loading system configuration loading override configuration from /home/nexmap/pkwi/mxtest/mctest/../mccodelib/mcxtrace-test/McXtrace-1.x_CPU_MPICC/mccode_config.json INFO: Using directory: "1" INFO: Using existing c-file: ./Test_SX.c INFO: Using existing binary: ./Test_SX.out INFO: === Simulation 'Test_SX' (/home/nexmap/pkwi/xTESTS/2022-12-01/McXtrace-1.x_CPU_MPICC_5e7/Test_SX/Test_SX.instr): running on 16 nodes (master is 'elearn1.fysik.dtu.dk', MPI version 3.1). Opening input file '/home/nexmap/pkwi/McXtrace/mcxtrace/1.x-dev/tools/Python/mxrun/../mccodelib/../../../data/Mo.lau' (Table_Read_Offset) Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Opening input file '/home/nexmap/pkwi/McXtrace/mcxtrace/1.x-dev/tools/Python/mxrun/../mccodelib/../../../data/Mo.txt' (Table_Read_Offset) Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29276e-09 l2=1.33118e-05 x=4.9555e-05 y=0.000325269 z=-6.6569e-06 kx=0.000150892 ky=-0.000262869 kz=22.9515 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32806e-09 l2=7.34392e-06 x=-4.98652e-05 y=0.000379594 z=-3.67092e-06 kx=0.000785585 ky=0.00131643 kz=23.0274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58174e-09 l2=2.40115e-05 x=-4.85376e-05 y=-0.00041138 z=-1.20057e-05 kx=0.000405242 ky=-0.000508901 kz=23.2944 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4373e-09 l2=1.66192e-05 x=-4.93049e-05 y=0.000411844 z=-8.30969e-06 kx=0.00028887 ky=0.000867373 kz=23.2934 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56739e-09 l2=7.34185e-06 x=-4.98652e-05 y=4.48838e-05 z=-3.67089e-06 kx=0.000374873 ky=0.000356032 kz=22.951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02356e-09 l2=4.26366e-05 x=-4.52282e-05 y=8.06938e-05 z=-2.13179e-05 kx=0.000459714 ky=-0.000456436 kz=23.1367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44505e-09 l2=1.37522e-05 x=-4.95253e-05 y=8.55401e-05 z=-6.87471e-06 kx=0.000950336 ky=-0.0001006 kz=22.4507 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04161e-09 l2=2.18688e-05 x=-4.87903e-05 y=0.000248549 z=-1.09328e-05 kx=0.00101568 ky=0.000386805 kz=23.2768 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46016e-09 l2=8.71946e-06 x=-4.98095e-05 y=3.61723e-05 z=-4.36322e-06 kx=-0.0010343 ky=0.00109093 kz=22.7852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23674e-09 l2=2.18834e-05 x=4.8788e-05 y=-0.000416333 z=-1.09434e-05 kx=0.000514215 ky=-0.00153222 kz=23.0273 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16507e-09 l2=1.75466e-05 x=4.92241e-05 y=0.000178926 z=-8.77525e-06 kx=0.000612886 ky=0.00139037 kz=22.3414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68096e-09 l2=6.74138e-06 x=-4.98863e-05 y=0.000445714 z=-3.37153e-06 kx=2.16716e-07 ky=0.00124584 kz=22.3299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78644e-09 l2=2.75442e-06 x=4.99811e-05 y=-3.58751e-05 z=-1.37763e-06 kx=-0.000214769 ky=-0.000296864 kz=22.488 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04545e-09 l2=2.57608e-05 x=4.83131e-05 y=0.000315847 z=-1.28793e-05 kx=-0.000795581 ky=0.00034824 kz=22.912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22909e-09 l2=2.57222e-05 x=-4.83182e-05 y=9.62198e-05 z=-1.28602e-05 kx=0.000725077 ky=0.000160038 kz=22.7015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05343e-09 l2=3.12147e-05 x=-4.75022e-05 y=-0.000259837 z=-1.56069e-05 kx=0.00047623 ky=3.81547e-05 kz=23.3003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.064e-09 l2=2.42974e-05 x=-4.85011e-05 y=-0.000286749 z=-1.21518e-05 kx=-0.00122006 ky=-0.000928055 kz=22.643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46482e-09 l2=1.06924e-05 x=-4.97136e-05 y=0.000205493 z=-5.34512e-06 kx=0.000831735 ky=0.000678013 kz=23.0298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13418e-09 l2=4.28901e-06 x=4.99541e-05 y=0.000384651 z=-2.14511e-06 kx=-0.000212108 ky=-6.81936e-05 kz=22.8726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.20834e-09 l2=8.47959e-06 x=-4.98201e-05 y=-0.000329058 z=-4.24016e-06 kx=0.000342612 ky=-9.40944e-05 kz=23.0736 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09709e-09 l2=1.18713e-05 x=4.96466e-05 y=0.000155324 z=-5.93533e-06 kx=-0.00040314 ky=-0.000166109 kz=22.8377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.91022e-09 l2=3.68744e-06 x=-4.99661e-05 y=-7.56921e-06 z=-1.84522e-06 kx=0.000440349 ky=-0.000910726 kz=22.916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23288e-09 l2=5.01456e-06 x=-4.99371e-05 y=-0.000455696 z=-2.50849e-06 kx=-4.07619e-05 ky=-0.000869012 kz=23.1387 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04512e-09 l2=3.94559e-05 x=4.59434e-05 y=0.00026194 z=-1.97293e-05 kx=0.00040613 ky=-0.000137397 kz=23.0326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2746e-09 l2=2.04016e-05 x=-4.89489e-05 y=-0.00017122 z=-1.01996e-05 kx=0.0008387 ky=0.000186615 kz=22.3472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39322e-09 l2=1.80281e-05 x=4.91813e-05 y=0.000477415 z=-9.0127e-06 kx=-0.000955677 ky=0.00224344 kz=23.1699 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02457e-09 l2=2.29373e-05 x=-4.86666e-05 y=-0.000374458 z=-1.14712e-05 kx=-0.000968807 ky=-0.000639849 kz=22.8156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.48734e-09 l2=4.58582e-06 x=4.99476e-05 y=-8.74636e-05 z=-2.29302e-06 kx=-0.000729426 ky=-0.00123009 kz=22.3348 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87877e-09 l2=6.20866e-06 x=4.99037e-05 y=-0.000291721 z=-3.10369e-06 kx=-0.000714898 ky=-0.00126428 kz=22.635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27276e-09 l2=2.68021e-05 x=-4.81714e-05 y=-0.000151278 z=-1.33997e-05 kx=0.00093528 ky=-0.00020577 kz=22.9769 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00846e-09 l2=2.14041e-05 x=-4.88408e-05 y=0.000215202 z=-1.07051e-05 kx=-0.00118454 ky=0.00142028 kz=23.1541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27342e-09 l2=3.40941e-05 x=4.70044e-05 y=0.000249907 z=-1.70479e-05 kx=0.000120871 ky=6.74918e-05 kz=22.981 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16458e-08 l2=9.30464e-07 x=-4.99979e-05 y=-0.000309336 z=-4.77319e-07 kx=-0.000573188 ky=0.000275601 kz=22.6646 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58308e-09 l2=4.2619e-06 x=-4.99546e-05 y=0.000320451 z=-2.13301e-06 kx=-0.000345535 ky=4.4212e-05 kz=22.5236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47935e-09 l2=1.05634e-05 x=-4.97201e-05 y=0.000467727 z=-5.28453e-06 kx=-0.00095134 ky=0.000132941 kz=22.5144 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98744e-09 l2=8.31857e-06 x=-4.98267e-05 y=0.000225539 z=-4.16073e-06 kx=-0.000205855 ky=-0.000559931 kz=23.0604 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43479e-09 l2=3.74403e-06 x=-4.9965e-05 y=0.00012195 z=-1.8714e-06 kx=0.000616102 ky=0.00141157 kz=23.0457 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10427e-09 l2=1.89026e-05 x=4.90984e-05 y=-0.000256612 z=-9.45325e-06 kx=0.000644149 ky=0.000457025 kz=22.7 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25022e-09 l2=1.99936e-05 x=4.89901e-05 y=2.50684e-05 z=-9.9996e-06 kx=0.00100339 ky=-0.000864869 kz=22.7905 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.044e-09 l2=2.60859e-05 x=4.82688e-05 y=0.000447367 z=-1.30442e-05 kx=0.000306018 ky=0.00203658 kz=22.4166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04441e-09 l2=3.09684e-05 x=4.75422e-05 y=0.000268633 z=-1.54844e-05 kx=-0.000149727 ky=0.000128001 kz=23.2858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.96687e-09 l2=5.24816e-06 x=-4.99312e-05 y=-0.000151209 z=-2.62675e-06 kx=-0.000316069 ky=0.000528531 kz=22.7836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33712e-09 l2=5.60421e-06 x=-4.99214e-05 y=3.80232e-05 z=-2.80564e-06 kx=-0.00109801 ky=0.000502539 kz=23.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71608e-09 l2=1.13379e-05 x=-4.96776e-05 y=0.000246824 z=-5.67132e-06 kx=-0.000467991 ky=0.000913053 kz=22.7644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01294e-09 l2=3.52396e-05 x=-4.67932e-05 y=-0.000482384 z=-1.76192e-05 kx=0.000525799 ky=7.69586e-06 kz=22.3985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29042e-09 l2=2.29245e-05 x=-4.86691e-05 y=-0.000289221 z=-1.14608e-05 kx=0.000978567 ky=-0.00170381 kz=23.0309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0221e-09 l2=2.36781e-05 x=-4.85782e-05 y=0.000306156 z=-1.18398e-05 kx=-0.00011705 ky=0.000828006 kz=22.7007 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28204e-09 l2=1.1006e-05 x=-4.96962e-05 y=-8.58425e-05 z=-5.5047e-06 kx=-0.000465705 ky=-0.000836557 kz=22.304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64753e-09 l2=4.06289e-06 x=4.99587e-05 y=0.000377035 z=-2.03382e-06 kx=0.000696931 ky=0.00172645 kz=22.4071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18822e-09 l2=1.65375e-05 x=-4.93112e-05 y=-0.000196056 z=-8.27181e-06 kx=-0.00111309 ky=0.000542643 kz=22.4765 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7058e-09 l2=1.08271e-05 x=4.9706e-05 y=-0.000446298 z=-5.41635e-06 kx=0.000885927 ky=-0.000666345 kz=22.9166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21547e-09 l2=1.00941e-05 x=4.97447e-05 y=0.000318771 z=-5.04774e-06 kx=3.43088e-05 ky=-5.55219e-05 kz=22.4251 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02629e-09 l2=1.36388e-05 x=4.95326e-05 y=-0.000279979 z=-6.82135e-06 kx=0.000663607 ky=-0.000249623 kz=23.1605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5901e-09 l2=6.08187e-06 x=4.99077e-05 y=-0.000171647 z=-3.04082e-06 kx=-0.000879375 ky=0.000131414 kz=23.015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32745e-09 l2=8.1131e-06 x=-4.98353e-05 y=8.90678e-06 z=-4.05634e-06 kx=0.000409821 ky=0.000709231 kz=23.2504 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05355e-09 l2=1.32963e-05 x=4.95563e-05 y=-0.00036761 z=-6.64697e-06 kx=-0.000772928 ky=-0.000518479 kz=22.3248 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46302e-09 l2=2.94942e-05 x=4.77763e-05 y=-6.26509e-05 z=-1.47469e-05 kx=-0.000468235 ky=-0.000375523 kz=23.2961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67455e-09 l2=2.7955e-05 x=4.80061e-05 y=-0.000218541 z=-1.39806e-05 kx=0.00108491 ky=-0.00137252 kz=22.9845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32769e-08 l2=1.06839e-06 x=-4.99972e-05 y=4.08209e-05 z=-5.4286e-07 kx=-0.000927308 ky=-0.000588014 kz=22.8556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56694e-09 l2=2.23586e-05 x=4.87338e-05 y=0.00040386 z=-1.11825e-05 kx=0.001111 ky=0.000213248 kz=22.633 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03032e-08 l2=1.47955e-06 x=4.99946e-05 y=-0.000302641 z=-7.4387e-07 kx=-0.000483976 ky=-0.000571839 kz=22.9014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38516e-09 l2=4.82449e-06 x=4.99419e-05 y=-0.000439956 z=-2.41122e-06 kx=-0.00102896 ky=-0.00138929 kz=23.1493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34898e-09 l2=3.98033e-06 x=-4.99604e-05 y=0.000137508 z=-1.98983e-06 kx=0.000457658 ky=-0.000436673 kz=22.7527 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31713e-09 l2=1.88152e-05 x=-4.91069e-05 y=-9.44147e-05 z=-9.40929e-06 kx=-0.000470143 ky=0.000111697 kz=22.7258 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02911e-09 l2=2.82564e-05 x=4.79622e-05 y=-0.000289878 z=-1.41298e-05 kx=0.000521325 ky=-0.00158205 kz=22.329 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43417e-09 l2=1.18723e-05 x=4.96464e-05 y=-0.000231532 z=-5.93694e-06 kx=3.9221e-05 ky=0.000498857 kz=22.512 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07561e-09 l2=8.90283e-06 x=-4.98017e-05 y=0.000360671 z=-4.44985e-06 kx=0.000957623 ky=0.00156901 kz=22.6866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06697e-09 l2=9.83045e-06 x=-4.9758e-05 y=-0.000133811 z=-4.91471e-06 kx=0.000477305 ky=0.000361688 kz=22.6644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2266e-09 l2=1.92955e-05 x=4.90608e-05 y=-0.000131423 z=-9.64672e-06 kx=-0.0007546 ky=-0.000749765 kz=22.4581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89115e-09 l2=9.39141e-06 x=-4.97791e-05 y=3.49085e-05 z=-4.69701e-06 kx=-0.000167377 ky=-0.00104276 kz=22.9729 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.99488e-09 l2=5.16858e-06 x=-4.99331e-05 y=-0.000440779 z=-2.58839e-06 kx=-0.00117388 ky=-0.000289994 kz=22.5188 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.93259e-09 l2=8.41912e-06 x=-4.98227e-05 y=-0.000271883 z=-4.20988e-06 kx=0.000532777 ky=-0.000458091 kz=23.1045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26537e-09 l2=2.23992e-05 x=4.87292e-05 y=0.000438878 z=-1.12024e-05 kx=0.00100751 ky=0.00194639 kz=23.2002 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56943e-09 l2=1.05576e-05 x=-4.97207e-05 y=-0.000451984 z=-5.2793e-06 kx=0.000121566 ky=-0.00182596 kz=23.1889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56268e-09 l2=1.60625e-05 x=4.93507e-05 y=3.94924e-05 z=-8.03314e-06 kx=0.000511465 ky=0.00125119 kz=23.2863 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07727e-09 l2=1.88419e-05 x=4.91043e-05 y=0.000295422 z=-9.42285e-06 kx=0.000621964 ky=0.00144484 kz=22.4031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85898e-09 l2=7.23528e-06 x=-4.9869e-05 y=-0.000386903 z=-3.61928e-06 kx=-9.35251e-05 ky=-0.000355667 kz=22.7417 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13506e-09 l2=1.84472e-05 x=4.91415e-05 y=0.000461689 z=-9.22684e-06 kx=0.00126068 ky=0.000857282 kz=23.2787 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01215e-09 l2=1.73595e-05 x=-4.92412e-05 y=-0.000387095 z=-8.67878e-06 kx=0.000686762 ky=-0.000752444 kz=23.1296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42699e-09 l2=2.4248e-05 x=4.85081e-05 y=0.000205698 z=-1.21241e-05 kx=-0.000286623 ky=0.00130973 kz=22.9479 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11407e-09 l2=1.97765e-05 x=-4.90129e-05 y=0.000101449 z=-9.88723e-06 kx=0.00075486 ky=-0.000600352 kz=23.0747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58518e-09 l2=1.06138e-05 x=4.97176e-05 y=0.000406602 z=-5.30781e-06 kx=4.86186e-05 ky=0.00036492 kz=22.6935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34123e-09 l2=9.50543e-06 x=4.97736e-05 y=0.000387312 z=-4.75554e-06 kx=0.00076624 ky=-2.4968e-05 kz=23.0971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.891e-09 l2=2.09629e-05 x=-4.88896e-05 y=0.000391365 z=-1.04809e-05 kx=0.000717804 ky=0.00191532 kz=22.6374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35927e-09 l2=8.90255e-06 x=4.98017e-05 y=0.000416776 z=-4.4512e-06 kx=-0.000587417 ky=0.00193443 kz=23.2513 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29434e-09 l2=2.71344e-05 x=4.81243e-05 y=-0.000346899 z=-1.35678e-05 kx=1.07934e-06 ky=-0.00166887 kz=22.4847 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10698e-09 l2=1.08865e-05 x=4.9703e-05 y=-6.97037e-05 z=-5.44314e-06 kx=-0.000303403 ky=-0.00122908 kz=22.4948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49861e-09 l2=1.65448e-05 x=-4.93108e-05 y=-8.71468e-05 z=-8.27438e-06 kx=-0.000580487 ky=-0.000294596 kz=22.8277 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.71252e-09 l2=5.99501e-06 x=4.99102e-05 y=-0.000184041 z=-2.99942e-06 kx=2.53704e-05 ky=-0.000774317 kz=22.4651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16292e-09 l2=2.07732e-05 x=-4.89091e-05 y=-0.000390406 z=-1.03885e-05 kx=-0.000633944 ky=-0.000366756 kz=22.5493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02239e-09 l2=2.35137e-05 x=4.85984e-05 y=-0.000101923 z=-1.17567e-05 kx=-0.000337416 ky=0.000772425 kz=23.0395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91199e-09 l2=2.01547e-05 x=-4.89742e-05 y=0.000221498 z=-1.0078e-05 kx=0.00011333 ky=0.00110529 