 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27347e-09 l2=1.62127e-05 x=-4.93383e-05 y=1.51096e-05 z=-8.10876e-06 kx=-0.000220758 ky=-0.000103202 kz=6.08591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46459e-09 l2=1.80442e-05 x=-4.91795e-05 y=0.000234395 z=-9.02331e-06 kx=6.24152e-07 ky=0.000285261 kz=4.29965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6527e-09 l2=1.32668e-05 x=4.95584e-05 y=-0.000115091 z=-6.6326e-06 kx=-0.000176436 ky=-0.000183182 kz=5.44169 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73848e-09 l2=1.87256e-05 x=4.91158e-05 y=0.000415893 z=-9.36341e-06 kx=-2.33541e-05 ky=0.000146401 kz=4.32496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14392e-09 l2=2.69482e-05 x=4.81501e-05 y=-0.000451805 z=-1.34758e-05 kx=8.94289e-05 ky=-0.000128441 kz=4.02424 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05897e-09 l2=4.88247e-05 x=-4.36344e-05 y=-0.000458242 z=-2.4415e-05 kx=-0.000327615 ky=-0.000607736 kz=6.55841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72013e-09 l2=1.56594e-05 x=-4.93836e-05 y=-0.000285473 z=-7.8288e-06 kx=0.000128675 ky=4.53225e-05 kz=3.58605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21432e-09 l2=2.17085e-05 x=-4.88081e-05 y=0.000421899 z=-1.08536e-05 kx=9.20435e-05 ky=3.2467e-05 kz=3.48283 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55196e-09 l2=1.13095e-05 x=4.96794e-05 y=-4.29192e-06 z=-5.6542e-06 kx=-0.000149333 ky=-0.000154498 kz=5.49784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22367e-09 l2=3.21695e-05 x=-4.7342e-05 y=-7.79487e-05 z=-1.60866e-05 kx=-4.10992e-05 ky=-4.30545e-05 kz=1.61493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09485e-09 l2=2.30927e-05 x=-4.86481e-05 y=-0.000134876 z=-1.15492e-05 kx=-0.000255709 ky=-0.000155062 kz=5.2684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.71371e-09 l2=1.94938e-06 x=4.99906e-05 y=-0.00028368 z=-9.74823e-07 kx=-0.000269685 ky=-0.000290324 kz=6.05639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62939e-09 l2=9.11952e-06 x=4.97919e-05 y=-0.000190909 z=-4.55879e-06 kx=-2.28033e-05 ky=-1.13482e-05 kz=0.634917 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08961e-09 l2=5.00652e-05 x=4.32835e-05 y=0.000292902 z=-2.50319e-05 kx=-9.39508e-05 ky=-9.7723e-06 kz=3.27873 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22253e-09 l2=7.29026e-06 x=-4.98669e-05 y=-0.000220718 z=-3.64763e-06 kx=-5.95603e-05 ky=-0.000113389 kz=2.13087 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20989e-09 l2=2.02332e-05 x=-4.8966e-05 y=0.000254169 z=-1.0117e-05 kx=1.25192e-05 ky=0.000126526 kz=2.99831 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11487e-09 l2=3.55332e-05 x=4.67377e-05 y=-0.000302203 z=-1.77659e-05 kx=-0.000171036 ky=-0.000148612 kz=6.53793 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.07852e-09 l2=2.12053e-05 x=4.88633e-05 y=-0.000103973 z=-1.0603e-05 kx=-4.79635e-05 ky=-0.000159966 kz=3.24961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08239e-09 l2=3.07112e-05 x=-4.75831e-05 y=1.02407e-05 z=-1.53585e-05 kx=-0.000177348 ky=4.34813e-05 kz=3.56718 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13294e-09 l2=1.50281e-05 x=4.94322e-05 y=-0.000112742 z=-7.51499e-06 kx=4.46781e-05 ky=0.000173265 kz=5.74887 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93496e-09 l2=7.7384e-06 x=-4.98501e-05 y=-0.000417614 z=-3.87061e-06 kx=-3.5283e-05 ky=-0.000153955 kz=3.97526 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16057e-09 l2=1.51792e-05 x=-4.9421e-05 y=5.02188e-05 z=-7.58833e-06 kx=0.000175143 ky=2.8266e-05 kz=4.68695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.71371e-09 l2=1.94938e-06 x=4.99906e-05 y=-0.00028368 z=-9.74823e-07 kx=-0.000269685 ky=-0.000290324 kz=6.05639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47995e-09 l2=1.35828e-05 x=4.95365e-05 y=0.000372537 z=-6.795e-06 kx=7.09674e-05 ky=8.62437e-05 kz=1.49101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39855e-09 l2=1.07185e-05 x=4.97122e-05 y=-0.000300313 z=-5.35918e-06 kx=-0.000134234 ky=-0.000340569 kz=5.17467 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.21857e-09 l2=4.61368e-06 x=-4.99468e-05 y=0.000291574 z=-2.31183e-06 kx=-0.000233587 ky=0.000277302 kz=4.91213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98716e-09 l2=1.42957e-05 x=-4.94866e-05 y=-0.000176331 z=-7.14878e-06 kx=4.91542e-06 ky=-0.000131965 kz=2.89939 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3205e-09 l2=3.74982e-05 x=4.63511e-05 y=0.000278913 z=-1.87517e-05 kx=0.000211028 ky=0.000226491 kz=4.96862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03235e-09 l2=2.51546e-05 x=-4.8393e-05 y=-0.000469049 z=-1.25757e-05 kx=0.000226196 ky=-0.000441828 kz=5.1383 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05975e-09 l2=3.49101e-05 x=-4.68544e-05 y=-2.27744e-05 z=-1.74556e-05 kx=-2.20959e-06 ky=-6.45664e-05 kz=2.3696 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52674e-09 l2=1.75218e-05 x=-4.92265e-05 y=0.000200965 z=-8.76239e-06 kx=-1.41241e-05 ky=2.25982e-05 kz=0.972978 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51456e-09 l2=2.15086e-05 x=-4.883e-05 y=5.90892e-05 z=-1.07548e-05 kx=3.54719e-05 ky=0.000323818 kz=7.01856 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33588e-09 l2=8.05891e-06 x=-4.98375e-05 y=-0.000104929 z=-4.02905e-06 kx=1.66391e-05 ky=2.63934e-05 kz=0.773323 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69512e-09 l2=1.2889e-05 x=-4.95831e-05 y=-5.33872e-05 z=-6.44505e-06 kx=2.07827e-06 ky=-1.34399e-05 kz=0.375018 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82357e-09 l2=2.74435e-05 x=4.80812e-05 y=-0.000324024 z=-1.37205e-05 kx=-9.70057e-05 ky=1.69186e-05 kz=2.15628 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10329e-09 l2=1.7511e-05 x=-4.92273e-05 y=-0.000451872 z=-8.7575e-06 kx=-0.000181245 ky=-0.000115302 kz=6.17084 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49148e-09 l2=2.50062e-05 x=4.8411e-05 y=0.000425017 z=-1.25064e-05 kx=5.50253e-05 ky=5.3291e-05 kz=1.01633 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.41349e-09 l2=6.39297e-06 x=-4.98978e-05 y=-0.000437513 z=-3.19986e-06 kx=-0.000163665 ky=-0.000586022 kz=7.02383 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00366e-09 l2=2.56926e-05 x=4.83212e-05 y=-0.000395353 z=-1.28486e-05 kx=7.14837e-05 ky=-4.54124e-05 kz=1.92348 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09022e-09 l2=4.16055e-05 x=-4.54671e-05 y=0.00020502 z=-2.08036e-05 kx=-5.31553e-05 ky=0.000195023 kz=6.65932 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58377e-09 l2=9.60439e-06 x=4.97688e-05 y=-0.000130726 z=-4.80514e-06 kx=0.000119336 ky=-0.000145287 kz=3.59293 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0081e-09 l2=1.18856e-05 x=4.96459e-05 y=-0.000413082 z=-5.94248e-06 kx=-9.95581e-05 ky=-0.0003118 kz=3.68157 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04286e-09 l2=3.38453e-05 x=4.70499e-05 y=-6.94791e-05 z=-1.69216e-05 kx=-0.00021143 ky=-6.72946e-05 kz=6.43709 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.88557e-09 l2=9.93234e-06 x=4.97529e-05 y=-0.000194996 z=-4.96824e-06 kx=1.83535e-05 ky=-0.000185668 kz=7.00585 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82085e-09 l2=1.68369e-05 x=-4.92862e-05 y=-6.56927e-05 z=-8.42139e-06 kx=-0.000202503 ky=-0.000122213 kz=6.44816 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23525e-09 l2=8.17507e-06 x=-4.98327e-05 y=0.000459814 z=-4.08772e-06 kx=3.18371e-05 ky=0.000210092 kz=3.66253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09852e-09 l2=2.73732e-05 x=4.80907e-05 y=-0.000148131 z=-1.36863e-05 kx=-5.98124e-05 ky=-3.10634e-05 kz=3.33794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01931e-09 l2=3.40497e-05 x=4.7012e-05 y=-0.000127872 z=-1.70268e-05 kx=0.000115203 ky=-0.000138935 kz=3.8458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0418e-09 l2=2.77321e-05 x=4.80384e-05 y=-0.000476784 z=-1.38687e-05 kx=0.000157598 ky=-0.000245538 kz=3.63012 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35218e-09 l2=8.12681e-06 x=4.98345e-05 y=3.46374e-05 z=-4.06696e-06 kx=2.58183e-05 ky=-1.48038e-06 kz=0.540995 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60553e-09 l2=1.44056e-05 x=-4.94783e-05 y=0.000190664 z=-7.20561e-06 kx=-2.62832e-05 ky=4.36514e-05 kz=0.648674 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48893e-09 l2=3.89437e-05 x=4.60531e-05 y=0.000245163 z=-1.94723e-05 kx=-2.1484e-05 ky=4.24123e-05 kz=3.55711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.82148e-09 l2=6.5836e-06 x=-4.98915e-05 y=-2.8318e-05 z=-3.29639e-06 kx=-0.000320141 ky=-9.2324e-05 kz=5.95152 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31215e-09 l2=2.55153e-05 x=4.83451e-05 y=0.000409999 z=-1.27587e-05 kx=1.50877e-05 ky=7.69657e-05 kz=2.03245 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85172e-09 l2=7.15899e-06 x=-4.98717e-05 y=0.000115279 z=-3.58233e-06 kx=-7.30865e-05 ky=1.63458e-05 kz=2.58551 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05037e-09 l2=4.49077e-05 x=4.46753e-05 y=0.000355536 z=-2.24537e-05 kx=-1.23017e-05 ky=3.17125e-05 kz=0.811004 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.85378e-09 l2=1.56834e-05 x=4.93815e-05 y=-7.12415e-05 z=-7.84173e-06 kx=-8.32343e-05 ky=-9.48747e-05 kz=4.47824 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01477e-09 l2=5.5725e-05 x=4.1518e-05 y=-0.000286812 z=-2.78624e-05 kx=-6.29917e-05 ky=-0.000175295 kz=4.57405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07078e-09 l2=4.70083e-05 x=4.41316e-05 y=-0.00044242 z=-2.35043e-05 kx=-5.54052e-05 ky=-0.000412582 kz=6.92126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63613e-09 l2=3.06826e-05 x=4.75886e-05 y=-0.000166742 z=-1.53419e-05 kx=-3.23232e-05 ky=-0.000241822 kz=6.71881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89497e-09 l2=1.79131e-05 x=4.91917e-05 y=0.000493711 z=-8.9562e-06 kx=-0.000162584 ky=0.000567844 kz=6.18378 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17567e-09 l2=6.81191e-06 x=-4.98839e-05 y=-0.000136664 z=-3.4061e-06 kx=2.59987e-05 ky=-0.000139801 kz=2.96606 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02541e-09 l2=5.04352e-05 x=4.3176e-05 y=0.000411041 z=-2.52168e-05 kx=-7.16443e-05 ky=0.000174657 kz=2.37646 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29307e-09 l2=2.29323e-05 x=4.86679e-05 y=0.000363304 z=-1.14657e-05 kx=-5.93492e-05 ky=7.53381e-06 kz=2.59993 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.10465e-09 l2=1.10387e-05 x=4.96945e-05 y=0.00027643 z=-5.52228e-06 kx=8.94024e-05 ky=3.40513e-05 kz=3.24661 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89973e-09 l2=1.14563e-05 x=4.96707e-05 y=-8.19702e-05 z=-5.73086e-06 kx=4.76208e-05 ky=-5.52149e-05 kz=1.34785 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00073e-09 l2=3.9789e-05 x=4.58709e-05 y=-9.87511e-05 z=-1.98973e-05 kx=0.000182407 ky=3.6631e-05 kz=3.70314 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33634e-09 l2=1.51348e-05 x=4.94238e-05 y=-0.00014668 z=-7.57046e-06 kx=0.000135011 ky=2.98666e-05 