kz=22.595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.75903e-09 l2=5.8832e-06 x=-4.99135e-05 y=0.000406639 z=-2.94429e-06 kx=-0.000377722 ky=0.00123137 kz=23.2556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74169e-09 l2=1.78906e-05 x=4.91938e-05 y=0.000127176 z=-8.94433e-06 kx=-0.00084463 ky=-9.2664e-05 kz=22.7139 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26976e-09 l2=1.49539e-05 x=4.9438e-05 y=3.79702e-05 z=-7.4771e-06 kx=-0.000213824 ky=0.000510744 kz=22.3217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39726e-09 l2=1.95158e-05 x=4.90386e-05 y=0.000307152 z=-9.75927e-06 kx=0.000316562 ky=0.000744229 kz=22.4576 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.81872e-09 l2=9.49508e-06 x=-4.97742e-05 y=0.000170637 z=-4.74937e-06 kx=-0.000190576 ky=-4.79489e-05 kz=22.72 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00221e-09 l2=8.75374e-06 x=4.98083e-05 y=0.000208981 z=-4.37552e-06 kx=-0.000854156 ky=0.000131707 kz=22.9328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05266e-09 l2=1.93055e-05 x=-4.90591e-05 y=-0.000499733 z=-9.65507e-06 kx=-0.000859883 ky=-0.00151501 kz=23.2296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04246e-09 l2=1.36583e-05 x=-4.95315e-05 y=0.000434306 z=-6.82989e-06 kx=-8.84114e-05 ky=0.000516792 kz=22.9616 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03682e-09 l2=3.10176e-05 x=-4.75336e-05 y=-4.77721e-06 z=-1.55111e-05 kx=-0.000822397 ky=-0.000755341 kz=22.4115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05e-09 l2=1.7371e-05 x=4.92402e-05 y=0.00026773 z=-8.68525e-06 kx=-0.000600605 ky=0.000526774 kz=23.2916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.08019e-09 l2=1.30669e-05 x=-4.95717e-05 y=0.000486886 z=-6.53264e-06 kx=0.000852613 ky=0.00220934 kz=22.9352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48065e-09 l2=2.35011e-05 x=-4.86002e-05 y=0.000493479 z=-1.17495e-05 kx=0.000840932 ky=0.00148653 kz=22.5207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19443e-09 l2=2.14329e-05 x=-4.88386e-05 y=0.000364122 z=-1.07152e-05 kx=0.000865883 ky=0.00168599 kz=23.0502 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04904e-09 l2=2.28402e-05 x=-4.86786e-05 y=-0.00019931 z=-1.14199e-05 kx=0.000350992 ky=2.15518e-05 kz=22.4116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2496e-09 l2=1.46039e-05 x=4.94642e-05 y=0.000188936 z=-7.30148e-06 kx=-0.000505943 ky=-0.000712622 kz=23.212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01819e-09 l2=2.16949e-05 x=-4.88094e-05 y=-0.000497898 z=-1.08472e-05 kx=0.000369733 ky=-0.000112415 kz=23.225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37849e-09 l2=4.46142e-06 x=4.99503e-05 y=0.000171972 z=-2.23025e-06 kx=-0.00051863 ky=0.000805122 kz=22.4531 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12325e-08 l2=4.12265e-06 x=-4.99578e-05 y=3.93709e-05 z=-2.06512e-06 kx=0.000833035 ky=-0.000171187 kz=22.8285 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1025e-09 l2=3.57112e-05 x=4.67034e-05 y=0.000461999 z=-1.78558e-05 kx=-0.000168554 ky=0.00202397 kz=23.0612 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12421e-09 l2=2.02537e-05 x=-4.89643e-05 y=0.000255808 z=-1.01253e-05 kx=0.00100163 ky=0.00158689 kz=22.8903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58811e-09 l2=7.86741e-06 x=-4.98451e-05 y=0.000274911 z=-3.93518e-06 kx=-8.31482e-05 ky=0.000776243 kz=22.9204 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00351e-09 l2=1.17408e-05 x=-4.96544e-05 y=0.000474581 z=-5.86938e-06 kx=0.000688705 ky=0.00209544 kz=22.6907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21479e-09 l2=2.41514e-05 x=-4.85204e-05 y=0.000205215 z=-1.20746e-05 kx=0.000790587 ky=0.00144102 kz=22.4999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21809e-09 l2=2.80175e-05 x=4.79974e-05 y=-6.96512e-05 z=-1.401e-05 kx=0.000299174 ky=-0.00107746 kz=22.8818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49973e-09 l2=2.77432e-05 x=-4.80381e-05 y=-0.000156618 z=-1.38702e-05 kx=0.000989357 ky=-0.000971457 kz=22.4791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11591e-09 l2=3.79216e-05 x=4.6265e-05 y=-4.50596e-05 z=-1.8963e-05 kx=0.000844422 ky=0.00037228 kz=23.1071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.01662e-09 l2=7.46899e-06 x=4.98606e-05 y=-0.000256676 z=-3.73447e-06 kx=-0.00094255 ky=-0.00104214 kz=23.1573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41957e-09 l2=1.54804e-05 x=4.9397e-05 y=2.34311e-05 z=-7.74354e-06 kx=0.0012001 ky=-0.000371236 kz=22.3586 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18944e-09 l2=1.78264e-05 x=4.91997e-05 y=-0.000201198 z=-8.91247e-06 kx=-0.000836397 ky=0.000214804 kz=22.8653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.91896e-09 l2=3.03684e-06 x=-4.9977e-05 y=0.000491649 z=-1.52387e-06 kx=-0.000920309 ky=0.00211368 kz=23.1094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.193e-09 l2=1.09394e-05 x=4.96998e-05 y=0.000309701 z=-5.47264e-06 kx=0.000844453 ky=0.00104664 kz=22.8034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02566e-09 l2=3.42413e-05 x=4.69769e-05 y=0.000457981 z=-1.71232e-05 kx=0.000997554 ky=-6.2884e-05 kz=22.796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51829e-09 l2=1.18086e-05 x=-4.96504e-05 y=-0.000310012 z=-5.90411e-06 kx=0.000436738 ky=-0.000713574 kz=23.0715 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13379e-09 l2=3.31216e-05 x=-4.71784e-05 y=-0.000497202 z=-1.65601e-05 kx=0.000603792 ky=-0.00102017 kz=22.9235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6162e-09 l2=2.06275e-05 x=-4.89251e-05 y=0.000394651 z=-1.03133e-05 kx=0.000573533 ky=-4.70859e-05 kz=22.3529 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02202e-09 l2=3.15199e-05 x=-4.7452e-05 y=7.9543e-05 z=-1.57589e-05 kx=0.00072322 ky=-0.000611997 kz=22.4056 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07753e-09 l2=1.85921e-05 x=-4.91283e-05 y=0.000141219 z=-9.29678e-06 kx=-7.97246e-05 ky=0.00101242 kz=23.0554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55156e-09 l2=1.37245e-05 x=4.95266e-05 y=-0.000156525 z=-6.8654e-06 kx=0.00109889 ky=-0.00044299 kz=23.0787 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62907e-09 l2=1.65113e-05 x=-4.93142e-05 y=-0.000397088 z=-8.25471e-06 kx=0.00080343 ky=-0.000780206 kz=22.9041 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12382e-09 l2=1.13845e-05 x=-4.96748e-05 y=0.000463697 z=-5.69406e-06 kx=-0.000576047 ky=0.000771132 kz=23.0865 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35157e-09 l2=8.11765e-06 x=4.9835e-05 y=0.00028781 z=-4.05948e-06 kx=-9.43811e-06 ky=9.28475e-06 kz=22.8638 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1988e-09 l2=1.66639e-05 x=-4.9301e-05 y=0.00010183 z=-8.33243e-06 kx=4.45042e-05 ky=0.000803789 kz=22.5072 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25703e-09 l2=1.24059e-05 x=-4.96138e-05 y=0.000309521 z=-6.20379e-06 kx=-8.82093e-05 ky=0.00085341 kz=22.4002 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24831e-09 l2=2.6651e-05 x=-4.81917e-05 y=-0.000487882 z=-1.33266e-05 kx=-0.000212092 ky=-0.000207462 kz=22.7354 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66484e-09 l2=9.69485e-06 x=4.97644e-05 y=-0.000386149 z=-4.84932e-06 kx=0.000491336 ky=-0.000938826 kz=22.9328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09147e-09 l2=2.49406e-05 x=4.84202e-05 y=-0.000340812 z=-1.24703e-05 kx=-0.00025815 ky=-0.000596194 kz=22.8671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51774e-09 l2=1.15965e-05 x=4.96625e-05 y=0.000382133 z=-5.80147e-06 kx=0.00113005 ky=0.000815685 kz=22.797 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04104e-09 l2=1.44385e-05 x=-4.94763e-05 y=-5.81422e-05 z=-7.21911e-06 kx=0.000308147 ky=-0.00122629 kz=22.7812 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18226e-09 l2=5.76042e-06 x=-4.9917e-05 y=2.16496e-05 z=-2.88154e-06 kx=-0.000330189 ky=0.000690072 kz=22.4721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09498e-09 l2=2.40696e-05 x=4.85301e-05 y=0.000495252 z=-1.20355e-05 kx=5.79585e-05 ky=0.00107289 kz=22.4157 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50985e-09 l2=2.09393e-05 x=4.88914e-05 y=-9.78539e-06 z=-1.04718e-05 kx=0.00065939 ky=-0.000229705 kz=22.7408 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.8905e-09 l2=4.80563e-06 x=4.99423e-05 y=-0.000488766 z=-2.40614e-06 kx=0.00061706 ky=-0.000217716 kz=22.3214 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18481e-09 l2=1.36843e-05 x=-4.95299e-05 y=-0.000464 z=-6.84135e-06 kx=0.000651703 ky=-0.00138946 kz=22.8192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28665e-09 l2=2.51028e-05 x=4.83989e-05 y=0.000302422 z=-1.2553e-05 kx=0.000472055 ky=-0.000320798 kz=23.2774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24056e-09 l2=1.04643e-05 x=4.97255e-05 y=-0.000246032 z=-5.23452e-06 kx=0.000572721 ky=-0.000990008 kz=22.9063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01598e-09 l2=2.18275e-05 x=-4.87941e-05 y=-3.66007e-05 z=-1.09158e-05 kx=-0.000706138 ky=0.000699974 kz=23.2276 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.54947e-09 l2=5.91829e-06 x=-4.99124e-05 y=0.000159913 z=-2.96441e-06 kx=-0.00113775 ky=0.00111497 kz=22.8037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68842e-09 l2=1.69001e-05 x=-4.92812e-05 y=0.000392188 z=-8.4492e-06 kx=0.000768217 ky=0.000977102 kz=22.6217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18819e-09 l2=2.17375e-05 x=-4.8804e-05 y=-4.2974e-05 z=-1.08719e-05 kx=-0.00122264 ky=-0.000201727 kz=23.2164 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63033e-09 l2=2.90401e-05 x=4.78452e-05 y=-0.000347751 z=-1.45218e-05 kx=0.000460018 ky=-0.00104709 kz=22.8326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54461e-09 l2=1.60641e-05 x=-4.93506e-05 y=-5.15289e-06 z=-8.03361e-06 kx=-0.000365921 ky=0.000129371 kz=22.5185 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88558e-09 l2=4.31753e-06 x=-4.99535e-05 y=0.000337233 z=-2.15876e-06 kx=0.00042518 ky=0.00187446 kz=22.4814 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29056e-09 l2=1.28958e-05 x=-4.95823e-05 y=-2.57969e-05 z=-6.45059e-06 kx=-0.000923364 ky=0.000686853 kz=22.4286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24908e-09 l2=1.64602e-05 x=-4.93177e-05 y=-9.50553e-05 z=-8.23302e-06 kx=-0.00103213 ky=-0.000727271 kz=22.3645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.89029e-09 l2=7.96349e-06 x=-4.98415e-05 y=-0.000284737 z=-3.98115e-06 kx=0.000939339 ky=-2.33688e-05 kz=22.9948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.34754e-09 l2=2.60994e-06 x=4.99829e-05 y=0.000170987 z=-1.30918e-06 kx=0.00116482 ky=0.00103022 kz=22.9879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42427e-09 l2=1.69337e-05 x=4.92781e-05 y=-0.00020947 z=-8.46688e-06 kx=-0.000333171 ky=-0.00161817 kz=23.2982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11469e-09 l2=1.77782e-05 x=4.92034e-05 y=-0.000145221 z=-8.8916e-06 kx=0.000673959 ky=0.000761812 kz=23.0035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81033e-09 l2=8.27187e-06 x=4.98289e-05 y=-0.000464406 z=-4.13524e-06 kx=-0.000748374 ky=-0.00138487 kz=23.2643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.04846e-09 l2=4.02552e-06 x=4.99595e-05 y=-6.72137e-06 z=-2.01488e-06 kx=0.000270806 ky=-0.000940771 kz=22.7653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23409e-09 l2=1.42631e-05 x=4.94886e-05 y=0.00012705 z=-7.134e-06 kx=0.000844266 ky=-9.754e-05 kz=22.6732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07953e-09 l2=2.02344e-05 x=-4.89655e-05 y=-0.000482129 z=-1.01192e-05 kx=-0.000699463 ky=-0.00122463 kz=23.3074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17868e-09 l2=6.63096e-06 x=4.98899e-05 y=-1.19523e-05 z=-3.31702e-06 kx=0.000428819 ky=-0.000790545 kz=22.4984 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12843e-09 l2=4.49605e-05 x=-4.46616e-05 y=-0.000176965 z=-2.24809e-05 kx=-2.55305e-05 ky=-0.000663442 kz=23.0718 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39256e-09 l2=2.07183e-05 x=-4.89154e-05 y=-0.000351685 z=-1.03594e-05 kx=0.000235163 ky=0.0001197 kz=22.9849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.29527e-09 l2=5.7667e-06 x=-4.99168e-05 y=-7.38927e-05 z=-2.88601e-06 kx=-0.000694606 ky=0.000416101 kz=22.9823 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3151e-09 l2=1.65817e-05 x=4.9308e-05 y=5.21614e-05 z=-8.29121e-06 kx=-0.000137494 ky=3.35312e-05 kz=23.3099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.42349e-09 l2=1.45589e-05 x=-4.94676e-05 y=4.27672e-05 z=-7.27972e-06 kx=0.000432696 ky=0.000524788 kz=22.6756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29265e-09 l2=2.17053e-05 x=-4.88083e-05 y=0.00032407 z=-1.08524e-05 kx=0.000442463 ky=0.000706352 kz=23.1429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60053e-09 l2=3.01932e-05 x=4.7666e-05 y=7.60363e-05 z=-1.50997e-05 kx=0.00110636 ky=-5.04676e-05 kz=23.2094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6577e-09 l2=4.5942e-06 x=-4.99472e-05 y=0.000223674 z=-2.29815e-06 kx=-9.9163e-05 ky=0.000128636 kz=22.4262 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03807e-09 l2=2.55894e-05 x=4.83353e-05 y=0.000370421 z=-1.27954e-05 kx=7.60263e-05 ky=0.000259125 kz=22.9922 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05885e-09 l2=2.10344e-05 x=-4.88818e-05 y=0.000187329 z=-1.05164e-05 kx=0.000640508 ky=0.000278191 kz=22.9372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49287e-09 l2=8.36005e-06 x=4.98249e-05 y=0.000359926 z=-4.1824e-06 kx=0.000757975 ky=0.0011062 kz=23.1641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01479e-09 l2=2.18547e-05 x=-4.87909e-05 y=0.000114238 z=-1.09302e-05 kx=-0.00108531 ky=-0.00080606 kz=22.4228 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32505e-09 l2=8.4929e-06 x=4.98193e-05 y=0.000382613 z=-4.24811e-06 kx=0.000464644 ky=-0.000146521 kz=23.249 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03293e-09 l2=2.46341e-05 x=-4.84589e-05 y=0.000387179 z=-1.2319e-05 kx=-0.000707687 ky=0.000770246 kz=23.2684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44147e-09 l2=1.13649e-05 x=4.96761e-05 y=0.000229869 z=-5.68357e-06 kx=0.000191062 ky=0.00105031 kz=22.4034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10551e-09 l2=7.04723e-06 x=4.98756e-05 y=0.000132627 z=-3.52656e-06 kx=0.00108432 ky=0.00105538 kz=22.6279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18194e-09 l2=2.41605e-05 x=4.85183e-05 y=0.000451573 z=-1.20831e-05 kx=0.00105162 ky=0.00195247 kz=22.7952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22373e-09 l2=2.40317e-05 x=-4.85351e-05 y=0.000321168 z=-1.20158e-05 kx=0.000343819 ky=9.61118e-05 kz=23.1656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91899e-09 l2=1.26305e-05 x=-4.95998e-05 y=6.47028e-05 z=-6.31575e-06 kx=0.000210215 ky=-0.00085082 kz=23.1914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98187e-09 l2=1.99182e-05 x=-4.89978e-05 y=-0.000135631 z=-9.96275e-06 kx=-0.00123777 ky=-0.00120159 kz=22.7441 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14551e-09 l2=2.33386e-05 x=-4.86196e-05 y=0.000245175 z=-1.16688e-05 kx=0.000471934 ky=-0.000360225 kz=22.3611 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.67966e-09 l2=4.17813e-06 x=4.99563e-05 y=-0.000450939 z=-2.09365e-06 kx=0.00102858 ky=-0.000840621 kz=22.8545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16011e-09 l2=1.77715e-05 x=4.92041e-05 y=0.000202019 z=-8.88716e-06 kx=0.00039445 ky=-0.000330938 kz=23.1412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89239e-09 l2=1.34705e-05 x=4.95444e-05 y=-9.46385e-05 z=-6.73607e-06 