kz=2.80856 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4502e-09 l2=1.21237e-05 x=4.9631e-05 y=-0.00037236 z=-6.0656e-06 kx=9.07946e-05 ky=-5.05829e-05 kz=1.79599 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20464e-09 l2=2.62099e-05 x=-4.82521e-05 y=0.000194751 z=-1.31059e-05 kx=-4.24409e-05 ky=0.00036744 kz=6.94664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05849e-09 l2=1.18285e-05 x=-4.96492e-05 y=-0.000290097 z=-5.9146e-06 kx=2.30627e-05 ky=-7.81395e-05 kz=1.66428 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30529e-09 l2=3.17715e-05 x=4.74094e-05 y=0.000308496 z=-1.58869e-05 kx=7.13809e-05 ky=0.000271069 kz=7.02438 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42787e-09 l2=2.49692e-05 x=4.84164e-05 y=0.000386913 z=-1.24856e-05 kx=5.78228e-06 ky=3.24422e-05 kz=0.936137 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20346e-09 l2=1.95437e-05 x=-4.90364e-05 y=-0.000491732 z=-9.77026e-06 kx=3.95184e-05 ky=-5.1728e-07 kz=0.887982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22633e-09 l2=2.36219e-05 x=4.85852e-05 y=-7.94866e-05 z=-1.18114e-05 kx=-2.3094e-05 ky=-5.85888e-05 kz=6.88715 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63013e-09 l2=1.24276e-05 x=-4.96127e-05 y=0.000387688 z=-6.21308e-06 kx=0.000183618 ky=0.000301216 kz=5.93145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0205e-09 l2=1.8411e-05 x=-4.91453e-05 y=-9.06208e-05 z=-9.20651e-06 kx=-7.3305e-05 ky=2.81728e-05 kz=6.99998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1803e-09 l2=2.13723e-05 x=4.88449e-05 y=-0.000467917 z=-1.06864e-05 kx=-4.02994e-05 ky=-0.000651454 kz=6.74213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.15657e-09 l2=1.37494e-05 x=4.95254e-05 y=-0.000268306 z=-6.87594e-06 kx=-4.58677e-05 ky=-0.000414597 kz=6.41433 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.88123e-09 l2=1.21086e-05 x=4.96323e-05 y=-0.000423136 z=-6.05567e-06 kx=-3.73676e-06 ky=-3.76413e-05 kz=2.09886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.9363e-09 l2=2.32271e-06 x=-4.99866e-05 y=0.000311163 z=-1.16389e-06 kx=7.18323e-05 ky=8.26929e-05 kz=3.84017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12013e-09 l2=3.1718e-05 x=-4.74191e-05 y=-0.000275818 z=-1.58575e-05 kx=0.000166051 ky=2.87701e-05 kz=3.8568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40981e-09 l2=1.1646e-05 x=-4.96596e-05 y=0.00023286 z=-5.826e-06 kx=-0.000203144 ky=-1.47565e-05 kz=4.38185 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79216e-09 l2=1.21768e-05 x=4.9628e-05 y=0.000271712 z=-6.08965e-06 kx=4.73355e-05 ky=-5.55461e-05 kz=6.8946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0541e-09 l2=3.07291e-05 x=4.75814e-05 y=-0.000392613 z=-1.53635e-05 kx=-4.00449e-05 ky=-7.59892e-05 kz=1.23893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20552e-09 l2=2.2971e-05 x=4.86635e-05 y=-0.000327454 z=-1.14846e-05 kx=-0.000112981 ky=-0.000247623 kz=3.7099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22854e-09 l2=2.27382e-05 x=4.86899e-05 y=0.000164433 z=-1.13719e-05 kx=8.29183e-05 ky=1.70518e-05 kz=1.79973 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34972e-09 l2=1.89516e-05 x=4.90938e-05 y=-0.000133748 z=-9.47753e-06 kx=8.33057e-05 ky=-4.50603e-06 kz=3.81523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95343e-09 l2=2.44585e-05 x=-4.84813e-05 y=-6.13693e-06 z=-1.22317e-05 kx=-0.000193004 ky=-0.000307673 kz=6.62711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.21741e-09 l2=4.33861e-06 x=4.99531e-05 y=-8.56823e-05 z=-2.17021e-06 kx=-5.94085e-05 ky=2.34491e-05 kz=1.73914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2024e-08 l2=1.81503e-06 x=-4.99919e-05 y=-0.000143057 z=-9.11488e-07 kx=5.5876e-05 ky=4.47122e-05 kz=1.36862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.85038e-09 l2=9.83547e-06 x=-4.97578e-05 y=-0.000317165 z=-4.91721e-06 kx=0.000173586 ky=8.0515e-05 kz=5.96977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88429e-09 l2=2.21598e-05 x=-4.87573e-05 y=0.000418859 z=-1.10799e-05 kx=0.000122891 ky=3.63029e-05 kz=6.81602 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.458e-09 l2=2.65715e-05 x=4.82021e-05 y=-0.000378645 z=-1.32888e-05 kx=0.000253676 ky=-3.5384e-05 kz=5.26161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24651e-09 l2=8.35015e-06 x=-4.98256e-05 y=0.000376277 z=-4.17452e-06 kx=3.10966e-05 ky=1.41892e-05 kz=0.922757 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23182e-09 l2=1.60094e-05 x=-4.9355e-05 y=0.00038789 z=-8.00731e-06 kx=-0.000191833 ky=0.000110276 kz=6.32305 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35535e-09 l2=1.11121e-05 x=-4.96906e-05 y=0.000297141 z=-5.55652e-06 kx=3.42513e-05 ky=0.000168782 kz=2.34985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55411e-09 l2=1.86835e-05 x=-4.91193e-05 y=-0.000131611 z=-9.34469e-06 kx=-4.93982e-05 ky=-3.84433e-05 kz=1.11713 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03447e-09 l2=5.62023e-05 x=-4.13571e-05 y=0.00035577 z=-2.81007e-05 kx=3.70856e-05 ky=0.000108191 kz=1.6589 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13228e-09 l2=2.22331e-05 x=-4.87488e-05 y=-8.67942e-05 z=-1.11166e-05 kx=4.47566e-05 ky=9.40411e-05 kz=3.79177 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48549e-09 l2=1.71147e-05 x=4.92621e-05 y=-0.000452228 z=-8.56007e-06 kx=8.88248e-06 ky=-1.74228e-05 kz=0.219693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33003e-09 l2=2.78593e-05 x=-4.80208e-05 y=0.000465193 z=-1.39298e-05 kx=1.75759e-05 ky=-3.50039e-06 kz=1.6722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32198e-09 l2=4.18003e-05 x=-4.5422e-05 y=2.67697e-05 z=-2.0902e-05 kx=-0.000184262 ky=-0.000306402 kz=6.86298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68181e-09 l2=2.08622e-05 x=4.89e-05 y=-0.000461233 z=-1.0432e-05 kx=1.51441e-06 ky=-4.22575e-06 kz=1.3916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84373e-09 l2=1.29047e-05 x=-4.95822e-05 y=-0.000224323 z=-6.45198e-06 kx=0.000159783 ky=-9.2071e-05 kz=6.20684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22975e-09 l2=2.02151e-05 x=-4.89677e-05 y=-3.67081e-05 z=-1.01089e-05 kx=-2.86903e-05 ky=-7.1743e-05 kz=1.90775 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32206e-09 l2=2.85709e-05 x=-4.79158e-05 y=0.000226672 z=-1.42868e-05 kx=-7.03985e-06 ky=2.00256e-05 kz=0.465534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.53807e-09 l2=1.83208e-05 x=4.9154e-05 y=0.000232171 z=-9.16139e-06 kx=-3.98674e-05 ky=0.000276873 kz=6.43447 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.7415e-09 l2=6.05706e-06 x=4.99082e-05 y=0.000369722 z=-3.03192e-06 kx=0.000168052 ky=0.000286015 kz=5.51852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08486e-09 l2=2.93469e-05 x=4.77982e-05 y=0.000271131 z=-1.46753e-05 kx=2.16184e-05 ky=3.71473e-05 kz=0.806719 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61221e-09 l2=1.81451e-05 x=4.91701e-05 y=0.000347405 z=-9.07344e-06 kx=4.98575e-06 ky=2.68823e-05 kz=2.23832 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5584e-09 l2=1.04085e-05 x=-4.97284e-05 y=-0.000432372 z=-5.20589e-06 kx=-4.2571e-05 ky=-6.1612e-05 kz=2.54126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08327e-09 l2=1.19373e-05 x=-4.96424e-05 y=0.000478684 z=-5.97011e-06 kx=-9.84704e-05 ky=0.000487386 kz=5.31567 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72558e-09 l2=2.50604e-05 x=4.8405e-05 y=0.000116904 z=-1.25301e-05 kx=-6.63686e-05 ky=5.42651e-05 kz=3.40755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07443e-09 l2=1.13002e-05 x=-4.96799e-05 y=0.000380809 z=-5.64934e-06 kx=3.33442e-06 ky=2.50951e-06 kz=0.130503 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40885e-09 l2=3.43076e-05 x=4.69652e-05 y=0.000292574 z=-1.71556e-05 kx=0.000138566 ky=7.49713e-05 kz=5.78971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.28996e-09 l2=3.3697e-06 x=4.99717e-05 y=0.000465428 z=-1.6874e-06 kx=-2.16231e-06 ky=7.13103e-05 kz=1.13908 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05025e-09 l2=3.14739e-05 x=-4.74598e-05 y=0.000125335 z=-1.57354e-05 kx=2.94834e-05 ky=3.11298e-05 kz=0.67999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.94772e-09 l2=1.64296e-05 x=-4.93204e-05 y=0.000231088 z=-8.21794e-06 kx=-0.000213109 ky=0.000194243 kz=4.88977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03511e-09 l2=7.21063e-06 x=4.987e-05 y=-0.000447492 z=-3.60373e-06 kx=-2.93984e-05 ky=-6.59563e-05 kz=0.698187 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.90868e-09 l2=4.00884e-06 x=4.996e-05 y=-0.000219307 z=-2.00416e-06 kx=-0.00025286 ky=-0.000188354 kz=5.70387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11978e-09 l2=3.41227e-05 x=4.69996e-05 y=0.000350105 z=-1.70608e-05 kx=-7.71535e-05 ky=0.000269743 kz=3.31481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.34972e-09 l2=6.72872e-06 x=-4.98868e-05 y=-5.07552e-05 z=-3.36768e-06 kx=-8.77522e-05 ky=-0.000218254 kz=6.72655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07324e-09 l2=2.46331e-05 x=4.84596e-05 y=-5.65732e-05 z=-1.23165e-05 kx=-4.77173e-05 ky=-0.000230096 kz=4.32709 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.80654e-09 l2=1.55803e-05 x=-4.93894e-05 y=-0.000329444 z=-7.79284e-06 kx=-0.00015736 ky=-0.000460747 kz=6.04789 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03487e-09 l2=1.70346e-05 x=-4.9269e-05 y=-5.80012e-05 z=-8.52081e-06 kx=-0.000334512 ky=-0.000177891 kz=6.60728 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28763e-09 l2=3.07997e-05 x=4.75703e-05 y=1.85273e-05 z=-1.53984e-05 kx=-8.81419e-05 ky=5.5467e-05 kz=2.00385 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35376e-09 l2=3.44277e-05 x=4.69434e-05 y=0.000199097 z=-1.72153e-05 kx=0.000104662 ky=-4.98803e-06 kz=6.60392 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73656e-09 l2=1.27662e-05 x=-4.95909e-05 y=-0.000284342 z=-6.38453e-06 kx=-2.92163e-06 ky=-1.63053e-06 kz=0.248169 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0569e-09 l2=2.2052e-05 x=-4.87694e-05 y=0.000399727 z=-1.10257e-05 kx=6.63756e-05 ky=0.000139612 kz=3.73809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.19848e-09 l2=8.60492e-06 x=-4.98145e-05 y=0.000398423 z=-4.30617e-06 kx=-0.000122544 ky=9.98601e-05 kz=2.8943 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95246e-09 l2=1.00215e-05 x=-4.97486e-05 y=-0.000214123 z=-5.01072e-06 kx=3.90508e-06 ky=-7.32356e-07 kz=0.127109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48635e-09 l2=2.77179e-05 x=-4.80416e-05 y=-9.85401e-05 z=-1.38581e-05 kx=0.000104979 ky=5.52296e-05 kz=3.25756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.94885e-09 l2=2.13397e-05 x=4.8849e-05 y=-0.000482026 z=-1.06687e-05 kx=-0.000154627 ky=-0.000193865 kz=3.555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37278e-09 l2=2.55584e-05 x=4.83395e-05 y=-0.00016582 z=-1.27799e-05 kx=-7.78689e-08 ky=-5.75689e-05 kz=1.14737 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08579e-09 l2=2.20341e-05 x=-4.87713e-05 y=-0.000460915 z=-1.10174e-05 kx=1.6872e-05 ky=-6.93077e-05 