kx=-5.38593e-05 ky=0.000848251 kz=22.9997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80878e-09 l2=9.21879e-06 x=4.9787e-05 y=-1.38584e-05 z=-4.61175e-06 kx=0.000672562 ky=-0.00023093 kz=23.0792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.55535e-09 l2=7.66581e-06 x=4.98528e-05 y=0.000369982 z=-3.83664e-06 kx=0.00112753 ky=0.0018351 kz=22.8831 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33862e-09 l2=1.0669e-05 x=-4.97144e-05 y=0.000336253 z=-5.33748e-06 kx=-0.001088 ky=0.00117101 kz=23.2241 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02776e-09 l2=9.90705e-06 x=4.9754e-05 y=0.000141509 z=-4.95566e-06 kx=0.000518352 ky=0.00119836 kz=23.0082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.90227e-09 l2=4.66803e-06 x=4.84206e-05 y=-0.000238427 z=-1.24686e-05 kx=4.55622 ky=-1.5037 kz=21.8692 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58465e-09 l2=2.15406e-05 x=4.88269e-05 y=-7.79915e-05 z=-1.0769e-05 kx=-0.000989995 ky=0.000670001 kz=22.8194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30453e-09 l2=7.58266e-06 x=4.98562e-05 y=4.89442e-06 z=-3.79034e-06 kx=-0.000757028 ky=0.000413614 kz=22.9622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33338e-09 l2=1.66797e-05 x=4.92994e-05 y=-0.000395698 z=-8.34234e-06 kx=0.00083656 ky=-0.00135863 kz=22.8524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14657e-09 l2=1.78836e-05 x=-4.91939e-05 y=-0.000477386 z=-8.94312e-06 kx=-0.000355096 ky=-0.00085225 kz=22.8194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0542e-09 l2=2.50119e-05 x=-4.84108e-05 y=0.000240234 z=-1.25068e-05 kx=-0.00016095 ky=-0.000385895 kz=22.4794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86883e-09 l2=1.00684e-05 x=4.97458e-05 y=-0.000120949 z=-5.03738e-06 kx=0.00104722 ky=-0.00139633 kz=22.9922 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43037e-09 l2=2.89278e-05 x=-4.78624e-05 y=-0.00043809 z=-1.44648e-05 kx=-7.34664e-05 ky=-0.00215293 kz=23.2386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05649e-09 l2=1.79325e-05 x=-4.91896e-05 y=-4.10141e-05 z=-8.96646e-06 kx=0.000154859 ky=0.000406982 kz=22.9019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67928e-09 l2=9.59866e-06 x=4.9769e-05 y=5.07717e-05 z=-4.80222e-06 kx=0.000937044 ky=0.00094682 kz=22.7359 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21731e-09 l2=1.55023e-05 x=4.93957e-05 y=-0.000429997 z=-7.75133e-06 kx=-0.00018175 ky=-0.000136576 kz=22.3815 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98684e-09 l2=1.52347e-05 x=4.94161e-05 y=2.97257e-05 z=-7.62103e-06 kx=0.00122736 ky=-0.000862262 kz=22.7017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4113e-09 l2=2.3983e-05 x=4.85409e-05 y=-0.000296717 z=-1.19924e-05 kx=9.67687e-05 ky=-0.000865743 kz=22.85 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27583e-09 l2=1.29952e-05 x=-4.95759e-05 y=-0.000232303 z=-6.50012e-06 kx=-0.00086617 ky=-0.000458612 kz=22.9657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37145e-09 l2=3.17607e-05 x=4.74119e-05 y=-0.000325876 z=-1.58795e-05 kx=-0.000763645 ky=-0.000381106 kz=23.259 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33996e-09 l2=2.46254e-05 x=4.84604e-05 y=-0.00036501 z=-1.23135e-05 kx=6.13051e-05 ky=-0.0013133 kz=22.8225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08338e-09 l2=8.03797e-06 x=-4.98381e-05 y=0.000110501 z=-4.02187e-06 kx=-0.00107225 ky=0.000661333 kz=22.7572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43622e-09 l2=2.13254e-05 x=-4.88505e-05 y=0.000327958 z=-1.06613e-05 kx=0.000991823 ky=-0.000180281 kz=23.0497 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15454e-09 l2=9.80125e-06 x=-4.97591e-05 y=8.38967e-05 z=-4.903e-06 kx=-0.000828737 ky=-0.000140393 kz=22.9703 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.26554e-09 l2=1.11913e-05 x=-4.9686e-05 y=9.93552e-05 z=-5.5971e-06 kx=-0.000135242 ky=2.29044e-05 kz=22.3784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18463e-09 l2=3.54871e-05 x=-4.67467e-05 y=-0.00021144 z=-1.77423e-05 kx=0.000944991 ky=-0.00135858 kz=23.2272 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34706e-09 l2=1.4424e-05 x=4.94772e-05 y=0.000372421 z=-7.21316e-06 kx=0.000229123 ky=0.00158417 kz=22.5663 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92114e-09 l2=1.4829e-05 x=4.94476e-05 y=0.00021666 z=-7.41379e-06 kx=-0.000786344 ky=0.000815999 kz=23.1262 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19023e-09 l2=1.50326e-05 x=-4.94319e-05 y=-0.000354628 z=-7.51668e-06 kx=9.75119e-05 ky=-0.00135627 kz=22.3177 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63086e-09 l2=1.62876e-05 x=-4.93322e-05 y=0.000433071 z=-8.14648e-06 kx=-0.000847687 ky=0.000928492 kz=22.6155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02858e-09 l2=2.76666e-05 x=-4.80489e-05 y=0.000354629 z=-1.38321e-05 kx=0.000806192 ky=0.000296604 kz=23.0982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66576e-09 l2=1.21313e-05 x=4.96308e-05 y=-0.000266568 z=-6.06683e-06 kx=0.00015911 ky=-0.000618162 kz=22.5236 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13488e-09 l2=2.71782e-05 x=4.81181e-05 y=-1.11798e-05 z=-1.35896e-05 kx=-1.83303e-05 ky=-0.000199482 kz=22.64 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2931e-09 l2=6.58487e-06 x=-4.98916e-05 y=8.09709e-05 z=-3.29239e-06 kx=0.000319531 ky=-0.000737217 kz=23.0518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.48842e-09 l2=7.61578e-06 x=4.98549e-05 y=-0.000452644 z=-3.8101e-06 kx=0.000210278 ky=-0.000486022 kz=22.3792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02903e-09 l2=1.77355e-05 x=-4.9207e-05 y=-0.000103511 z=-8.87047e-06 kx=-0.00103092 ky=-0.00114011 kz=22.9074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0763e-09 l2=8.0759e-06 x=4.98368e-05 y=-0.000372845 z=-4.0386e-06 kx=-0.000174375 ky=-0.000865279 kz=22.7164 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13194e-09 l2=2.13708e-05 x=4.88448e-05 y=0.000468479 z=-1.0687e-05 kx=0.000510217 ky=0.000802141 kz=23.2326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.17376e-09 l2=3.28449e-06 x=-4.99731e-05 y=-0.000293476 z=-1.64778e-06 kx=-0.000668776 ky=-0.000100131 kz=23.1129 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44597e-09 l2=2.4113e-05 x=4.85246e-05 y=0.00035106 z=-1.20582e-05 kx=0.000442202 ky=0.00148928 kz=22.3784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.64783e-09 l2=6.75936e-06 x=-4.98857e-05 y=-0.000118643 z=-3.3812e-06 kx=-9.00603e-05 ky=-7.89914e-05 kz=22.7201 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16113e-09 l2=2.82165e-05 x=-4.79685e-05 y=-0.000296328 z=-1.41086e-05 kx=9.51517e-05 ky=-0.00102617 kz=22.8464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68531e-09 l2=1.07497e-05 x=-4.97105e-05 y=-0.000184634 z=-5.37467e-06 kx=0.000491833 ky=-0.000416001 kz=23.2988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19519e-09 l2=2.64589e-05 x=-4.82179e-05 y=-0.000209226 z=-1.32313e-05 kx=-0.00060646 ky=-0.00132059 kz=22.9231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.10702e-09 l2=5.63259e-06 x=4.99208e-05 y=-0.000348409 z=-2.817e-06 kx=-0.000391831 ky=-0.00188705 kz=22.9541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.64073e-09 l2=8.33606e-06 x=4.9826e-05 y=-0.000434968 z=-4.17073e-06 kx=0.000634023 ky=-0.00164811 kz=22.91 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0654e-09 l2=3.21989e-05 x=4.73372e-05 y=0.000270868 z=-1.61004e-05 kx=0.000193327 ky=0.00108329 kz=23.1764 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0954e-09 l2=3.10044e-05 x=-4.75363e-05 y=8.46471e-05 z=-1.55027e-05 kx=-6.35926e-07 ky=-0.000172172 kz=22.3046 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.37495e-09 l2=8.87484e-06 x=4.9803e-05 y=-0.000453691 z=-4.43709e-06 kx=-0.000920942 ky=-0.000619986 kz=22.7116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15776e-09 l2=2.75101e-05 x=4.80713e-05 y=3.66947e-05 z=-1.37544e-05 kx=-0.000567101 ky=-0.000528213 kz=22.3281 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0326e-09 l2=3.01839e-05 x=4.76681e-05 y=-0.000256761 z=-1.50926e-05 kx=5.13494e-05 ky=-0.0011915 kz=22.4732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10046e-09 l2=3.28726e-05 x=-4.72221e-05 y=-0.000407568 z=-1.6435e-05 kx=0.000881305 ky=-0.00100186 kz=22.4046 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.43943e-09 l2=3.15569e-06 x=4.99752e-05 y=-3.94425e-05 z=-1.58267e-06 kx=0.000275574 ky=0.00094099 kz=22.9382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25397e-09 l2=1.72126e-05 x=-4.92534e-05 y=0.000400009 z=-8.60959e-06 kx=-0.00122723 ky=0.00192094 kz=22.5234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23735e-09 l2=1.98234e-05 x=-4.90074e-05 y=-0.000285144 z=-9.91465e-06 kx=-0.00108173 ky=-0.00165116 kz=23.0087 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39529e-09 l2=4.26577e-06 x=-4.99546e-05 y=0.000115817 z=-2.13246e-06 kx=0.000508415 ky=0.000112854 kz=22.5095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.57129e-09 l2=1.019e-05 x=4.97401e-05 y=-0.000360627 z=-5.0942e-06 kx=-0.000950569 ky=-0.00168323 kz=22.5925 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95074e-09 l2=1.85047e-05 x=-4.91363e-05 y=-0.000204447 z=-9.25524e-06 kx=-0.000875894 ky=0.000554863 kz=22.4668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08503e-09 l2=2.42159e-05 x=-4.85118e-05 y=0.000400949 z=-1.21092e-05 kx=-0.000329647 ky=0.00132337 kz=22.6262 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28195e-09 l2=2.19359e-05 x=-4.87824e-05 y=-0.000377502 z=-1.09684e-05 kx=9.689e-05 ky=-0.000845921 kz=23.2223 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07154e-09 l2=1.26398e-05 x=4.95991e-05 y=0.00037063 z=-6.32e-06 kx=-0.00020852 ky=0.00162751 kz=22.5423 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63652e-09 l2=2.00108e-05 x=4.89888e-05 y=0.000402315 z=-1.00067e-05 kx=0.000229875 ky=0.00125318 kz=22.697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.18075e-09 l2=7.01097e-06 x=-4.98771e-05 y=-9.69291e-05 z=-3.5064e-06 kx=0.000307105 ky=0.00058601 kz=22.7642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11069e-09 l2=1.25657e-05 x=4.96041e-05 y=-0.000487334 z=-6.28201e-06 kx=-0.000887591 ky=-0.0021427 kz=23.1081 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.59173e-09 l2=1.17089e-05 x=-4.96563e-05 y=-0.000210586 z=-5.85468e-06 kx=0.000468851 ky=0.000143896 kz=22.3732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28092e-09 l2=1.1784e-05 x=-4.96517e-05 y=-0.000400174 z=-5.89234e-06 kx=0.000149882 ky=-0.000244521 kz=23.052 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17086e-09 l2=1.04094e-05 x=4.97283e-05 y=-2.22622e-05 z=-5.20682e-06 kx=0.000694088 ky=-0.000136732 kz=22.5106 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05341e-09 l2=1.03835e-05 x=-4.97297e-05 y=-2.2059e-05 z=-5.19325e-06 kx=-0.000452947 ky=0.000176608 kz=23.198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81761e-09 l2=1.24185e-05 x=-4.96132e-05 y=0.000262 z=-6.20943e-06 kx=0.000334007 ky=0.000530318 kz=23.2044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34165e-09 l2=1.28257e-05 x=-4.95869e-05 y=-0.000132274 z=-6.41621e-06 kx=-0.00102431 ky=-0.000211567 kz=23.2217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09709e-09 l2=2.4634e-05 x=4.84594e-05 y=-0.000388982 z=-1.23172e-05 kx=-0.000135371 ky=-0.000721378 kz=23.103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.27875e-09 l2=1.1807e-05 x=4.96505e-05 y=0.000181096 z=-5.90462e-06 kx=-0.000245499 ky=0.000879239 kz=23.2109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.87555e-09 l2=3.77023e-06 x=4.99647e-05 y=-0.000103035 z=-1.88762e-06 kx=-0.000642803 ky=-0.00011679 kz=22.4414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05997e-09 l2=1.1281e-05 x=-4.96809e-05 y=-0.000178706 z=-5.64104e-06 kx=-1.14101e-05 ky=-0.00124023 kz=22.9773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02861e-09 l2=3.02322e-05 x=-4.76609e-05 y=0.000302946 z=-1.51152e-05 kx=0.000667146 ky=0.000404117 kz=22.9709 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.21502e-09 l2=6.22905e-06 x=-4.9903e-05 y=-0.000149348 z=-3.11569e-06 kx=-2.5512e-05 ky=-0.000453934 kz=22.6757 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12523e-09 l2=2.45587e-05 x=-4.84684e-05 y=0.000430308 z=-1.22818e-05 kx=-0.000895628 ky=0.00104574 kz=23.0705 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13662e-09 l2=9.40908e-06 x=-4.97783e-05 y=0.000474774 z=-4.70476e-06 kx=0.000159787 ky=0.00101798 kz=22.5996 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82685e-09 l2=1.1412e-05 x=-4.96736e-05 y=0.000364664 z=-5.70599e-06 kx=0.000422044 ky=0.00188871 kz=22.5342 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6502e-09 l2=1.92705e-05 x=-4.90626e-05 y=-0.000128192 z=-9.63799e-06 kx=-0.000878204 ky=0.000242226 kz=22.5024 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.16355e-09 l2=9.73709e-06 x=-4.97627e-05 y=0.000151086 z=-4.86858e-06 kx=0.000701233 ky=0.000156998 kz=22.6138 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98038e-09 l2=8.17928e-06 x=-4.98327e-05 y=-0.000497136 z=-4.08934e-06 kx=0.000824838 ky=-0.00035382 kz=22.8683 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51367e-09 l2=1.77372e-05 x=4.92073e-05 y=-0.000399581 z=-8.86955e-06 kx=9.91829e-05 ky=-0.00173941 kz=23.2373 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58463e-09 l2=2.6874e-05 x=4.81602e-05 y=0.000257067 z=-1.34401e-05 kx=0.00110613 ky=0.00147347 kz=22.8817 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05202e-09 l2=6.18891e-06 x=-4.99043e-05 y=0.000142308 z=-3.09424e-06 kx=0.000579123 ky=0.00106571 kz=23.2845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17312e-09 l2=6.06194e-06 x=-4.9908e-05 y=-3.09639e-05 z=-3.0331e-06 kx=-0.000692519 ky=0.00095585 kz=22.3863 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14171e-09 l2=1.27654e-05 x=4.95912e-05 y=0.000391861 z=-6.38255e-06 kx=-0.000569765 ky=0.000441232 kz=22.9108 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91323e-09 l2=4.78146e-06 x=4.99429e-05 y=0.000485802 z=-2.3903e-06 kx=-0.000636051 ky=0.00167769 kz=22.8645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46243e-09 l2=6.09031e-06 x=4.99071e-05 y=0.000326676 z=-3.04889e-06 kx=0.00114848 ky=0.00176294 kz=22.902 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11611e-09 l2=5.3582e-06 x=-4.99283e-05 y=-0.000427795 z=-2.67865e-06 kx=0.000678331 ky=-0.000934 kz=22.482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.53028e-09 l2=3.84441e-06 x=4.9963e-05 y=8.88634e-05 z=-1.9263e-06 kx=0.00105043 ky=0.000769656 kz=22.5194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0104e-09 l2=1.1574e-05 x=-4.96641e-05 y=0.000282287 z=-5.78757e-06 kx=0.00019303 ky=-0.000355979 kz=23.1943 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77693e-09 l2=7.00608e-06 x=-4.98772e-05 y=0.000257383 z=-3.5034e-06 kx=0.000235739 ky=-0.000303086 kz=22.4572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.49293e-09 l2=4.87635e-06 x=4.99407e-05 y=0.00034055 z=-2.4393e-06 kx=-0.00051225 ky=-0.00025246 kz=22.8399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35723e-09 l2=1.60395e-05 x=4.93524e-05 y=0.000216539 z=-8.02268e-06 kx=0.0010178 ky=0.000468129 kz=22.5582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71406e-09 l2=3.50125e-06 x=-4.99694e-05 y=-0.000405542 z=-1.75116e-06 kx=0.000147867 ky=-0.00148947 kz=22.9465 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23314e-09 l2=2.7274e-05 x=-4.81041e-05 y=2.12404e-05 z=-1.36394e-05 kx=-0.000826293 ky=0.000631257 kz=22.3118 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02696e-09 l2=3.01784e-05 x=4.76695e-05 y=-0.000373616 