kz=4.44518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68887e-09 l2=2.93772e-05 x=4.7794e-05 y=0.000228083 z=-1.46895e-05 kx=7.72792e-06 ky=6.28996e-05 kz=4.4072 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32293e-09 l2=3.73329e-05 x=4.63855e-05 y=7.50906e-06 z=-1.86664e-05 kx=-1.34859e-05 ky=-9.5477e-06 kz=0.842233 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95754e-09 l2=2.19674e-05 x=-4.87788e-05 y=0.000388528 z=-1.09852e-05 kx=-7.15812e-05 ky=0.000566736 kz=6.79517 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06668e-09 l2=1.90961e-05 x=-4.90795e-05 y=0.000199085 z=-9.55117e-06 kx=-5.9824e-05 ky=3.90765e-05 kz=1.13862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36249e-09 l2=8.62507e-06 x=4.98135e-05 y=5.63797e-06 z=-4.31579e-06 kx=1.03469e-05 ky=2.45966e-07 kz=0.200019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20453e-09 l2=2.41756e-05 x=4.85172e-05 y=0.00030973 z=-1.20877e-05 kx=-6.43212e-05 ky=5.39554e-05 kz=4.59845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01183e-09 l2=1.11645e-05 x=4.96877e-05 y=-0.000325476 z=-5.58142e-06 kx=-0.000150866 ky=-0.00019722 kz=4.02852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04383e-09 l2=3.26245e-05 x=4.72648e-05 y=-6.13485e-05 z=-1.63117e-05 kx=-9.29024e-05 ky=0.00010285 kz=4.25779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01183e-09 l2=1.11645e-05 x=4.96877e-05 y=-0.000325476 z=-5.58142e-06 kx=-0.000150866 ky=-0.00019722 kz=4.02852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.7383e-09 l2=3.48113e-06 x=4.99699e-05 y=-0.000285364 z=-1.74381e-06 kx=-4.29004e-05 ky=-0.000108046 kz=3.42504 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02299e-09 l2=1.85917e-05 x=4.91284e-05 y=-0.000100072 z=-9.29637e-06 kx=4.17829e-06 ky=-6.30539e-06 kz=6.66809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2993e-09 l2=1.89868e-05 x=-4.90906e-05 y=-0.00045464 z=-9.49387e-06 kx=2.25474e-05 ky=-0.000355688 kz=6.30677 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69576e-09 l2=3.76264e-05 x=4.63259e-05 y=-0.000223195 z=-1.88142e-05 kx=2.55712e-06 ky=1.31867e-05 kz=0.815722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13086e-09 l2=1.34614e-05 x=4.95448e-05 y=-0.000300419 z=-6.73254e-06 kx=6.82764e-06 ky=-1.20953e-05 kz=0.270979 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38738e-09 l2=4.20559e-06 x=4.99558e-05 y=0.000334127 z=-2.10351e-06 kx=3.04583e-07 ky=1.41506e-05 kz=0.755038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.59073e-09 l2=1.69007e-06 x=4.99929e-05 y=0.000352454 z=-8.50617e-07 kx=2.12764e-05 ky=2.57299e-05 kz=0.595833 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61149e-09 l2=2.58008e-05 x=-4.83079e-05 y=-1.45707e-05 z=-1.28992e-05 kx=5.73394e-05 ky=-2.9672e-05 kz=1.35109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43191e-09 l2=1.9896e-05 x=-4.90003e-05 y=-0.000465192 z=-9.94998e-06 kx=-4.80342e-05 ky=-1.8051e-05 kz=1.84155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47213e-09 l2=2.95065e-05 x=-4.77746e-05 y=-0.000300192 z=-1.47524e-05 kx=0.000230493 ky=-0.000143213 kz=6.84893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10173e-09 l2=1.46184e-05 x=4.94631e-05 y=3.15913e-05 z=-7.30874e-06 kx=-0.000131713 ky=0.00026173 kz=6.30501 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33121e-09 l2=2.9486e-05 x=4.77778e-05 y=-0.000458976 z=-1.47418e-05 kx=-0.00015764 ky=-0.000210194 kz=4.03392 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14273e-09 l2=1.69651e-05 x=-4.92755e-05 y=0.0001148 z=-8.48325e-06 kx=2.25133e-05 ky=1.33942e-05 kz=3.06701 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20817e-09 l2=2.20582e-05 x=4.8769e-05 y=4.53638e-05 z=-1.10276e-05 kx=-0.000168589 ky=-5.5043e-05 kz=3.81864 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38466e-09 l2=2.47609e-05 x=-4.84427e-05 y=-0.000268694 z=-1.23829e-05 kx=-0.00017813 ky=8.82523e-05 kz=4.97014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66087e-09 l2=2.74824e-05 x=-4.80752e-05 y=-0.000211062 z=-1.37411e-05 kx=3.9966e-06 ky=9.9785e-07 kz=0.217282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02699e-09 l2=1.10482e-05 x=4.96937e-05 y=0.000407225 z=-5.52726e-06 kx=0.000109543 ky=0.000165929 kz=2.06246 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84548e-09 l2=1.74594e-05 x=4.92323e-05 y=0.000373499 z=-8.72996e-06 kx=-8.63716e-05 ky=0.000347157 kz=6.25783 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34925e-09 l2=1.94415e-05 x=-4.90463e-05 y=7.52252e-05 z=-9.72041e-06 kx=3.2233e-05 ky=2.98971e-05 kz=1.56202 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97348e-09 l2=1.85703e-05 x=-4.91301e-05 y=-0.000384008 z=-9.28818e-06 kx=-3.97989e-05 ky=-3.91432e-06 kz=0.946838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70511e-09 l2=2.37332e-06 x=-4.9986e-05 y=-0.000163348 z=-1.18692e-06 kx=7.30919e-05 ky=1.4491e-05 kz=6.22068 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00077e-09 l2=5.17226e-05 x=-4.27915e-05 y=6.32071e-05 z=-2.58639e-05 kx=-0.000195203 ky=7.34384e-05 kz=4.03874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13774e-09 l2=3.31091e-05 x=4.71792e-05 y=-0.000269261 z=-1.65577e-05 kx=0.000377691 ky=-0.000401509 kz=6.90985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21242e-09 l2=1.09269e-05 x=4.97008e-05 y=0.000353714 z=-5.46452e-06 kx=-3.82825e-05 ky=0.000245213 kz=3.72742 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21328e-09 l2=4.24114e-05 x=-4.52815e-05 y=0.000497862 z=-2.12046e-05 kx=8.4117e-05 ky=4.28061e-05 kz=2.3042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96433e-09 