z=-1.50882e-05 kx=-0.00074337 ky=-0.000704482 kz=23.0209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39885e-08 l2=2.11062e-07 x=4.99999e-05 y=-0.000370465 z=-1.17923e-07 kx=0.000182695 ky=-0.00101759 kz=22.9516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3139e-09 l2=9.22536e-06 x=4.9787e-05 y=-5.41268e-05 z=-4.61281e-06 kx=-0.000477499 ky=-0.00106389 kz=23.1871 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22934e-09 l2=1.05243e-05 x=4.97222e-05 y=-0.000442059 z=-5.26481e-06 kx=0.000942539 ky=-0.000197386 kz=22.7145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43417e-09 l2=2.34197e-05 x=-4.86096e-05 y=-1.66539e-05 z=-1.17107e-05 kx=-7.29719e-05 ky=0.00101985 kz=22.5568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0614e-09 l2=9.20744e-06 x=-4.97875e-05 y=0.000351181 z=-4.6063e-06 kx=-0.000934079 ky=0.00086871 kz=22.6444 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04325e-09 l2=2.73609e-05 x=-4.80921e-05 y=-0.000195999 z=-1.36814e-05 kx=-0.00018822 ky=-0.00147534 kz=23.2118 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12955e-09 l2=2.15964e-05 x=4.88203e-05 y=-0.000138398 z=-1.07983e-05 kx=-0.000214911 ky=0.000549779 kz=23.2209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09111e-09 l2=7.0595e-06 x=-4.98754e-05 y=-0.000176917 z=-3.52856e-06 kx=0.000795764 ky=-0.000643806 kz=22.82 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25268e-09 l2=1.2396e-05 x=4.96146e-05 y=-0.000499153 z=-6.19695e-06 kx=-0.000761353 ky=-0.000448764 kz=22.6702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44875e-09 l2=1.75543e-05 x=4.92239e-05 y=0.000473698 z=-8.77711e-06 kx=-0.00036126 ky=0.00104155 kz=23.086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10004e-09 l2=9.92942e-06 x=-4.97528e-05 y=-4.87091e-05 z=-4.96663e-06 kx=-0.000630631 ky=0.000975878 kz=22.9521 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20023e-09 l2=1.68718e-05 x=4.92831e-05 y=-0.000402195 z=-8.43784e-06 kx=0.00061232 ky=-0.0019922 kz=22.6173 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16287e-09 l2=2.56888e-05 x=-4.83227e-05 y=0.000401776 z=-1.2843e-05 kx=0.000923775 ky=-0.000191598 kz=22.9281 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23083e-09 l2=2.64394e-05 x=4.8221e-05 y=-6.63428e-05 z=-1.32198e-05 kx=-0.000214971 ky=0.000164561 kz=23.1235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47567e-09 l2=1.01637e-05 x=4.97413e-05 y=-6.93846e-06 z=-5.08237e-06 kx=-0.000341567 ky=0.000694325 kz=23.0211 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13322e-09 l2=3.39941e-05 x=-4.70222e-05 y=0.00037233 z=-1.69985e-05 kx=-0.000425851 ky=0.000172101 kz=23.0885 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28611e-09 l2=1.45517e-05 x=-4.94676e-05 y=-2.89408e-05 z=-7.27854e-06 kx=-0.000966713 ky=-0.000932999 kz=23.2569 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08966e-09 l2=1.21872e-05 x=4.96274e-05 y=0.000225813 z=-6.09376e-06 kx=-0.000181869 ky=0.000439026 kz=23.1944 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7193e-09 l2=3.56652e-06 x=4.99682e-05 y=-0.000442721 z=-1.78517e-06 kx=0.000479976 ky=-0.000458553 kz=22.929 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4064e-09 l2=1.60711e-05 x=4.935e-05 y=-0.00037408 z=-8.03743e-06 kx=0.000547839 ky=-0.00170678 kz=23.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13323e-09 l2=1.7847e-05 x=-4.9197e-05 y=-0.000395645 z=-8.92597e-06 kx=-0.00087803 ky=-0.00121952 kz=22.5828 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.14932e-09 l2=6.4403e-06 x=-4.98963e-05 y=0.000165569 z=-3.22178e-06 kx=-2.59912e-05 ky=0.00113641 kz=23.2479 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18521e-09 l2=3.26122e-05 x=4.72664e-05 y=-0.000209976 z=-1.63073e-05 kx=0.000304744 ky=-0.000397065 kz=22.9923 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.27413e-09 l2=1.03778e-05 x=4.97303e-05 y=0.000302484 z=-5.18974e-06 kx=-0.000362006 ky=-0.000215856 kz=22.8185 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82161e-09 l2=5.72471e-06 x=-4.99181e-05 y=-6.28329e-05 z=-2.86209e-06 kx=0.000541228 ky=1.02501e-05 kz=22.9796 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37439e-09 l2=1.25699e-05 x=-4.96033e-05 y=0.000200999 z=-6.28745e-06 kx=-0.000855724 ky=0.000890599 kz=23.1178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1567e-09 l2=2.16248e-05 x=4.88173e-05 y=-0.000175448 z=-1.08116e-05 kx=-0.00062425 ky=-0.000430227 kz=22.5371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25829e-09 l2=1.06824e-05 x=-4.9714e-05 y=0.000244481 z=-5.3416e-06 kx=0.000110463 ky=0.00145114 kz=23.2774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35829e-09 l2=1.3312e-05 x=4.95553e-05 y=-0.000184639 z=-6.65575e-06 kx=-0.000643803 ky=-0.000138997 kz=22.5125 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63235e-09 l2=2.00217e-05 x=-4.89874e-05 y=0.000495895 z=-1.00135e-05 kx=-0.000886782 ky=0.000522015 kz=23.0827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2191e-09 l2=3.55309e-05 x=4.67373e-05 y=-0.00021573 z=-1.7767e-05 kx=0.000454483 ky=-0.00148105 kz=22.8274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93455e-09 l2=1.56612e-05 x=-4.93828e-05 y=0.000314136 z=-7.83371e-06 kx=-0.000987613 ky=0.000798756 kz=22.6013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.65311e-09 l2=1.16981e-05 x=4.96568e-05 y=0.000155075 z=-5.85133e-06 kx=0.000438272 ky=0.000330554 kz=22.7235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.92216e-09 l2=9.3815e-06 x=4.97798e-05 y=4.45981e-05 z=-4.69355e-06 kx=-7.63352e-05 ky=-0.000867835 kz=22.7418 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55028e-09 l2=1.96131e-05 x=-4.90289e-05 y=-0.000434411 z=-9.80799e-06 kx=-0.000306996 ky=-0.0003344 kz=22.3189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72808e-09 l2=7.63567e-06 x=-4.98542e-05 y=4.1925e-06 z=-3.81726e-06 kx=0.000660056 ky=-0.000597709 kz=22.8452 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02112e-09 l2=1.43393e-05 x=4.94832e-05 y=-0.000261883 z=-7.17152e-06 kx=0.000612047 ky=0.000331376 kz=22.3545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05769e-09 l2=2.69022e-05 x=-4.81563e-05 y=-0.000412082 z=-1.34536e-05 kx=-0.000961876 ky=-0.00118088 kz=23.0186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.081e-09 l2=2.966e-05 x=-4.77505e-05 y=-0.000133102 z=-1.48298e-05 kx=0.000350838 ky=-0.00135423 kz=23.0595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.52941e-09 l2=8.46025e-06 x=4.98209e-05 y=7.95381e-05 z=-4.23088e-06 kx=-0.000233272 ky=0.0011131 kz=22.8426 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75084e-09 l2=1.35628e-05 x=4.95379e-05 y=-0.000336479 z=-6.78356e-06 kx=0.000584706 ky=-0.00152822 kz=22.3252 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27748e-09 l2=1.90937e-05 x=4.90805e-05 y=-0.000487298 z=-9.54606e-06 kx=-0.0006718 ky=-0.000375143 kz=22.9019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75316e-09 l2=9.53146e-06 x=4.97726e-05 y=0.00047137 z=-4.76509e-06 kx=-0.000698203 ky=0.000494029 kz=22.875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.68086e-09 l2=9.78529e-06 x=4.976e-05 y=0.000233784 z=-4.89555e-06 kx=0.000714017 ky=0.000150026 kz=22.7519 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7023e-09 l2=1.97575e-05 x=4.90144e-05 y=0.000258305 z=-9.8805e-06 kx=0.000423046 ky=0.000914695 kz=22.4763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4937e-09 l2=1.99631e-05 x=-4.89938e-05 y=-0.000156156 z=-9.98182e-06 kx=0.000215781 ky=-0.00111697 kz=23.2231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01108e-09 l2=2.75206e-05 x=-4.80688e-05 y=0.000222842 z=-1.37631e-05 kx=-0.00103982 ky=0.000440363 kz=22.439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27308e-09 l2=1.15352e-05 x=-4.96662e-05 y=4.39027e-05 z=-5.76877e-06 kx=-0.000256435 ky=0.000334706 kz=22.8757 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.7417e-09 l2=6.54938e-06 x=-4.98927e-05 y=-0.00036997 z=-3.27954e-06 kx=-0.000923921 ky=-0.000729865 kz=23.234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37869e-09 l2=3.1281e-05 x=-4.74903e-05 y=-0.000269241 z=-1.56433e-05 kx=-0.00104684 ky=-0.00177392 kz=23.2948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12598e-09 l2=1.63457e-05 x=4.93276e-05 y=-0.000407501 z=-8.17334e-06 kx=-3.36222e-05 ky=0.00010123 kz=22.793 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95563e-09 l2=4.19166e-06 x=4.99561e-05 y=-0.000307486 z=-2.09668e-06 kx=-5.67956e-05 ky=-0.00159134 kz=22.6134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11522e-09 l2=2.76543e-05 x=4.80498e-05 y=8.56927e-05 z=-1.38291e-05 kx=0.000664432 ky=0.00017051 kz=22.6946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54034e-09 l2=1.53808e-05 x=4.94048e-05 y=0.000331034 z=-7.69362e-06 kx=0.00111071 ky=0.000322862 kz=22.5795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52384e-09 l2=1.17416e-05 x=4.96541e-05 y=0.000482051 z=-5.87272e-06 kx=0.000539506 ky=0.000421228 kz=23.0205 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.4672e-09 l2=5.46249e-06 x=4.99253e-05 y=4.99368e-05 z=-2.73486e-06 kx=0.000845837 ky=0.00105073 kz=22.4199 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.26407e-09 l2=5.20458e-06 x=4.99323e-05 y=7.18154e-05 z=-2.60386e-06 kx=0.00019562 ky=-0.000575835 kz=22.4859 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34682e-09 l2=1.18092e-05 x=-4.96504e-05 y=-0.000289664 z=-5.90386e-06 kx=0.000632749 ky=0.000361655 kz=22.5956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.27861e-09 l2=5.0176e-06 x=4.99371e-05 y=0.000102947 z=-2.51091e-06 kx=0.000215219 ky=0.000308181 kz=22.9193 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87028e-09 l2=1.31575e-05 x=4.95657e-05 y=-0.000291058 z=-6.57798e-06 kx=-0.000788424 ky=-0.000770062 kz=22.5998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3009e-09 l2=8.32468e-06 x=4.98265e-05 y=0.000232933 z=-4.16447e-06 kx=0.000440714 ky=0.000903638 kz=22.3773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01827e-09 l2=2.91635e-05 x=4.78262e-05 y=0.000251153 z=-1.45836e-05 kx=0.000627067 ky=0.000127433 kz=22.6014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53213e-09 l2=1.97019e-05 x=-4.90204e-05 y=-0.000155768 z=-9.85052e-06 kx=0.000542554 ky=-0.000972199 kz=22.3411 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00102e-09 l2=1.44347e-05 x=4.94765e-05 y=-0.000138455 z=-7.2171e-06 kx=-0.000361372 ky=-9.81174e-05 kz=23.1127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14857e-09 l2=2.83395e-05 x=4.79502e-05 y=-0.000448001 z=-1.41709e-05 kx=0.000271265 ky=-0.000274713 kz=22.6715 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.32685e-09 l2=8.09536e-06 x=4.98361e-05 y=-7.1773e-05 z=-4.04856e-06 kx=-0.00036402 ky=-0.000584869 kz=23.0466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41594e-09 l2=1.54143e-05 x=-4.94026e-05 y=0.000453337 z=-7.70714e-06 kx=0.000335058 ky=0.000580415 kz=22.3697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44415e-09 l2=3.0836e-05 x=-4.75634e-05 y=-0.000325063 z=-1.54198e-05 kx=-0.000519951 ky=-8.2808e-05 kz=22.7803 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1397e-09 l2=2.37281e-05 x=-4.85722e-05 y=-0.000153378 z=-1.18646e-05 kx=1.1088e-05 ky=-0.00146645 kz=22.9869 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59591e-09 l2=2.44246e-05 x=-4.84857e-05 y=0.000219063 z=-1.22138e-05 kx=-0.000338931 ky=-0.00061947 kz=23.3027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.99593e-09 l2=1.42615e-05 x=-4.94891e-05 y=-0.000132188 z=-7.13171e-06 kx=1.55109e-05 ky=-0.00125865 kz=22.567 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07566e-09 l2=2.5322e-05 x=4.8371e-05 y=0.00044071 z=-1.26598e-05 kx=-0.000790122 ky=0.00016871 kz=22.3995 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55797e-09 l2=1.12348e-05 x=-4.96834e-05 y=0.000462416 z=-5.61941e-06 kx=-0.00056695 ky=-2.92146e-05 kz=23.1156 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04251e-09 l2=1.13689e-05 x=-4.96757e-05 y=3.42665e-05 z=-5.68795e-06 kx=-0.00115512 ky=0.00018797 kz=23.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16595e-09 l2=9.12279e-06 x=4.97916e-05 y=0.000261691 z=-4.56133e-06 kx=-0.000299909 ky=0.00164944 kz=23.0977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76836e-09 l2=2.00752e-05 x=4.89825e-05 y=-0.000206995 z=-1.00373e-05 kx=-0.000579475 ky=-0.00138037 kz=23.1773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6206e-09 l2=2.03667e-05 x=-4.89519e-05 y=8.67438e-05 z=-1.01855e-05 kx=-0.000633542 ky=0.00106923 kz=23.1765 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63188e-09 l2=2.72036e-05 x=-4.81148e-05 y=0.000299999 z=-1.36019e-05 kx=0.000318128 ky=-0.000201732 kz=23.1434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36415e-09 l2=1.29759e-05 x=-4.95775e-05 y=0.000436445 z=-6.48745e-06 kx=0.000538694 ky=0.00149809 kz=22.7998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93763e-09 l2=6.77536e-06 x=4.98852e-05 y=-0.000353453 z=-3.38784e-06 kx=-0.000374127 ky=-0.0017877 kz=23.0843 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30679e-09 l2=2.70379e-05 x=4.81377e-05 y=0.000164123 z=-1.35203e-05 kx=0.000354154 ky=0.000876057 kz=23.2966 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42526e-09 l2=8.05124e-06 x=4.98377e-05 y=-8.07905e-05 z=-4.02706e-06 kx=0.000332519 ky=0.000745295 kz=22.7681 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60805e-09 l2=1.21374e-05 x=4.96302e-05 y=-0.000190939 z=-6.07164e-06 kx=0.0009926 ky=-0.000648408 kz=23.1609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71566e-09 l2=1.88619e-05 x=4.91028e-05 y=0.000349247 z=-9.43129e-06 kx=-0.000251169 ky=-1.22991e-05 kz=23.1333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44112e-09 l2=1.91572e-05 x=4.90745e-05 y=0.000143711 z=-9.57735e-06 kx=-0.000900004 ky=-0.000544416 kz=22.6287 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30674e-08 l2=1.40453e-06 x=4.99952e-05 y=0.000249866 z=-7.13958e-07 kx=7.12964e-05 ky=0.0010345 kz=22.6735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.88042e-09 l2=4.89607e-06 x=-4.99402e-05 y=0.000375769 z=-2.44964e-06 kx=0.000606889 ky=0.00129112 kz=22.7682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16296e-09 l2=1.77207e-05 x=-4.9209e-05 y=-6.33525e-05 z=-8.8609e-06 kx=0.000243653 ky=-0.000277796 kz=22.9977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12577e-09 l2=3.77516e-05 x=-4.62996e-05 y=-0.000353176 z=-1.88784e-05 kx=-0.000996826 ky=-0.00153234 kz=23.0137 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23935e-09 l2=8.42895e-06 x=4.98221e-05 y=-6.16337e-05 z=-4.21687e-06 kx=0.00059375 ky=0.000342297 kz=23.2121 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.981e-09 l2=1.13133e-05 x=4.96791e-05 y=-0.000321004 z=-5.65786e-06 kx=9.28073e-05 ky=-0.00177972 kz=22.3625 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02974e-09 l2=3.01761e-05 x=4.76687e-05 y=-0.000281079 z=-1.50906e-05 kx=0.00095394 ky=-0.000418787 kz=23.1437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.55155e-09 l2=9.65993e-06 x=-4.97662e-05 y=-0.000292724 z=-4.83343e-06 kx=-0.000786133 ky=-0.00020437 kz=23.1866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0297e-09 l2=1.38313e-05 x=-4.95195e-05 y=0.00036313 z=-6.91588e-06 kx=0.000123987 ky=0.00192111 kz=22.6309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44818e-09 l2=1.55024e-05 x=-4.93958e-05 y=0.00038455 z=-7.75122e-06 kx=0.000323644 ky=0.00153365 kz=22.3186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22004e-09 l2=3.12264e-05 x=-4.75006e-05 y=0.000472776 z=-1.5612e-05 kx=0.000870303 ky=1.28353e-05 kz=22.9116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0286e-09 