l2=1.35463e-05 x=-4.95391e-05 y=0.000497767 z=-6.77492e-06 kx=-6.06435e-05 ky=0.000256799 kz=3.83356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05031e-09 l2=3.05405e-05 x=-4.76118e-05 y=0.000200445 z=-1.52693e-05 kx=1.29278e-05 ky=2.0227e-06 kz=0.421145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5498e-09 l2=1.63237e-05 x=-4.93293e-05 y=-0.000475494 z=-8.16391e-06 kx=-6.75935e-05 ky=-0.000162192 kz=2.60137 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82476e-09 l2=1.11569e-05 x=-4.96878e-05 y=0.00049876 z=-5.58196e-06 kx=-0.000108153 ky=0.000201198 kz=2.58779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21328e-09 l2=4.24114e-05 x=-4.52815e-05 y=0.000497862 z=-2.12046e-05 kx=8.4117e-05 ky=4.28061e-05 kz=2.3042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51794e-09 l2=2.14164e-05 x=-4.88396e-05 y=0.000213355 z=-1.07112e-05 kx=-0.000217734 ky=-5.01881e-05 kz=4.74458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77653e-09 l2=2.36488e-05 x=-4.85816e-05 y=-7.66609e-05 z=-1.18266e-05 kx=-0.000165486 ky=-1.19556e-05 kz=6.30415 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06032e-09 l2=5.70078e-05 x=4.10792e-05 y=-0.000334759 z=-2.85055e-05 kx=4.50641e-05 ky=-0.000120591 kz=1.82843 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.94124e-09 l2=1.46079e-05 x=4.94635e-05 y=0.000140408 z=-7.30813e-06 kx=0.000362875 ky=-0.000218132 kz=6.61663 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18156e-09 l2=2.48334e-05 x=4.84336e-05 y=0.000256408 z=-1.24185e-05 kx=7.58556e-05 ky=7.40899e-05 kz=3.03101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.522e-09 l2=3.92584e-06 x=-4.99617e-05 y=0.000280476 z=-1.96595e-06 kx=0.000141667 ky=-3.73427e-05 kz=5.76679 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16898e-09 l2=4.12645e-05 x=-4.55442e-05 y=0.000283573 z=-2.06343e-05 kx=-5.99378e-05 ky=5.9495e-05 kz=1.90368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42612e-09 l2=1.35375e-05 x=-4.95397e-05 y=-0.000227039 z=-6.77056e-06 kx=-8.26519e-05 ky=-0.000209277 kz=3.69925 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30125e-09 l2=3.67735e-05 x=-4.64958e-05 y=0.000473998 z=-1.83899e-05 kx=-0.000342099 ky=0.000400695 kz=6.50618 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0147e-09 l2=3.48186e-05 x=-4.68706e-05 y=0.000427142 z=-1.74121e-05 kx=-0.000249504 ky=0.000258823 kz=5.21485 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1236e-09 l2=2.90535e-05 x=-4.78427e-05 y=0.000402818 z=-1.45297e-05 kx=-0.000338652 ky=0.000258273 kz=6.9381 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24911e-09 l2=1.4724e-05 x=4.9455e-05 y=-0.000318167 z=-7.36325e-06 kx=4.60618e-05 ky=-0.000139339 kz=3.6042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.84789e-09 l2=1.89976e-05 x=-4.90898e-05 y=-0.000292968 z=-9.49893e-06 kx=3.40466e-05 ky=4.14128e-05 kz=2.17597 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01369e-09 l2=2.37946e-05 x=4.8564e-05 y=0.000356796 z=-1.1898e-05 kx=3.05009e-06 ky=5.45365e-05 kz=0.670853 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04953e-09 l2=2.15231e-05 x=-4.88277e-05 y=0.000257369 z=-1.07646e-05 kx=-4.66248e-05 ky=1.32769e-05 kz=0.906607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24421e-09 l2=1.41241e-05 x=-4.94992e-05 y=0.000425638 z=-7.061e-06 kx=0.000266784 ky=-4.03483e-05 kz=6.05865 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.076e-09 l2=1.55816e-05 x=-4.93895e-05 y=-0.000218018 z=-7.79137e-06 kx=5.21499e-05 ky=5.76627e-05 kz=5.76619 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.7876e-09 l2=9.83854e-06 x=-4.97573e-05 y=0.000261376 z=-4.92302e-06 kx=-0.000328529 ky=-4.2821e-05 kz=6.93667 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62659e-09 l2=2.47435e-05 x=-4.8445e-05 y=0.000346784 z=-1.23743e-05 kx=-0.000119185 ky=0.000255777 kz=3.38361 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38924e-09 l2=1.96477e-05 x=-4.90259e-05 y=0.000298339 z=-9.82298e-06 kx=4.46643e-05 ky=9.74109e-05 kz=1.40155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.12127e-09 l2=1.25962e-05 x=-4.96018e-05 y=-0.000196302 z=-6.30115e-06 kx=-3.40904e-05 ky=-2.73213e-05 kz=1.11711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52532e-09 l2=2.82145e-05 x=4.79693e-05 y=1.55301e-06 z=-1.41063e-05 kx=-0.000143535 ky=0.000125909 kz=4.00558 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34633e-09 l2=1.21857e-05 x=4.96276e-05 y=-0.000394106 z=-6.09356e-06 kx=-1.73352e-05 ky=-5.77061e-05 kz=1.91025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28259e-09 l2=2.90063e-05 x=-4.7851e-05 y=0.000242534 z=-1.45025e-05 kx=5.89648e-05 ky=7.26987e-05 kz=2.20887 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40629e-09 l2=1.27038e-05 x=-4.95947e-05 y=-7.88593e-05 z=-6.3546e-06 kx=-0.000183118 ky=-0.000107983 kz=4.56829 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22205e-09 l2=3.33638e-05 x=4.71354e-05 y=-0.0003958 z=-1.66822e-05 kx=-9.40109e-06 ky=-0.000104495 kz=1.22753 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24212e-09 l2=3.22683e-05 x=-4.73253e-05 y=-0.000363292 z=-1.61355e-05 kx=-2.47599e-05 ky=-3.98788e-05 kz=1.77295 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24911e-09 l2=1.4724e-05 x=4.9455e-05 y=-0.000318167 z=-7.36325e-06 kx=4.60618e-05 ky=-0.000139339 kz=3.6042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28259e-09 l2=2.90063e-05 x=-4.7851e-05 y=0.000242534 z=-1.45025e-05 kx=5.89648e-05 ky=7.26987e-05 kz=2.20887 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53482e-09 