l2=1.88095e-05 x=4.91072e-05 y=-0.000279342 z=-9.40762e-06 kx=0.00107551 ky=-0.0015579 kz=22.3591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02296e-09 l2=3.20971e-05 x=4.73544e-05 y=-0.000458483 z=-1.60497e-05 kx=0.000295292 ky=-0.000839024 kz=22.9016 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09315e-09 l2=9.02893e-06 x=4.97956e-05 y=0.000163632 z=-4.51707e-06 kx=0.000944737 ky=-0.000559277 kz=22.8043 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.60987e-09 l2=1.25675e-05 x=4.96035e-05 y=-0.000356538 z=-6.28667e-06 kx=0.00074334 ky=-0.000376621 kz=22.4817 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1611e-09 l2=7.58165e-06 x=-4.98563e-05 y=-8.6553e-06 z=-3.78986e-06 kx=0.000692958 ky=0.000252887 kz=22.4079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19554e-09 l2=1.84459e-05 x=4.91419e-05 y=-0.000353906 z=-9.22486e-06 kx=0.000606598 ky=-0.00183292 kz=22.5659 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07581e-09 l2=1.28502e-05 x=-4.95857e-05 y=-0.000457078 z=-6.42453e-06 kx=0.000529198 ky=-0.000856522 kz=23.1948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81669e-09 l2=1.06586e-05 x=-4.97153e-05 y=0.000271709 z=-5.33039e-06 kx=-8.05321e-05 ky=0.00149035 kz=22.9407 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47914e-09 l2=1.4705e-05 x=4.94565e-05 y=-0.000147434 z=-7.35446e-06 kx=0.000317802 ky=-0.000634257 kz=22.5965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.313e-09 l2=2.70446e-05 x=4.81375e-05 y=0.000198198 z=-1.35209e-05 kx=-0.000990168 ky=0.000169146 kz=23.1658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08321e-09 l2=1.37046e-05 x=-4.95282e-05 y=1.24834e-05 z=-6.85354e-06 kx=-0.000318995 ky=0.00100625 kz=22.5602 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01839e-09 l2=1.68737e-05 x=-4.9283e-05 y=-0.00018515 z=-8.43803e-06 kx=-0.000302372 ky=0.000332629 kz=22.889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26306e-09 l2=1.86043e-05 x=-4.91273e-05 y=0.000333903 z=-9.30202e-06 kx=0.000352772 ky=0.000837814 kz=22.304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24931e-09 l2=3.56791e-06 x=-4.99681e-05 y=-9.22094e-05 z=-1.78568e-06 kx=-0.000497435 ky=0.000151475 kz=22.6726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36099e-08 l2=1.16527e-06 x=4.99967e-05 y=0.000318059 z=-5.89419e-07 kx=-1.00665e-05 ky=0.000222011 kz=22.881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27854e-09 l2=9.53326e-06 x=4.97724e-05 y=-0.000203506 z=-4.76625e-06 kx=-0.000462411 ky=-0.000219897 kz=22.7315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02897e-09 l2=1.80204e-05 x=-4.9182e-05 y=0.000448509 z=-9.00913e-06 kx=0.000985481 ky=0.00167905 kz=23.1421 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45932e-09 l2=1.79119e-05 x=4.91914e-05 y=0.000255721 z=-8.95719e-06 kx=0.000244179 ky=0.00144173 kz=22.7511 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75865e-09 l2=1.28382e-05 x=-4.95865e-05 y=-0.000151767 z=-6.41877e-06 kx=0.000555886 ky=-0.00105341 kz=23.0552 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41891e-09 l2=2.80618e-05 x=-4.79908e-05 y=-0.000288136 z=-1.40329e-05 kx=-0.00063602 ky=0.000116001 kz=22.8682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74094e-09 l2=1.51846e-05 x=4.94205e-05 y=0.000109308 z=-7.59185e-06 kx=-0.00061185 ky=0.00106354 kz=23.0195 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01066e-09 l2=3.96525e-05 x=4.59022e-05 y=-0.000482817 z=-1.9825e-05 kx=-0.000885018 ky=-0.00207038 kz=23.097 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08371e-09 l2=1.2362e-05 x=4.96167e-05 y=8.33991e-05 z=-6.18049e-06 kx=-0.000471443 ky=-0.000496625 kz=22.4844 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35074e-09 l2=1.82313e-05 x=-4.91624e-05 y=0.000242979 z=-9.11515e-06 kx=0.000531436 ky=0.00125336 kz=22.5263 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60229e-09 l2=2.14895e-05 x=-4.88321e-05 y=0.000494072 z=-1.07451e-05 kx=0.000232762 ky=0.000711609 kz=23.0642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45113e-09 l2=1.22406e-05 x=-4.96241e-05 y=-0.00046089 z=-6.12131e-06 kx=-0.000127361 ky=-0.00128046 kz=22.7366 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01935e-08 l2=2.173e-06 x=-4.99883e-05 y=0.000281683 z=-1.09301e-06 kx=-0.00064397 ky=-0.000302769 kz=22.782 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13744e-09 l2=4.6444e-05 x=-4.42793e-05 y=6.75453e-05 z=-2.32248e-05 kx=-0.001167 ky=0.000749017 kz=22.8759 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03059e-09 l2=2.37187e-05 x=4.8573e-05 y=0.000168494 z=-1.1861e-05 kx=0.000546292 ky=0.000394232 kz=22.9184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48193e-09 l2=2.08249e-05 x=4.89035e-05 y=-0.000119957 z=-1.04151e-05 kx=0.000887727 ky=-0.0011423 kz=22.5318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09902e-09 l2=6.24752e-06 x=4.99023e-05 y=-1.89236e-05 z=-3.12534e-06 kx=0.000466902 ky=-0.000156211 kz=22.7114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04957e-09 l2=2.00458e-05 x=-4.89853e-05 y=-6.47381e-05 z=-1.0023e-05 kx=0.000178305 ky=0.000123821 kz=22.7266 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42345e-09 l2=4.54166e-06 x=-4.99485e-05 y=0.000179971 z=-2.26954e-06 kx=0.000906383 ky=0.000704675 kz=22.6556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92927e-09 l2=8.34765e-06 x=-4.98255e-05 y=0.000473399 z=-4.17512e-06 kx=-0.0001535 ky=0.000433001 kz=23.1793 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09043e-09 l2=3.11996e-05 x=-4.75038e-05 y=-0.000248698 z=-1.56021e-05 kx=-0.00086103 ky=-0.00150295 kz=23.3071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4209e-09 l2=1.90669e-06 x=-4.99909e-05 y=-0.000384797 z=-9.538e-07 kx=0.000114967 ky=-0.000568525 kz=22.6184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88959e-09 l2=1.03698e-05 x=4.97307e-05 y=0.000152551 z=-5.18429e-06 kx=-0.00069925 ky=0.00104571 kz=22.493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.33565e-09 l2=4.66524e-06 x=-4.99455e-05 y=0.000169742 z=-2.33621e-06 kx=-0.000884267 ky=0.000292208 kz=22.908 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54719e-09 l2=2.00571e-05 x=-4.89845e-05 y=-0.000268955 z=-1.00272e-05 kx=0.000964283 ky=-0.000478092 kz=22.7053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45134e-09 l2=1.15244e-05 x=4.96669e-05 y=-0.0001709 z=-5.76301e-06 kx=2.90388e-05 ky=0.0002286 kz=22.6948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7019e-09 l2=1.68326e-05 x=4.92868e-05 y=-0.000435639 z=-8.41647e-06 kx=-0.00031982 ky=-0.00165009 kz=22.5079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41845e-09 l2=2.8962e-05 x=-4.78569e-05 y=-0.000467803 z=-1.44829e-05 kx=-0.000559291 ky=-0.00152296 kz=23.0664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21565e-09 l2=2.60241e-05 x=-4.82772e-05 y=0.000481198 z=-1.30132e-05 kx=-0.000276186 ky=0.000225516 kz=22.6336 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53648e-09 l2=7.46692e-06 x=4.98603e-05 y=-0.000391832 z=-3.7365e-06 kx=0.00103477 ky=-0.00024726 kz=22.6475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13928e-09 l2=2.47143e-05 x=4.84491e-05 y=-0.000122922 z=-1.23576e-05 kx=-5.53189e-05 ky=0.00052329 kz=22.5776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4067e-09 l2=9.82974e-06 x=-4.97578e-05 y=-0.000376187 z=-4.91744e-06 kx=-0.000625035 ky=-0.00109875 kz=22.8284 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52281e-09 l2=1.48854e-05 x=-4.9443e-05 y=0.000412407 z=-7.44424e-06 kx=-0.00036396 ky=0.00192784 kz=22.8447 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17692e-09 l2=2.93705e-05 x=4.77948e-05 y=0.000207072 z=-1.46864e-05 kx=0.000272184 ky=-0.000222205 kz=23.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.61364e-09 l2=7.18382e-06 x=-4.98711e-05 y=-0.000460127 z=-3.59114e-06 kx=0.000945302 ky=-0.00117162 kz=22.6455 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95486e-09 l2=1.21025e-05 x=4.96324e-05 y=0.000297213 z=-6.0541e-06 kx=0.00085159 ky=-0.00045317 kz=22.7693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81793e-09 l2=8.92199e-06 x=-4.98006e-05 y=-2.55124e-05 z=-4.4623e-06 kx=-0.000178673 ky=-0.000361318 kz=22.5064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10997e-09 l2=1.07941e-05 x=4.97077e-05 y=-0.000448156 z=-5.39934e-06 kx=0.000791792 ky=-0.000153916 kz=22.7313 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08917e-09 l2=2.39468e-05 x=4.85457e-05 y=0.000471852 z=-1.19723e-05 kx=-0.000755739 ky=0.000470194 kz=22.311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66333e-09 l2=1.23898e-05 x=-4.96149e-05 y=-0.000402092 z=-6.19523e-06 kx=0.000224811 ky=-0.000702579 kz=23.062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22741e-09 l2=7.70935e-06 x=4.98513e-05 y=0.000483196 z=-3.85399e-06 kx=-0.000590721 ky=0.00204745 kz=22.7471 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.25955e-09 l2=4.42719e-06 x=-4.99512e-05 y=0.000387355 z=-2.21451e-06 kx=0.000793587 ky=0.00130242 kz=23.1572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97233e-09 l2=9.35726e-06 x=-4.97806e-05 y=7.70929e-05 z=-4.68073e-06 kx=-0.000516061 ky=0.000908099 kz=23.035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37965e-09 l2=7.77327e-06 x=4.98489e-05 y=-2.08485e-05 z=-3.88511e-06 kx=-0.00102055 ky=-0.000239963 kz=23.0244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.4508e-09 l2=8.93436e-06 x=-4.98003e-05 y=-2.94842e-05 z=-4.46753e-06 kx=0.000643008 ky=-0.000466476 kz=23.2755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08206e-09 l2=2.25108e-05 x=-4.87166e-05 y=0.000134578 z=-1.12567e-05 kx=-0.000383299 ky=0.000590633 kz=23.114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.77951e-09 l2=5.9317e-06 x=4.99119e-05 y=-0.00013817 z=-2.96984e-06 kx=0.00117518 ky=-0.000132394 kz=22.5256 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66069e-09 l2=8.36494e-06 x=4.98247e-05 y=-0.000170873 z=-4.18513e-06 kx=0.000829393 ky=-0.000707551 kz=22.5865 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47275e-09 l2=1.2827e-05 x=-4.95873e-05 y=-7.14157e-05 z=-6.41372e-06 kx=0.000468595 ky=0.000219568 kz=22.7109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11909e-09 l2=2.79238e-05 x=4.80105e-05 y=0.000487704 z=-1.3965e-05 kx=0.00122299 ky=0.000655151 kz=23.0779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.76778e-09 l2=9.3428e-06 x=4.97814e-05 y=-0.000499262 z=-4.67306e-06 kx=0.000125288 ky=-0.00223962 kz=23.0035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5238e-09 l2=4.88725e-06 x=4.99404e-05 y=-0.000396381 z=-2.44319e-06 kx=-0.0009877 ky=-0.00145993 kz=22.4439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.99369e-09 l2=5.63967e-06 x=4.99206e-05 y=0.00031852 z=-2.81909e-06 kx=-0.00103652 ky=-0.000369414 kz=23.0649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12088e-09 l2=2.94826e-05 x=4.77782e-05 y=0.000181219 z=-1.47403e-05 kx=-0.000739477 ky=-0.000657447 kz=22.4822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36554e-09 l2=1.22686e-05 x=4.96221e-05 y=-0.000499359 z=-6.13689e-06 kx=0.000899245 ky=-0.00194285 kz=23.2613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01303e-09 l2=9.03096e-06 x=4.97958e-05 y=-5.19151e-05 z=-4.515e-06 kx=-0.00044637 ky=-0.000593602 kz=22.4683 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1339e-09 l2=1.68161e-05 x=-4.92879e-05 y=0.000366231 z=-8.40974e-06 kx=-0.00051729 ky=0.00131797 kz=22.4393 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71771e-09 l2=6.15565e-06 x=-4.99051e-05 y=-4.16123e-05 z=-3.08142e-06 kx=-0.00100808 ky=-0.000457634 kz=22.4539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36942e-09 l2=2.92053e-05 x=4.78204e-05 y=6.89497e-05 z=-1.46031e-05 kx=-0.000109271 ky=0.00121344 kz=23.1538 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75697e-09 l2=1.4377e-05 x=-4.9481e-05 y=0.00031168 z=-7.1874e-06 kx=0.000931241 ky=0.00155016 kz=23.0216 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03064e-09 l2=1.3204e-05 x=4.95624e-05 y=-0.000191511 z=-6.60305e-06 kx=1.67951e-05 ky=0.000198539 kz=23.3066 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.42949e-09 l2=8.50443e-06 x=4.98189e-05 y=6.90807e-05 z=-4.25471e-06 kx=0.000585796 ky=-0.000202137 kz=22.8301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.2053e-09 l2=6.4116e-06 x=-4.98973e-05 y=0.000140674 z=-3.20487e-06 kx=0.000946297 ky=-0.000568864 kz=23.2643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23661e-09 l2=3.05568e-05 x=4.76083e-05 y=-0.000293807 z=-1.52803e-05 kx=0.000640146 ky=8.56953e-05 kz=23.0475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05398e-09 l2=1.2575e-05 x=-4.9603e-05 y=0.000441094 z=-6.28961e-06 kx=-0.000705149 ky=0.00209399 kz=22.4382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63592e-09 l2=3.56118e-06 x=4.99683e-05 y=-0.000485142 z=-1.78163e-06 kx=0.000101293 ky=-0.00151319 kz=22.3055 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00873e-09 l2=3.90068e-05 x=4.60392e-05 y=0.000498996 z=-1.95046e-05 kx=0.000346299 ky=0.000896322 kz=22.8086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.25139e-09 l2=4.28088e-06 x=-4.99543e-05 y=-0.000461045 z=-2.14195e-06 kx=0.000280173 ky=-0.00183106 kz=22.556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16052e-09 l2=2.8117e-05 x=4.79828e-05 y=-0.000167182 z=-1.40599e-05 kx=0.00041175 ky=0.000517009 kz=22.8066 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.97371e-09 l2=8.35296e-06 x=4.98252e-05 y=0.0002632 z=-4.18063e-06 kx=0.00120236 ky=0.00113559 kz=22.5044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29606e-09 l2=8.62366e-06 x=-4.98137e-05 y=0.000307162 z=-4.31365e-06 kx=-0.000531924 ky=0.000518545 kz=22.5523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10379e-09 l2=1.85408e-05 x=4.91329e-05 y=-7.56326e-05 z=-9.27263e-06 kx=0.000780866 ky=-0.00108793 kz=22.7073 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.05906e-09 l2=8.64816e-06 x=4.98127e-05 y=0.000496051 z=-4.32634e-06 kx=0.000336097 ky=0.000860138 kz=22.9375 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31122e-09 l2=7.47984e-06 x=4.98601e-05 y=0.000390838 z=-3.73906e-06 kx=-0.000682475 ky=0.00086296 kz=22.3895 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47073e-09 l2=8.28422e-06 x=-4.98283e-05 y=0.000138268 z=-4.14165e-06 kx=0.00054009 ky=0.00132917 kz=22.5547 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.78947e-09 l2=3.15826e-06 x=-4.99752e-05 y=-0.00021987 z=-1.58483e-06 kx=-0.000607778 ky=0.000436944 kz=23.2315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03977e-09 l2=2.60034e-05 x=-4.82801e-05 y=-0.000378662 z=-1.30022e-05 kx=2.66739e-05 ky=-0.00143031 kz=22.95 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06531e-09 l2=4.17875e-05 x=4.54259e-05 y=0.000265328 z=-2.08933e-05 kx=-0.00052509 ky=0.00142568 kz=23.2723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00584e-09 l2=2.59334e-05 x=-4.82894e-05 y=-0.00046828 z=-1.29677e-05 kx=-0.000229512 ky=-0.000433497 kz=22.6901 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98486e-09 l2=7.15218e-06 x=-4.98721e-05 y=4.95404e-05 z=-3.57691e-06 kx=0.000309117 ky=0.000267608 kz=22.9064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74568e-09 l2=1.56501e-05 x=-4.93838e-05 y=0.000334508 z=-7.82743e-06 kx=-0.000719975 ky=0.00143038 kz=23.1472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.10539e-09 l2=7.03546e-06 x=4.98763e-05 y=0.00018358 z=-3.51821e-06 kx=-0.000489976 ky=-4.30269e-05 kz=22.7111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20262e-09 l2=2.94354e-05 x=4.77843e-05 y=-0.000471132 z=-1.47205e-05 kx=0.00106002 ky=-0.00103045 kz=23.2238 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07562e-09 