l2=2.43446e-05 x=-4.84954e-05 y=-0.000325366 z=-1.2175e-05 kx=-0.000176613 ky=-0.000174714 kz=4.3795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12205e-09 l2=3.06155e-05 x=-4.75998e-05 y=7.51609e-05 z=-1.53066e-05 kx=6.4845e-05 ky=8.00276e-05 kz=1.78971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02621e-09 l2=3.97774e-05 x=4.58745e-05 y=0.000293833 z=-1.98889e-05 kx=-2.11531e-05 ky=0.000112197 kz=3.23356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00796e-09 l2=1.29767e-05 x=4.95773e-05 y=-0.00033357 z=-6.48848e-06 kx=-5.0496e-05 ky=-0.000446138 kz=6.6544 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39433e-09 l2=1.67785e-05 x=4.9291e-05 y=-0.000478013 z=-8.39177e-06 kx=0.000173017 ky=-0.000317001 kz=4.64028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08831e-09 l2=3.22066e-05 x=4.7336e-05 y=0.00020761 z=-1.61039e-05 kx=3.74584e-06 ky=-0.000125916 kz=4.36778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58057e-09 l2=2.73922e-05 x=-4.80873e-05 y=-0.000216008 z=-1.36987e-05 kx=-0.000192358 ky=-0.00022686 kz=4.96628 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14789e-09 l2=2.71958e-05 x=-4.8116e-05 y=-0.000182733 z=-1.35972e-05 kx=2.87814e-05 ky=1.43232e-05 kz=1.07866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01151e-09 l2=4.59979e-05 x=-4.43977e-05 y=0.000388571 z=-2.29975e-05 kx=4.03597e-05 ky=2.67686e-05 kz=0.91914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73892e-09 l2=1.9178e-05 x=-4.90721e-05 y=-9.62287e-06 z=-9.58991e-06 kx=-3.71653e-06 ky=0.000197495 kz=4.07031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09338e-09 l2=3.41832e-05 x=-4.69886e-05 y=-0.000110629 z=-1.70911e-05 kx=0.000145507 ky=-0.00016499 kz=6.665 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81718e-09 l2=1.43904e-05 x=-4.94799e-05 y=-0.00025029 z=-7.1945e-06 kx=1.47603e-05 ky=-2.00522e-06 kz=0.447582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51694e-09 l2=2.2719e-05 x=4.86928e-05 y=-2.42485e-05 z=-1.13597e-05 kx=-8.06528e-05 ky=-0.000213207 kz=6.98639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.56608e-09 l2=6.98144e-06 x=4.98782e-05 y=0.000258563 z=-3.49192e-06 kx=-5.41403e-05 ky=-5.08383e-05 kz=4.67409 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13757e-09 l2=2.55538e-05 x=-4.83405e-05 y=0.000121948 z=-1.27759e-05 kx=0.000173412 ky=0.000275552 kz=5.28319 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45445e-09 l2=5.29047e-06 x=-4.99299e-05 y=-0.000264527 z=-2.64741e-06 kx=-0.000124982 ky=6.71643e-06 kz=4.32136 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45492e-09 l2=1.42306e-05 x=-4.94915e-05 y=-0.000360677 z=-7.11445e-06 kx=0.000157014 ky=-0.000187486 kz=4.90585 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51694e-09 l2=2.2719e-05 x=4.86928e-05 y=-2.42485e-05 z=-1.13597e-05 kx=-8.06528e-05 ky=-0.000213207 kz=6.98639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32805e-09 l2=1.37363e-05 x=4.95264e-05 y=-0.000288947 z=-6.86677e-06 kx=-0.000120878 ky=-6.5725e-05 kz=2.93913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63209e-09 l2=1.4449e-05 x=-4.94756e-05 y=-0.000435236 z=-7.22422e-06 kx=4.22168e-05 ky=-0.000167967 kz=1.92436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4576e-09 l2=2.37144e-05 x=4.85734e-05 y=1.10521e-05 z=-1.186e-05 kx=0.00030085 ky=-4.96678e-07 kz=6.8654 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.51042e-09 l2=7.06667e-06 x=4.98752e-05 y=-4.21695e-05 z=-3.53292e-06 kx=-8.8396e-05 ky=-2.26884e-05 kz=2.64188 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80356e-09 l2=1.45358e-05 x=-4.9469e-05 y=0.000248476 z=-7.26973e-06 kx=-1.26628e-05 ky=2.46428e-05 kz=0.683316 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36932e-09 l2=1.23651e-05 x=-4.96161e-05 y=-0.000445263 z=-6.18558e-06 kx=-6.16421e-05 ky=-0.000122232 kz=1.30731 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54267e-09 l2=1.65582e-05 x=4.93099e-05 y=0.00021009 z=-8.28024e-06 kx=7.34993e-06 ky=4.87762e-05 kz=1.02849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7334e-09 l2=2.90224e-05 x=-4.78484e-05 y=-0.000471449 z=-1.45113e-05 kx=2.60196e-05 ky=-7.88058e-05 kz=1.70141 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02349e-09 l2=1.51931e-05 x=4.94199e-05 y=-0.000475215 z=-7.5953e-06 kx=-0.000200608 ky=-0.000546426 kz=5.68649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02326e-09 l2=1.11382e-05 x=-4.96886e-05 y=-0.000492458 z=-5.57229e-06 kx=-0.000233557 ky=-7.85181e-05 kz=4.31737 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15694e-09 l2=3.25054e-05 x=-4.72844e-05 y=-0.000498528 z=-1.62549e-05 kx=-0.00015443 ky=-9.56657e-05 kz=4.39384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34113e-09 l2=3.14242e-05 x=4.7468e-05 y=-0.00037065 z=-1.57108e-05 kx=-0.000279783 ky=3.286e-05 kz=6.80777 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09115e-09 l2=2.44311e-05 x=-4.84845e-05 y=0.000233161 z=-1.2218e-05 kx=-0.000268222 ky=-4.45618e-05 kz=6.94315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29911e-09 l2=3.96494e-06 x=-4.99607e-05 y=-0.000485487 z=-1.98255e-06 kx=7.9984e-06 ky=-5.99597e-05 kz=0.704876 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64217e-09 l2=1.2363e-05 x=4.96162e-05 y=-0.000308878 z=-6.18492e-06 kx=0.00035327 ky=-0.000429097 kz=6.81358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06121e-09 l2=4.03006e-05 x=-4.57598e-05 y=-0.000106953 z=-2.01516e-05 kx=-0.000107222 ky=5.22579e-05 kz=6.7099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40132e-09 