l2=2.7001e-05 x=-4.81425e-05 y=-0.000395287 z=-1.3503e-05 kx=-0.000889127 ky=-0.00191607 kz=22.534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56999e-09 l2=1.06764e-05 x=4.97145e-05 y=-0.00034312 z=-5.33742e-06 kx=-0.000735484 ky=0.000124346 kz=23.1854 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29116e-09 l2=1.82638e-05 x=-4.91591e-05 y=0.000403661 z=-9.13264e-06 kx=-3.31803e-05 ky=0.000370073 kz=23.2248 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73259e-09 l2=9.97805e-06 x=4.97503e-05 y=0.000300327 z=-4.9921e-06 kx=0.00103247 ky=0.0015759 kz=23.2258 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4583e-09 l2=2.19932e-05 x=-4.87763e-05 y=-0.000479277 z=-1.09955e-05 kx=0.000866779 ky=-0.00220313 kz=22.5014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02262e-09 l2=7.07015e-06 x=4.98748e-05 y=0.000119203 z=-3.5367e-06 kx=0.000501303 ky=-0.000517521 kz=22.4254 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46147e-09 l2=2.29206e-05 x=4.86693e-05 y=0.000140806 z=-1.14599e-05 kx=-0.000560458 ky=0.00135341 kz=23.2191 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36277e-09 l2=1.91987e-05 x=-4.90699e-05 y=-0.000385507 z=-9.60054e-06 kx=-0.000228754 ky=-0.000864271 kz=22.5641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03492e-09 l2=1.19363e-05 x=-4.96427e-05 y=-0.000133333 z=-5.96846e-06 kx=0.000316719 ky=-0.0002996 kz=22.8908 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63498e-09 l2=1.4423e-05 x=-4.94772e-05 y=0.000300596 z=-7.21323e-06 kx=-0.00042488 ky=0.000102273 kz=22.9454 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.07718e-09 l2=2.13871e-06 x=4.99886e-05 y=3.02018e-05 z=-1.07336e-06 kx=0.000438253 ky=0.000264175 kz=22.6377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06057e-09 l2=5.84534e-06 x=-4.99146e-05 y=-0.000153977 z=-2.9215e-06 kx=0.000781614 ky=8.57337e-05 kz=22.8836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.66617e-09 l2=4.43509e-06 x=4.99509e-05 y=-0.00027038 z=-2.22015e-06 kx=0.000124314 ky=-0.00133145 kz=23.2147 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13348e-09 l2=6.37104e-06 x=4.98983e-05 y=-0.000187874 z=-3.18931e-06 kx=0.00123552 ky=-0.000629766 kz=22.6029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19082e-09 l2=2.3917e-05 x=4.85489e-05 y=0.000428211 z=-1.19595e-05 kx=0.000174923 ky=0.000203381 kz=23.2296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23357e-09 l2=1.68003e-05 x=4.92896e-05 y=0.000387591 z=-8.39953e-06 kx=-0.000582243 ky=0.0016402 kz=23.0089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03338e-09 l2=2.03657e-05 x=-4.89526e-05 y=-0.000406275 z=-1.01813e-05 kx=0.000958722 ky=-0.000109089 kz=23.1905 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25851e-09 l2=1.05318e-05 x=-4.97221e-05 y=-4.24868e-05 z=-5.26632e-06 kx=0.000340481 ky=0.000226831 kz=23.306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.9285e-09 l2=1.24216e-05 x=4.96127e-05 y=0.000454308 z=-6.21401e-06 kx=0.000784895 ky=0.00177437 kz=22.4152 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.40451e-09 l2=6.45778e-06 x=4.98958e-05 y=-0.000121008 z=-3.22989e-06 kx=-0.000326252 ky=-0.000729828 kz=23.0635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.58983e-09 l2=7.12954e-06 x=4.98728e-05 y=0.000139088 z=-3.56905e-06 kx=0.000903426 ky=0.00138912 kz=22.7111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.26046e-09 l2=6.54571e-06 x=-4.98927e-05 y=3.88766e-05 z=-3.27647e-06 kx=-0.000909475 ky=1.13981e-05 kz=22.8881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.16029e-09 l2=7.16812e-06 x=4.98716e-05 y=-7.02934e-05 z=-3.58484e-06 kx=-0.000359467 ky=0.000936742 kz=22.3668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.64454e-09 l2=1.20703e-05 x=-4.96347e-05 y=0.000486642 z=-6.03575e-06 kx=0.000326953 ky=0.00119856 kz=23.2792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46985e-09 l2=2.58502e-06 x=-4.99833e-05 y=0.000449533 z=-1.293e-06 kx=0.00034668 ky=0.000622327 kz=23.1233 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11053e-09 l2=8.80889e-06 x=-4.98058e-05 y=-0.000432514 z=-4.40343e-06 kx=0.000709139 ky=-0.000702423 kz=22.5324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36177e-09 l2=1.50736e-05 x=-4.94286e-05 y=-0.000328249 z=-7.53852e-06 kx=-0.000460532 ky=-0.00068992 kz=22.3371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83081e-09 l2=1.37179e-05 x=4.95274e-05 y=8.31252e-05 z=-6.86048e-06 kx=0.000282736 ky=-0.000130758 kz=23.2894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02541e-09 l2=2.35772e-05 x=4.85906e-05 y=0.000118497 z=-1.1789e-05 kx=-3.39241e-05 ky=0.000440124 kz=22.4543 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23453e-09 l2=1.83758e-05 x=-4.91483e-05 y=0.000161229 z=-9.19037e-06 kx=-0.000840193 ky=-0.000677242 kz=22.3319 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57358e-09 l2=8.08741e-06 x=-4.98363e-05 y=-0.000120646 z=-4.04442e-06 kx=3.08617e-05 ky=0.00022828 kz=22.8028 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43506e-09 l2=2.05011e-05 x=4.89376e-05 y=0.000246269 z=-1.02539e-05 kx=0.00124085 ky=-5.94996e-05 kz=22.8937 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42527e-09 l2=1.22741e-05 x=-4.9622e-05 y=3.39566e-05 z=-6.13832e-06 kx=-0.000257179 ky=0.00103916 kz=22.5807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05489e-09 l2=2.17056e-05 x=-4.88076e-05 y=-8.09312e-05 z=-1.08553e-05 kx=-0.000917802 ky=0.000829962 kz=22.6041 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72228e-09 l2=1.26323e-05 x=-4.95998e-05 y=-8.54569e-05 z=-6.31549e-06 kx=0.000705238 ky=0.000515097 kz=22.6634 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56915e-09 l2=1.96988e-05 x=4.90199e-05 y=-0.000239771 z=-9.85274e-06 kx=0.00119449 ky=-0.000409867 kz=22.9015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.22464e-09 l2=1.03446e-05 x=4.97318e-05 y=-5.40883e-05 z=-5.17492e-06 kx=0.0004691 ky=0.000467577 kz=22.7668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36006e-09 l2=1.76188e-05 x=4.92176e-05 y=0.000141213 z=-8.81214e-06 kx=0.000948819 ky=0.000652593 kz=22.6857 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10658e-09 l2=2.63903e-05 x=4.82278e-05 y=-0.000238132 z=-1.31952e-05 kx=-0.000245953 ky=0.000249437 kz=22.545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16719e-09 l2=1.91443e-05 x=4.90754e-05 y=-0.000269978 z=-9.57209e-06 kx=-0.000300816 ky=-0.00157148 kz=23.1711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53604e-09 l2=2.24971e-05 x=-4.87178e-05 y=-0.00014951 z=-1.12519e-05 kx=-0.00120879 ky=0.000185582 kz=22.744 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13657e-08 l2=7.61185e-07 x=-4.99986e-05 y=0.000151353 z=-3.8984e-07 kx=0.000656419 ky=0.000754282 kz=22.8644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34877e-09 l2=1.45246e-05 x=-4.94699e-05 y=0.000410402 z=-7.26269e-06 kx=0.000129397 ky=0.000531195 kz=22.4346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18641e-09 l2=1.74087e-05 x=-4.92363e-05 y=-0.000227782 z=-8.70685e-06 kx=-0.000898654 ky=-0.0012309 kz=23.0703 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16825e-09 l2=1.17195e-05 x=-4.96556e-05 y=-0.000193552 z=-5.85994e-06 kx=0.000183163 ky=-2.52212e-05 kz=23.0186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01767e-09 l2=1.20072e-05 x=4.96382e-05 y=-0.000129936 z=-6.00648e-06 kx=0.000871065 ky=-0.000852226 kz=22.8486 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09468e-09 l2=3.24728e-05 x=4.72902e-05 y=9.95799e-05 z=-1.62381e-05 kx=0.000525182 ky=-0.000350121 kz=22.6335 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31783e-09 l2=2.18451e-05 x=4.87923e-05 y=6.20083e-05 z=-1.09242e-05 kx=0.000454436 ky=-0.000488014 kz=22.4595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95138e-09 l2=6.51776e-06 x=-4.98939e-05 y=-0.000331394 z=-3.25844e-06 kx=0.000888024 ky=-0.00112032 kz=23.1061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45721e-09 l2=1.78748e-05 x=-4.91945e-05 y=0.000350851 z=-8.94042e-06 kx=-0.00106554 ky=0.000533956 kz=23.1255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95348e-09 l2=1.12431e-05 x=4.96833e-05 y=-0.000243071 z=-5.62035e-06 kx=-0.00101115 ky=-0.00140418 kz=22.8824 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06073e-09 l2=1.38391e-05 x=4.9519e-05 y=0.000476917 z=-6.92003e-06 kx=-2.00878e-05 ky=0.0022005 kz=22.7086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15441e-09 l2=2.3806e-05 x=4.8563e-05 y=8.97043e-05 z=-1.19022e-05 kx=-0.000691279 ky=-4.60596e-05 kz=23.1568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.08151e-09 l2=3.79489e-06 x=-4.99641e-05 y=-0.000293403 z=-1.90037e-06 kx=-0.000171017 ky=-0.000822097 kz=22.3574 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07436e-09 l2=2.38282e-05 x=-4.85602e-05 y=-3.45594e-05 z=-1.19134e-05 kx=0.000619284 ky=-0.000807442 kz=23.2183 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10962e-09 l2=2.62737e-05 x=-4.82431e-05 y=-0.000365177 z=-1.3139e-05 kx=-0.000754059 ky=-0.000682896 kz=22.8212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58153e-09 l2=2.71904e-05 x=4.81159e-05 y=-0.000101051 z=-1.35978e-05 kx=0.000842615 ky=0.000292936 kz=22.7794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30263e-09 l2=2.2207e-05 x=4.87512e-05 y=0.000273221 z=-1.11064e-05 kx=0.00108309 ky=0.000725315 kz=23.2034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06309e-09 l2=2.46221e-05 x=4.8461e-05 y=-0.000299293 z=-1.2311e-05 kx=-0.000249333 ky=8.33572e-05 kz=22.3948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.67952e-09 l2=3.93456e-06 x=-4.99614e-05 y=0.000326501 z=-1.96867e-06 kx=0.000200992 ky=0.000721855 kz=22.5506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.219e-09 l2=2.10794e-05 x=4.88762e-05 y=3.87711e-05 z=-1.05424e-05 kx=0.000974026 ky=0.00111872 kz=22.5697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.28268e-09 l2=5.37866e-06 x=-4.99278e-05 y=0.000264608 z=-2.69526e-06 kx=-0.000592976 ky=-7.11783e-05 kz=22.9202 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75033e-09 l2=7.24632e-06 x=4.98687e-05 y=-0.000456768 z=-3.62444e-06 kx=-4.16683e-05 ky=-0.00175872 kz=22.8169 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02029e-09 l2=3.98116e-05 x=-4.58675e-05 y=-0.000364853 z=-1.99051e-05 kx=0.000608724 ky=-0.000194536 kz=23.134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14226e-09 l2=1.1566e-05 x=4.96644e-05 y=-0.000266071 z=-5.78536e-06 kx=0.000605748 ky=-0.000555402 kz=22.9841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4101e-09 l2=2.15266e-05 x=4.88283e-05 y=0.000229834 z=-1.07624e-05 kx=-0.000734088 ky=0.000666216 kz=22.495 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.14456e-09 l2=1.85547e-06 x=4.99914e-05 y=0.000254728 z=-9.30652e-07 kx=0.000160431 ky=-0.000506516 kz=23.1958 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.78325e-09 l2=7.23182e-06 x=4.98692e-05 y=-0.000269133 z=-3.61738e-06 kx=3.62748e-05 ky=-0.000532849 kz=22.8504 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13533e-09 l2=2.39273e-05 x=-4.8548e-05 y=0.000208864 z=-1.19631e-05 kx=0.000536557 ky=-0.000400869 kz=22.5309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95e-09 l2=1.55789e-05 x=-4.93893e-05 y=0.000432291 z=-7.7929e-06 kx=-0.0011475 ky=2.75185e-05 kz=22.6414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77243e-09 l2=1.46438e-05 x=-4.94611e-05 y=-0.000340699 z=-7.32312e-06 kx=-0.000148468 ky=-0.00124545 kz=23.2356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58431e-09 l2=1.15346e-05 x=4.96665e-05 y=-0.000342337 z=-5.76716e-06 kx=-0.000421194 ky=-0.00184266 kz=22.4516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08519e-09 l2=2.154e-05 x=-4.88259e-05 y=-0.000228945 z=-1.07727e-05 kx=-0.00100495 ky=-0.000847635 kz=22.9179 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.51729e-09 l2=1.44606e-05 x=-4.94746e-05 y=0.000136315 z=-7.23181e-06 kx=-0.000114535 ky=-0.00018736 kz=23.1893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4082e-09 l2=7.4486e-06 x=4.98613e-05 y=-0.000184461 z=-3.72278e-06 kx=-0.00102476 ky=-0.000419706 kz=23.0133 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17056e-09 l2=1.53425e-05 x=-4.94084e-05 y=0.000369326 z=-7.67018e-06 kx=0.000767124 ky=0.00128171 kz=22.7915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41303e-09 l2=1.50314e-05 x=-4.94318e-05 y=0.000485781 z=-7.51815e-06 kx=-0.000787935 ky=0.000129999 kz=22.4429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.94937e-09 l2=2.37024e-06 x=-4.9986e-05 y=-0.000331091 z=-1.19013e-06 kx=-0.00024768 ky=0.000125909 kz=23.0126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58835e-09 l2=1.87734e-05 x=-4.91115e-05 y=-0.000125623 z=-9.38577e-06 kx=0.0008038 ky=0.000374127 kz=22.8503 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29371e-09 l2=8.88887e-06 x=4.98019e-05 y=-0.000101958 z=-4.44718e-06 kx=0.000946666 ky=-0.00121846 kz=22.4772 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23022e-09 l2=2.17403e-05 x=4.8804e-05 y=-0.000127033 z=-1.08719e-05 kx=0.000526724 ky=0.000264924 kz=23.2094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0541e-09 l2=2.82153e-05 x=-4.79681e-05 y=-0.000221026 z=-1.411e-05 kx=-0.000879062 ky=-0.000324557 kz=22.5204 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95645e-09 l2=1.29327e-05 x=4.958e-05 y=-0.000461423 z=-6.46901e-06 kx=0.000775983 ky=-0.000154503 kz=22.8102 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.18846e-09 l2=6.70457e-06 x=-4.98876e-05 y=-0.000422509 z=-3.35374e-06 kx=6.48581e-05 ky=-0.000546799 kz=22.9884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28908e-09 l2=9.45561e-06 x=4.9776e-05 y=-2.70162e-05 z=-4.73004e-06 kx=0.000507015 ky=0.00016533 kz=23.2469 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6951e-09 l2=2.12856e-05 x=-4.88544e-05 y=-0.000321747 z=-1.06437e-05 kx=5.56195e-06 ky=0.00036325 kz=22.6261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30968e-09 l2=2.44647e-05 x=4.84805e-05 y=-0.000474066 z=-1.22341e-05 kx=0.000516763 ky=-0.00143013 kz=22.9481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.114e-09 l2=1.50103e-05 x=-4.94338e-05 y=1.28959e-05 z=-7.50416e-06 kx=0.000718462 ky=0.00113089 kz=22.749 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.46601e-09 l2=6.44294e-06 x=-4.98962e-05 y=-0.000316174 z=-3.22313e-06 kx=3.56919e-05 ky=-0.000380937 kz=22.7653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05683e-09 l2=2.13718e-05 x=4.88443e-05 y=0.000274792 z=-1.06889e-05 kx=0.00115072 ky=0.00156289 kz=22.8807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31006e-09 l2=1.56987e-05 x=-4.93798e-05 y=-0.000200288 z=-7.8519e-06 kx=-0.000883966 ky=-0.000372311 kz=23.2265 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22389e-09 l2=1.24286e-05 x=4.96124e-05 y=7.69615e-05 z=-6.21483e-06 kx=-4.32917e-05 ky=0.000116488 kz=22.6357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29873e-09 l2=1.52093e-05 x=4.94183e-05 y=0.000313406 z=-7.60579e-06 kx=0.00023106 ky=0.000438008 kz=22.688 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08911e-09 l2=1.51247e-05 x=-4.94251e-05 y=-0.00038978 z=-7.56124e-06 kx=0.000770581 ky=-0.000921237 kz=23.1803 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25113e-09 l2=5.35502e-06 x=4.99283e-05 y=-0.000266645 z=-2.67785e-06 kx=-0.000129579 ky=-0.00133577 kz=22.8346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35507e-09 l2=1.05327e-05 x=-4.97221e-05 y=-0.000321913 z=-5.26576e-06 kx=0.000588366 ky=0.000332449 kz=23.2836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37727e-09 l2=1.72021e-05 x=-4.92544e-05 y=0.000343487 z=-8.60369e-06 kx=-0.000891346 ky=0.00154792 kz=22.526 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89124e-09 l2=7.20955e-06 x=4.98699e-05 y=0.000151812 z=-3.60655e-06 kx=0.000374892 ky=0.000458281 kz=22.6042 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53812e-09 l2=2.26163e-05 x=-4.87044e-05 y=-0.000156583 z=-1.13101e-05 kx=-0.000570941 ky=-0.00146399 kz=22.3332 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53638e-09 l2=8.12796e-06 x=-4.98347e-05 y=-0.000455587 z=-4.06441e-06 kx=0.000156254 ky=5.08518e-05 kz=22.9689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15099e-09 l2=1.56966e-05 x=4.93802e-05 y=9.46293e-05 z=-7.84916e-06 kx=0.000135631 ky=0.000771499 kz=22.682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13079e-09 l2=3.49399e-05 x=-4.68489e-05 y=0.000330833 z=-1.74705e-05 kx=-9.55141e-06 ky=7.02038e-05 kz=23.1065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45848e-09 l2=1.47922e-05 x=4.94498e-05 y=-0.000428371 z=-7.39855e-06 kx=0.000786418 ky=-0.00110637 kz=22.9075 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.8107e-09 l2=1.39246e-05 x=4.95129e-05 y=0.000160633 z=-6.96522e-06 kx=0.000685211 ky=0.00139622 kz=22.5463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86554e-09 l2=2.15755e-05 x=4.88227e-05 y=0.000292942 z=-1.07881e-05 kx=-0.000276295 ky=0.00110334 kz=22.8 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41651e-09 l2=1.57902e-05 x=4.93731e-05 y=-1.54194e-05 z=-7.89401e-06 kx=-0.000823229 ky=-0.000350663 kz=22.8327 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07003e-09 l2=2.9841e-05 x=4.77217e-05 y=0.00049584 z=-1.49223e-05 kx=0.000597674 ky=0.00203074 kz=23.2573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.817e-09 l2=1.479e-05 x=4.94504e-05 y=0.000191029 z=-7.39592e-06 kx=-0.000226528 ky=0.00023101 kz=22.6607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87176e-09 l2=1.20968e-05 x=4.96328e-05 y=-7.49583e-05 z=-6.0507e-06 kx=0.000624191 ky=-0.000649996 kz=23.0836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25117e-09 l2=1.28787e-05 x=4.95835e-05 y=-0.00010688 z=-6.44119e-06 kx=0.000536431 ky=0.000292981 kz=22.3095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16705e-09 l2=2.47889e-05 x=-4.84393e-05 y=-0.000263565 z=-1.2396e-05 kx=-0.000450855 ky=6.44364e-05 kz=22.3439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10173e-09 l2=7.94135e-06 x=-4.9842e-05 y=-0.00017617 z=-3.97387e-06 kx=-0.000984595 ky=-0.00072376 kz=22.83 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.2802e-09 l2=2.1833e-05 x=-4.87935e-05 y=-0.00031568 z=-1.09197e-05 kx=-0.000978135 ky=-0.000571577 kz=22.8187 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4656e-09 l2=1.78846e-06 x=4.9992e-05 y=0.000128532 z=-8.97738e-07 kx=0.001016 ky=0.000595018 kz=22.3397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79868e-09 l2=1.01064e-05 x=4.97441e-05 y=6.11145e-05 z=-5.05425e-06 kx=5.79121e-05 ky=-0.000933051 kz=22.781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67478e-09 l2=1.12709e-05 x=-4.96814e-05 y=0.000217834 z=-5.63796e-06 kx=-0.000524163 ky=-0.000325055 kz=22.3788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18579e-09 l2=9.82576e-06 x=4.97583e-05 y=0.000179487 z=-4.91266e-06 kx=-0.00061316 ky=-0.000171671 kz=23.2695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30252e-09 l2=1.0532e-05 x=4.97218e-05 y=-6.64729e-05 z=-5.2694e-06 kx=0.00102369 ky=-0.00118068 kz=22.7474 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21969e-09 l2=1.978e-05 x=-4.90123e-05 y=3.63204e-05 z=-9.8901e-06 kx=0.000240222 ky=-0.000502816 kz=23.0898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81553e-09 l2=7.08831e-06 x=4.98744e-05 y=-4.46486e-05 z=-3.54424e-06 kx=-0.000374406 ky=-0.000885677 kz=22.674 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16446e-09 l2=2.08671e-05 x=4.88999e-05 y=-0.000165806 z=-1.0432e-05 kx=-0.00101519 ky=-0.000151707 kz=22.7964 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.23066e-09 l2=8.0962e-06 x=-4.98358e-05 y=-0.000212924 z=-4.05273e-06 kx=-0.00115427 ky=-0.00124944 kz=22.8872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.71347e-09 l2=4.23525e-06 x=-4.99552e-05 y=0.000155689 z=-2.12183e-06 kx=-0.000605022 ky=0.00109548 kz=22.3971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03194e-09 l2=4.76151e-05 x=-4.39674e-05 y=0.000206538 z=-2.38099e-05 kx=-0.000962487 ky=0.000668681 kz=22.5878 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03479e-09 l2=1.53944e-05 x=4.94042e-05 y=-0.000471701 z=-7.69694e-06 kx=-0.000363754 ky=-0.00134538 kz=23.1062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35236e-09 l2=1.65748e-05 x=-4.93088e-05 y=-0.000196895 z=-8.28616e-06 kx=0.000887241 ky=0.000654552 kz=23.0155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.12409e-09 l2=1.31483e-05 x=-4.95662e-05 y=-0.000172296 z=-6.575e-06 kx=0.000331862 ky=-0.00100605 kz=22.7507 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42363e-09 l2=1.67366e-05 x=-4.9295e-05 y=0.000446554 z=-8.36794e-06 kx=0.000487568 ky=0.00212539 kz=22.7176 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10215e-09 l2=8.01284e-06 x=4.98395e-05 y=0.000123097 z=-4.00564e-06 kx=-0.000822113 ky=-0.000160781 kz=22.405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76032e-09 l2=1.0175e-05 x=-4.97404e-05 y=-0.000464938 z=-5.09041e-06 kx=-0.000944096 ky=7.16997e-05 kz=22.8809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02307e-09 l2=7.2966e-06 x=-4.98666e-05 y=-3.89913e-05 z=-3.65148e-06 kx=-0.00101174 ky=0.000551414 kz=23.3038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05195e-09 l2=7.24925e-06 x=-4.98686e-05 y=-0.000111635 z=-3.6238e-06 kx=0.00061356 ky=-0.00127786 kz=22.6303 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51713e-09 l2=1.33685e-05 x=4.9551e-05 y=0.000205754 z=-6.68749e-06 kx=0.00115507 ky=0.000963402 kz=22.9357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43299e-09 l2=1.63627e-05 x=4.9326e-05 y=-0.000284648 z=-8.18472e-06 kx=0.00100565 ky=-0.000892661 kz=22.9458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88857e-09 l2=1.96942e-05 x=-4.90208e-05 y=-0.000279023 z=-9.84856e-06 kx=-0.000240358 ky=-0.00154431 kz=22.6463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1497e-09 l2=1.2603e-05 x=-4.96011e-05 y=-2.64815e-05 z=-6.30447e-06 kx=-0.00108968 ky=-0.000292308 kz=22.3227 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30483e-09 l2=7.56101e-06 x=4.98568e-05 y=-0.000172299 z=-3.7838e-06 kx=0.000991142 ky=0.000639553 kz=23.1021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36766e-09 l2=2.3382e-05 x=-4.86139e-05 y=-0.00010437 z=-1.16926e-05 kx=-0.000430808 ky=-0.00083101 kz=22.4383 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29368e-09 l2=7.16453e-06 x=-4.98716e-05 y=-3.35341e-05 z=-3.58297e-06 kx=-2.81499e-05 ky=0.000922508 kz=22.6607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3334e-09 l2=2.67573e-05 x=-4.81773e-05 y=-0.000362358 z=-1.33786e-05 kx=0.000342788 ky=-0.00184575 kz=22.8727 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20068e-09 l2=3.1749e-05 x=-4.74127e-05 y=0.000233095 z=-1.58768e-05 kx=-0.000831823 ky=0.000748294 kz=22.8444 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30268e-09 l2=2.90105e-05 x=4.78493e-05 y=-4.02514e-05 z=-1.45081e-05 kx=0.00106362 ky=9.68016e-05 kz=22.9166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13276e-08 l2=1.83111e-06 x=4.99918e-05 y=-0.000376544 z=-9.19234e-07 kx=-0.000885661 ky=-0.00161017 kz=22.2995 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02471e-09 l2=1.54614e-05 x=4.93989e-05 y=-0.000287954 z=-7.73065e-06 kx=-0.000246843 ky=-0.000586453 kz=22.4111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69099e-09 l2=1.2416e-05 x=-4.96132e-05 y=-0.000470582 z=-6.20906e-06 kx=-9.67642e-05 ky=-0.001863 kz=22.3391 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0673e-09 l2=2.56172e-05 x=-4.83319e-05 y=-0.000358196 z=-1.28083e-05 kx=0.000393914 ky=-0.000871653 kz=22.3378 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13427e-09 l2=6.33651e-06 x=4.98997e-05 y=0.00035397 z=-3.16706e-06 kx=-0.000796796 ky=0.00168542 kz=22.5214 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65456e-09 l2=1.09984e-05 x=4.9697e-05 y=-0.000489155 z=-5.4979e-06 kx=-0.000974849 ky=-0.000142777 kz=22.9039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59463e-09 l2=1.2603e-05 x=4.96016e-05 y=-0.000222402 z=-6.30051e-06 kx=-0.000827092 ky=-0.00143173 kz=23.0128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13607e-09 l2=1.91759e-05 x=-4.90723e-05 y=0.000417039 z=-9.58793e-06 kx=0.000274979 ky=-4.89789e-05 kz=22.9957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13817e-09 l2=1.76911e-05 x=-4.92113e-05 y=0.000297005 z=-8.84688e-06 kx=-0.000359048 ky=0.000705528 kz=22.5603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1113e-09 l2=2.4247e-05 x=-4.85085e-05 y=0.000370644 z=-1.21225e-05 kx=0.000729935 ky=0.000260239 kz=22.9395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20743e-09 l2=9.19933e-06 x=-4.9788e-05 y=-0.000291629 z=-4.60043e-06 kx=-7.30871e-05 ky=-0.0011347 kz=22.7171 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.00264e-09 l2=4.19522e-06 x=4.99562e-05 y=-0.000477633 z=-2.09943e-06 kx=-0.000534026 ky=-0.000280001 kz=22.6089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.01303e-09 l2=5.4907e-06 x=-4.99248e-05 y=0.000291682 z=-2.74701e-06 kx=0.00060233 ky=0.00111359 kz=22.4022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13142e-09 l2=1.2274e-05 x=-4.96219e-05 y=-0.000126661 z=-6.13888e-06 kx=-0.000612081 ky=-0.00142112 kz=22.7009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77104e-09 l2=2.35352e-05 x=-4.85951e-05 y=0.000465437 z=-1.1771e-05 kx=-0.00120234 ky=0.00208511 kz=22.8551 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11729e-09 l2=3.10419e-05 x=4.75303e-05 y=-1.28431e-05 z=-1.55212e-05 kx=-0.000126188 ky=-0.000848256 kz=22.8274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51763e-09 l2=1.93012e-05 x=4.90599e-05 y=0.000222474 z=-9.65151e-06 kx=6.85156e-05 ky=-3.16112e-05 kz=22.6382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0223e-09 l2=1.43411e-05 x=-4.94835e-05 y=0.000443464 z=-7.16893e-06 kx=0.000997673 ky=0.000402363 kz=23.2027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87729e-09 l2=1.11068e-05 x=4.96905e-05 y=0.000193382 z=-5.55669e-06 kx=0.00106631 ky=0.000871586 kz=22.3816 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82559e-09 l2=9.04058e-06 x=-4.97954e-05 y=-4.96971e-05 z=-4.52149e-06 kx=0.000100729 ky=-0.00109634 kz=23.0655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66154e-09 l2=1.14755e-05 x=4.967e-05 y=0.000382597 z=-5.73694e-06 kx=-0.000773625 ky=-6.23819e-05 kz=23.1566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80096e-09 l2=3.25999e-06 x=-4.99735e-05 y=0.000349926 z=-1.63044e-06 kx=0.000203859 ky=0.00185734 kz=22.3128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05717e-09 l2=2.94812e-05 x=-4.7778e-05 y=-4.71236e-06 z=-1.4741e-05 kx=7.22689e-05 ky=-0.000661697 kz=23.3095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25244e-09 l2=1.6083e-05 x=4.93492e-05 y=0.000357488 z=-8.0419e-06 kx=-0.000101672 ky=-5.20711e-05 kz=22.5748 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.4317e-09 l2=2.3797e-06 x=4.99859e-05 y=-0.000292494 z=-1.19491e-06 kx=0.000848613 ky=-0.000501731 kz=22.9456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39104e-09 l2=2.78708e-05 x=-4.80187e-05 y=-9.53407e-05 z=-1.39371e-05 kx=-0.000473117 ky=-0.000192653 kz=22.6897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4295e-09 l2=1.76815e-05 x=4.92126e-05 y=0.000197331 z=-8.84011e-06 kx=-0.000635802 ky=0.000822848 kz=22.7774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46415e-09 l2=5.09001e-06 x=-4.99353e-05 y=3.94355e-05 z=-2.54501e-06 kx=0.00032349 ky=4.20324e-05 kz=22.4019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51011e-09 l2=1.78127e-06 x=-4.99921e-05 y=8.56382e-05 z=-8.91067e-07 kx=0.000149458 ky=-0.000180872 kz=23.2436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.718e-09 l2=9.35173e-06 x=4.9781e-05 y=-0.000479625 z=-4.67844e-06 kx=0.000332119 ky=-0.00201266 kz=23.1091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22543e-09 l2=1.4389e-05 x=4.94798e-05 y=0.000310573 z=-7.19504e-06 kx=-4.20148e-05 ky=0.00167619 kz=22.3336 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0901e-09 l2=2.95908e-05 x=4.77603e-05 y=-0.000441888 z=-1.47982e-05 kx=0.00107982 ky=-0.000952067 kz=22.9735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49762e-09 l2=2.11401e-05 x=-4.88697e-05 y=1.2784e-05 z=-1.05727e-05 kx=-0.000896959 ky=0.000989609 kz=23.1479 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55419e-09 l2=1.32679e-05 x=-4.95582e-05 y=-0.000336075 z=-6.6333e-06 kx=0.000639861 ky=-0.00109894 kz=22.6435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54607e-09 l2=1.24473e-05 x=4.96113e-05 y=0.00037965 z=-6.22395e-06 kx=-0.000207498 ky=0.00153668 kz=22.7544 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82843e-09 l2=1.54649e-05 x=4.93984e-05 y=-0.00027688 z=-7.73473e-06 kx=0.000634315 ky=0.000492702 kz=22.7951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26699e-09 l2=2.24305e-05 x=4.87263e-05 y=0.000351872 z=-1.12151e-05 kx=-0.000373426 ky=0.00163723 kz=23.1566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.66588e-09 l2=8.54014e-06 x=4.98173e-05 y=-0.000347356 z=-4.27364e-06 kx=0.00102782 ky=-0.000492908 kz=22.8914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06989e-09 l2=3.02529e-05 x=4.76571e-05 y=0.000277568 z=-1.51271e-05 kx=3.94918e-05 ky=0.000501612 kz=23.1846 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.04476e-09 l2=8.60356e-06 x=4.98149e-05 y=7.09621e-05 z=-4.30249e-06 kx=-0.000599391 ky=0.000331063 kz=22.8484 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06066e-09 l2=1.88084e-05 x=-4.91079e-05 y=-0.000175571 z=-9.40411e-06 kx=0.000281984 ky=-0.00153636 kz=22.8463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13143e-09 l2=1.56046e-05 x=4.93872e-05 y=6.93903e-05 z=-7.80499e-06 kx=0.000950336 ky=0.000542359 kz=22.3473 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03371e-09 l2=3.70325e-05 x=-4.64449e-05 y=0.000277546 z=-1.85177e-05 kx=-0.000456111 ky=0.000374225 kz=22.7954 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07829e-09 l2=1.96485e-05 x=-4.90251e-05 y=-0.00023927 z=-9.82673e-06 kx=-0.000891892 ky=0.000423319 kz=22.7645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31894e-09 l2=1.98378e-05 x=4.90066e-05 y=7.30905e-05 z=-9.91864e-06 kx=-0.000425431 ky=0.000440543 kz=22.6337 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5253e-09 l2=1.18736e-05 x=-4.96465e-05 y=4.86531e-05 z=-5.93687e-06 kx=0.00031621 ky=0.000570249 kz=22.7329 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07407e-09 l2=1.86168e-05 x=4.91255e-05 y=0.000151065 z=-9.31148e-06 kx=0.00119887 ky=0.000368844 kz=23.2282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95342e-09 l2=8.50225e-06 x=4.9819e-05 y=-0.000359235 z=-4.25354e-06 kx=0.00042043 ky=-0.00105525 kz=22.3358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90173e-09 l2=7.73347e-06 x=4.98503e-05 y=-0.000216466 z=-3.86856e-06 kx=0.000394345 ky=3.43649e-05 kz=22.642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00495e-09 l2=7.27601e-06 x=4.98673e-05 y=0.000385094 z=-3.6412e-06 kx=0.00123117 ky=0.000793685 kz=22.7776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65546e-09 l2=1.76128e-05 x=4.92182e-05 y=0.00018125 z=-8.80886e-06 kx=0.000780811 ky=0.000985124 kz=23.2222 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62824e-09 l2=2.2659e-05 x=4.86991e-05 y=-0.000288286 z=-1.13327e-05 kx=0.00114475 