l2=2.0137e-05 x=4.8976e-05 y=0.000417349 z=-1.00687e-05 kx=-3.30621e-05 ky=9.98579e-05 kz=3.01148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17712e-09 l2=1.25915e-05 x=-4.96019e-05 y=-6.7635e-05 z=-6.29843e-06 kx=-7.68033e-05 ky=7.82607e-06 kz=1.83367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4273e-09 l2=3.72992e-05 x=-4.63925e-05 y=-0.000285789 z=-1.86492e-05 kx=1.15538e-05 ky=4.60987e-06 kz=0.456287 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05341e-09 l2=2.32398e-05 x=-4.86308e-05 y=-0.000274594 z=-1.16219e-05 kx=-6.21849e-05 ky=-0.000101625 kz=2.06011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55484e-09 l2=2.76785e-05 x=-4.80474e-05 y=0.000280631 z=-1.38379e-05 kx=8.38592e-05 ky=4.68893e-05 kz=1.86399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06894e-09 l2=1.85377e-05 x=-4.91336e-05 y=-0.000420111 z=-9.26861e-06 kx=5.13232e-05 ky=-0.000291939 kz=3.31114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33189e-09 l2=1.2415e-05 x=-4.9613e-05 y=0.000474729 z=-6.21029e-06 kx=-0.000198773 ky=0.000296938 kz=4.64799 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58249e-09 l2=1.2869e-05 x=4.95844e-05 y=0.000154877 z=-6.43464e-06 kx=-4.08991e-05 ky=-3.23364e-05 kz=3.05824 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22428e-09 l2=1.80264e-05 x=4.91808e-05 y=-0.000371792 z=-9.01509e-06 kx=0.000180586 ky=-0.000313862 kz=6.9201 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56822e-09 l2=2.35445e-05 x=-4.85946e-05 y=-0.000222936 z=-1.17727e-05 kx=2.33904e-05 ky=-0.000152547 kz=3.54622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12078e-09 l2=1.36856e-05 x=4.95293e-05 y=-0.000474891 z=-6.84571e-06 kx=1.50988e-05 ky=-3.13948e-06 kz=0.31782 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36129e-09 l2=1.68578e-05 x=4.92846e-05 y=0.000125813 z=-8.42893e-06 kx=-3.1118e-05 ky=6.09703e-05 kz=2.30506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44324e-09 l2=1.87494e-05 x=-4.9113e-05 y=0.000108808 z=-9.37748e-06 kx=-0.000213129 ky=6.46943e-05 kz=5.0677 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10164e-09 l2=1.48572e-05 x=-4.94452e-05 y=5.93353e-05 z=-7.43019e-06 kx=-7.33049e-05 ky=0.000101379 kz=6.47937 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16135e-09 l2=2.91646e-05 x=-4.78263e-05 y=0.000295651 z=-1.45836e-05 kx=-2.93512e-05 ky=0.00011411 kz=1.90663 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02675e-09 l2=3.01537e-05 x=-4.76723e-05 y=-0.000161034 z=-1.50793e-05 kx=-4.44442e-05 ky=-4.3175e-05 kz=1.10008 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71569e-09 l2=5.1907e-06 x=-4.99327e-05 y=0.000394468 z=-2.5959e-06 kx=0.000101011 ky=0.000261483 kz=6.24886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81712e-09 l2=2.12858e-05 x=-4.88542e-05 y=0.000407894 z=-1.06446e-05 kx=-0.000117675 ky=0.000139193 kz=6.96628 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57468e-09 l2=2.01269e-05 x=-4.89774e-05 y=0.000407004 z=-1.00621e-05 kx=0.00016956 ky=0.000131922 kz=3.92449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15298e-09 l2=3.29026e-05 x=4.72167e-05 y=0.000490397 z=-1.64506e-05 kx=-9.7961e-05 ky=8.14061e-05 kz=3.53874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09627e-09 l2=2.04651e-05 x=4.89423e-05 y=-0.000499883 z=-1.02311e-05 kx=-0.000100935 ky=-0.000159214 kz=2.42956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32086e-09 l2=3.32425e-05 x=-4.71563e-05 y=0.000391868 z=-1.66231e-05 kx=-2.14478e-05 ky=2.67876e-05 kz=0.889362 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.68102e-09 l2=2.26574e-05 x=-4.86995e-05 y=-0.000244582 z=-1.13321e-05 kx=-0.000298835 ky=-0.000292013 kz=7.03529 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17029e-09 l2=4.88291e-05 x=4.36353e-05 y=-0.00032817 z=-2.44135e-05 kx=-0.000255735 ky=-0.000503114 kz=6.85236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29598e-09 l2=2.18955e-05 x=4.8787e-05 y=0.000342475 z=-1.0948e-05 kx=-3.69833e-05 ky=5.95673e-05 kz=4.6669 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60704e-09 l2=1.62212e-05 x=-4.93382e-05 y=-0.000367635 z=-8.11003e-06 kx=9.99301e-05 ky=-0.00018283 kz=3.61475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24225e-09 l2=7.35338e-06 x=-4.98647e-05 y=0.000166686 z=-3.67794e-06 kx=-1.9355e-06 ky=-9.55733e-06 kz=0.755997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01423e-09 l2=2.68894e-05 x=-4.81592e-05 y=2.41565e-05 z=-1.34431e-05 kx=0.000118421 ky=5.01236e-06 kz=2.72217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13718e-09 l2=1.34374e-05 x=4.95469e-05 y=0.000396728 z=-6.71826e-06 kx=-0.00014279 ky=0.000140932 kz=4.70163 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02221e-09 l2=3.92914e-05 x=-4.59796e-05 y=-0.000353313 z=-1.96447e-05 kx=0.000189996 ky=-0.00028379 kz=5.78328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.405e-09 l2=1.1837e-05 x=-4.96488e-05 y=-0.000233805 z=-5.91712e-06 kx=6.19613e-05 ky=-2.20402e-05 kz=1.47527 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.25259e-08 l2=1.10974e-06 x=4.99971e-05 y=-0.000142605 z=-5.71357e-07 kx=1.82095e-05 ky=0.000136965 kz=4.09013 *** TRACE end *** Detector: psd0_I=7.95775e-10 psd0_ERR=1.1254e-13 psd0_N=5e+07 "psd0.dat" Detector: psd4pi_I=7.95766e-10 psd4pi_ERR=1.12582e-13 psd4pi_N=5e+07 "psd4pi.dat" Single_crystal: sample: Error message was repeated 2891 times with absorbed x-rays. INFO: Placing instr file copy /home/nexmap/pkwi/xTESTS/2023-02-01/McXtrace_CPU_MPICC_KISS_5e7/Test_SX/Test_SX.instr in dataset 1