ky=-7.30176e-05 kz=22.9055 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08056e-09 l2=4.42216e-05 x=4.4845e-05 y=4.39574e-05 z=-2.21127e-05 kx=0.000683652 ky=0.00106543 kz=22.8362 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15297e-09 l2=2.0504e-05 x=-4.89378e-05 y=-0.000141737 z=-1.02528e-05 kx=-9.15668e-05 ky=-0.000324829 kz=23.0459 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29467e-09 l2=2.02161e-05 x=-4.8968e-05 y=-4.99415e-05 z=-1.01074e-05 kx=0.000620885 ky=-0.000840039 kz=22.6295 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03922e-09 l2=9.85538e-06 x=4.97564e-05 y=-0.000248293 z=-4.93077e-06 kx=0.00117399 ky=-0.00113615 kz=22.8116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03089e-09 l2=2.88993e-05 x=-4.78661e-05 y=-9.20569e-05 z=-1.44522e-05 kx=-0.000958138 ky=0.000355441 kz=22.7292 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08313e-09 l2=2.52946e-05 x=4.83739e-05 y=-4.82052e-05 z=-1.26489e-05 kx=0.000478456 ky=-0.00088225 kz=22.8676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20826e-09 l2=2.34544e-05 x=-4.86053e-05 y=9.90184e-05 z=-1.17283e-05 kx=-0.0002513 ky=-2.84513e-05 kz=22.7352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07469e-09 l2=2.12483e-05 x=-4.88587e-05 y=0.000165151 z=-1.06231e-05 kx=0.000779555 ky=0.000284281 kz=23.0807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09565e-09 l2=2.09362e-05 x=4.88922e-05 y=-2.39715e-05 z=-1.04677e-05 kx=-0.000432833 ky=-0.000330744 kz=22.7883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18927e-09 l2=1.10179e-05 x=4.96956e-05 y=0.000370473 z=-5.51135e-06 kx=0.000604822 ky=0.00171738 kz=22.773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27009e-09 l2=3.14959e-05 x=-4.74561e-05 y=-9.83842e-06 z=-1.57468e-05 kx=0.000885063 ky=0.00105888 kz=23.287 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65229e-09 l2=1.92987e-05 x=4.90604e-05 y=7.0713e-06 z=-9.64906e-06 kx=-0.000529559 ky=0.000683529 kz=23.2689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59681e-09 l2=1.29258e-05 x=-4.95805e-05 y=0.000242339 z=-6.46526e-06 kx=-0.000729682 ky=0.000879538 kz=23.2014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62245e-09 l2=8.5519e-06 x=-4.98168e-05 y=-0.000454027 z=-4.27847e-06 kx=-0.000549099 ky=-0.00167807 kz=22.7117 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24333e-09 l2=2.97301e-05 x=-4.77387e-05 y=-0.000424294 z=-1.48679e-05 kx=-0.00110149 ky=0.000141915 kz=23.1349 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12148e-09 l2=2.86763e-05 x=-4.78999e-05 y=0.000374082 z=-1.43398e-05 kx=-0.00053902 ky=0.000679616 kz=23.2456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16072e-09 l2=1.15426e-05 x=-4.96658e-05 y=0.000465184 z=-5.77252e-06 kx=-0.000282623 ky=0.00130244 kz=22.5097 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45811e-09 l2=1.04665e-05 x=4.97256e-05 y=9.32203e-05 z=-5.23217e-06 kx=-0.000832213 ky=0.00110734 kz=22.9554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32777e-09 l2=2.48388e-05 x=-4.84327e-05 y=-1.54149e-05 z=-1.2422e-05 kx=-0.000913741 ky=-0.000348182 kz=22.9924 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66407e-09 l2=2.47374e-05 x=4.84456e-05 y=0.000369254 z=-1.23721e-05 kx=0.00116742 ky=0.000371895 kz=22.3176 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1123e-09 l2=2.48819e-05 x=-4.84275e-05 y=-0.000434743 z=-1.24421e-05 kx=-0.000277474 ky=-0.000960951 kz=22.6902 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16782e-09 l2=2.34563e-05 x=4.86054e-05 y=0.000325014 z=-1.17279e-05 kx=-0.000390393 ky=0.00164148 kz=22.8864 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35133e-09 l2=6.92084e-06 x=4.98801e-05 y=-2.28836e-05 z=-3.46225e-06 kx=0.000293981 ky=-0.00105371 kz=22.436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26043e-09 l2=2.49515e-05 x=-4.84187e-05 y=-4.45501e-05 z=-1.24764e-05 kx=-2.55419e-05 ky=-0.000357079 kz=23.0079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1082e-09 l2=2.24673e-05 x=4.87213e-05 y=0.000378266 z=-1.12364e-05 kx=0.00101708 ky=0.00185291 kz=23.0564 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70762e-09 l2=1.42481e-05 x=4.94901e-05 y=0.00028494 z=-7.12406e-06 kx=-0.000375323 ky=0.0016173 kz=22.5951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38358e-09 l2=2.76264e-05 x=4.8054e-05 y=0.000249182 z=-1.38147e-05 kx=0.000411113 ky=0.000688893 kz=22.9487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07319e-09 l2=3.40987e-05 x=-4.70034e-05 y=-0.000377652 z=-1.70505e-05 kx=-0.00027241 ky=-0.00140649 kz=22.7129 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79592e-09 l2=1.29496e-05 x=4.95789e-05 y=0.000441134 z=-6.47708e-06 kx=0.000642273 ky=-2.01963e-05 kz=22.7464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50238e-09 l2=9.35384e-06 x=-4.97809e-05 y=4.11603e-05 z=-4.67699e-06 kx=0.000309566 ky=-2.68091e-05 kz=22.6516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29701e-09 l2=1.88643e-05 x=4.91019e-05 y=-0.000199879 z=-9.4354e-06 kx=0.0012065 ky=-0.000608129 kz=22.6017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82091e-09 l2=5.91775e-06 x=-4.99124e-05 y=0.000169066 z=-2.95942e-06 kx=0.00016627 ky=0.00100424 kz=22.7107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39152e-09 l2=7.18445e-06 x=4.98709e-05 y=-2.03966e-05 z=-3.59342e-06 kx=-2.9794e-06 ky=-0.000556259 kz=22.331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9668e-09 l2=1.91362e-05 x=4.9076e-05 y=0.000137635 z=-9.57012e-06 kx=0.000478264 ky=0.000611355 kz=22.8084 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43271e-09 l2=6.90988e-06 x=4.98804e-05 y=0.0003324 z=-3.45874e-06 kx=0.00120175 ky=0.00162993 kz=23.1917 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05678e-09 l2=1.71711e-05 x=4.92574e-05 y=7.19147e-05 z=-8.58763e-06 kx=0.000495421 ky=0.000322052 kz=22.7466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07301e-09 l2=1.7731e-05 x=4.92077e-05 y=9.25131e-05 z=-8.86675e-06 kx=0.000337428 ky=-0.000146966 kz=22.5713 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36475e-09 l2=2.14968e-05 x=-4.88311e-05 y=-0.000101575 z=-1.07495e-05 kx=-0.000179025 ky=0.000215788 kz=23.2754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60328e-09 l2=2.09321e-05 x=-4.88929e-05 y=-0.000395166 z=-1.04649e-05 kx=0.000898913 ky=-0.000334198 kz=22.6842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.61842e-09 l2=9.74523e-06 x=4.97621e-05 y=-0.000355143 z=-4.87538e-06 kx=0.00044354 ky=-0.00131723 kz=22.9835 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76818e-09 l2=9.27654e-06 x=4.97846e-05 y=-0.000385707 z=-4.63821e-06 kx=-0.000434208 ky=-0.00059887 kz=22.7878 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28217e-09 l2=1.07191e-05 x=4.97122e-05 y=-0.000400412 z=-5.35805e-06 kx=-0.000976959 ky=-0.000781762 kz=22.7791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78031e-09 l2=8.08953e-06 x=-4.98363e-05 y=-0.000154736 z=-4.0448e-06 kx=0.000383929 ky=0.000562006 kz=22.4326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63997e-09 l2=1.43967e-05 x=-4.94791e-05 y=6.73894e-05 z=-7.2015e-06 kx=-0.000860907 ky=-3.18843e-05 kz=23.298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16273e-09 l2=1.12248e-05 x=4.96838e-05 y=0.000434844 z=-5.6153e-06 kx=0.00104902 ky=0.00123342 kz=22.5353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36977e-09 l2=1.51649e-05 x=-4.94218e-05 y=0.000283134 z=-7.58333e-06 kx=-0.000100876 ky=-0.000343331 kz=22.4013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08584e-09 l2=1.31845e-05 x=4.95638e-05 y=0.00030046 z=-6.59106e-06 kx=-0.000808351 ky=0.000173837 kz=23.2493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73834e-09 l2=9.2251e-06 x=4.97868e-05 y=0.000161883 z=-4.61461e-06 kx=0.000551829 ky=-0.000603441 kz=22.9522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.26662e-09 l2=2.37941e-06 x=-4.99859e-05 y=-7.16074e-05 z=-1.19548e-06 kx=-0.000961449 ky=0.000625513 kz=22.4905 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37503e-09 l2=1.79936e-05 x=4.91844e-05 y=0.000181067 z=-8.99551e-06 kx=-0.000909399 ky=0.000365655 kz=22.8612 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65544e-09 l2=1.05797e-05 x=4.97194e-05 y=-0.000280895 z=-5.29119e-06 kx=0.000235629 ky=-0.00056693 kz=22.4851 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25764e-09 l2=1.54245e-05 x=4.9402e-05 y=-0.000267834 z=-7.71241e-06 kx=-0.000453611 ky=-0.00117005 kz=22.7415 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07878e-09 l2=2.15535e-05 x=4.88254e-05 y=-0.000289493 z=-1.07751e-05 kx=-0.00100807 ky=-0.000658686 kz=22.6103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19747e-09 l2=3.15588e-06 x=-4.9975e-05 y=0.000133244 z=-1.58099e-06 kx=-0.00113243 ky=-0.000774437 kz=23.1161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09648e-09 l2=3.86791e-05 x=4.61086e-05 y=0.000475095 z=-1.93402e-05 kx=3.44702e-05 ky=0.00119669 kz=22.7223 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98578e-09 l2=7.27403e-06 x=4.98677e-05 y=-0.000316039 z=-3.63822e-06 kx=-0.000130575 ky=-0.000248842 kz=22.3021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04265e-09 l2=1.64246e-05 x=4.93207e-05 y=0.000199052 z=-8.215e-06 kx=0.00101812 ky=-2.2122e-05 kz=23.1984 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11066e-09 l2=3.11883e-05 x=-4.75054e-05 y=0.000418458 z=-1.55972e-05 kx=-0.00121773 ky=0.000101174 kz=23.0432 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.44242e-09 l2=3.0316e-06 x=-4.99771e-05 y=-0.000370233 z=-1.51804e-06 kx=-8.17673e-06 ky=-0.00128924 kz=22.5466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80911e-09 l2=1.39599e-05 x=-4.95102e-05 y=0.000190327 z=-6.98299e-06 kx=-0.000978959 ky=-0.000602816 kz=22.9379 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.50278e-09 l2=1.25134e-05 x=-4.96072e-05 y=-0.000399661 z=-6.25733e-06 kx=0.000302004 ky=-0.000964238 kz=23.2678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88719e-09 l2=1.37023e-05 x=-4.95285e-05 y=-5.1856e-05 z=-6.85227e-06 kx=-8.77958e-05 ky=-0.000398068 kz=22.761 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.34839e-09 l2=6.62199e-06 x=4.98904e-05 y=-0.000471008 z=-3.31151e-06 kx=-0.000302696 ky=-1.71635e-07 kz=22.8029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70515e-09 l2=8.30993e-06 x=4.98271e-05 y=0.000341559 z=-4.15722e-06 kx=0.000406756 ky=0.00150655 kz=22.3312 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71127e-09 l2=9.86246e-06 x=-4.97564e-05 y=0.000187962 z=-4.93272e-06 kx=-6.4623e-05 ky=0.00105942 kz=23.1558 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38111e-09 l2=1.92633e-05 x=-4.90636e-05 y=0.000178748 z=-9.63252e-06 kx=-8.74814e-05 ky=0.000359416 kz=22.8671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40599e-09 l2=1.97549e-05 x=4.90148e-05 y=-0.000109215 z=-9.87833e-06 kx=7.8652e-05 ky=0.000216032 kz=23.2524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.81945e-09 l2=2.51665e-06 x=-4.99842e-05 y=-0.000323268 z=-1.25852e-06 kx=0.000541964 ky=0.000260171 kz=22.3553 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78527e-09 l2=4.69503e-06 x=4.99449e-05 y=0.000464026 z=-2.34877e-06 kx=0.000163417 ky=-7.99535e-07 kz=22.4493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41172e-09 l2=1.92257e-05 x=-4.9067e-05 y=5.59927e-05 z=-9.61534e-06 kx=-0.000829714 ky=-0.000150924 kz=22.7134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08774e-09 l2=9.81248e-06 x=4.97587e-05 y=0.000484105 z=-4.90752e-06 kx=0.000330103 ky=0.00108112 kz=22.3976 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13376e-09 l2=3.53484e-05 x=4.67726e-05 y=0.000452374 z=-1.76737e-05 kx=-0.000528274 ky=0.00102218 kz=23.0849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53727e-09 l2=1.13579e-05 x=-4.96768e-05 y=0.000472029 z=-5.67771e-06 kx=0.000907741 ky=0.000654525 kz=22.5524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14591e-09 l2=1.63988e-05 x=-4.93236e-05 y=-0.000296594 z=-8.19789e-06 kx=0.000984161 ky=-0.000123487 kz=23.2557 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80909e-09 l2=2.25953e-05 x=4.87076e-05 y=-0.000183672 z=-1.12966e-05 kx=-0.000879522 ky=-0.00116128 kz=22.6009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33176e-09 l2=1.86566e-05 x=4.91226e-05 y=0.000195472 z=-9.3271e-06 kx=-0.000848975 ky=0.00031138 kz=22.5309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29341e-09 l2=1.53442e-05 x=4.94078e-05 y=-2.16124e-05 z=-7.67395e-06 kx=0.000545987 ky=-0.00115592 kz=22.3093 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03233e-09 l2=1.89574e-05 x=4.90936e-05 y=5.48511e-05 z=-9.47853e-06 kx=-0.000317036 ky=0.00114396 kz=23.1335 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10385e-09 l2=2.59935e-05 x=4.8282e-05 y=0.00017227 z=-1.29953e-05 kx=-0.000950539 ky=0.000108151 kz=22.6451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46426e-09 l2=9.1989e-06 x=-4.97878e-05 y=0.00020021 z=-4.60259e-06 kx=-0.00110392 ky=-5.29494e-05 kz=22.8382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23024e-09 l2=1.26888e-05 x=-4.95961e-05 y=-4.14364e-05 z=-6.34353e-06 kx=0.000690166 ky=0.000445455 kz=23.246 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0488e-09 l2=1.58339e-05 x=4.93696e-05 y=-0.000320766 z=-7.916e-06 kx=-0.000677099 ky=-0.00163129 kz=22.6577 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13612e-09 l2=2.12991e-05 x=4.88527e-05 y=0.00034746 z=-1.06507e-05 kx=0.000255031 ky=-0.000236162 kz=22.6974 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10245e-09 l2=1.9592e-05 x=4.90313e-05 y=-0.00049738 z=-9.79532e-06 kx=-0.000561091 ky=-0.00123493 kz=22.8517 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06983e-09 l2=2.79479e-05 x=4.80074e-05 y=-0.000223566 z=-1.39757e-05 kx=0.000600679 ky=0.000506863 kz=23.1314 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13427e-09 l2=2.33748e-05 x=-4.86145e-05 y=-0.00012746 z=-1.16899e-05 kx=-0.000901612 ky=0.000376316 kz=22.9569 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18473e-09 l2=4.3045e-05 x=-4.51311e-05 y=-0.000261532 z=-2.15229e-05 kx=7.81056e-05 ky=-0.00111512 kz=22.6358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2932e-09 l2=2.82801e-05 x=-4.79587e-05 y=-4.59689e-05 z=-1.41423e-05 kx=-0.000756414 ky=-0.000325061 kz=23.2297 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93556e-09 l2=1.20428e-05 x=4.96364e-05 y=-0.000278519 z=-6.02077e-06 kx=-0.000741365 ky=0.000338696 kz=22.6353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14456e-09 l2=2.24112e-05 x=-4.87287e-05 y=-0.000445716 z=-1.12043e-05 kx=0.000858446 ky=-5.36338e-05 kz=22.3805 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05508e-09 l2=4.01947e-05 x=4.5784e-05 y=-1.1537e-05 z=-2.00965e-05 kx=-0.000674994 ky=-0.000220916 kz=23.189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22952e-09 l2=2.07092e-05 x=4.89159e-05 y=0.000417383 z=-1.03565e-05 kx=0.000608773 ky=0.00114311 kz=22.6189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.93681e-09 l2=2.71955e-06 x=4.99815e-05 y=5.63414e-05 z=-1.36119e-06 kx=-2.67289e-05 ky=0.00101615 kz=22.3311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04213e-09 l2=1.63966e-05 x=-4.93237e-05 y=0.000111959 z=-8.19666e-06 kx=0.00101707 ky=0.000951505 kz=23.1096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00674e-09 l2=2.55781e-05 x=4.83366e-05 y=-8.30448e-05 z=-1.27905e-05 kx=0.000466078 ky=0.000897322 kz=22.9045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07378e-09 l2=2.93389e-05 x=-4.77991e-05 y=-0.000218306 z=-1.46724e-05 kx=-0.0011502 ky=0.000403185 kz=22.6132 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27266e-09 l2=1.64069e-05 x=4.93221e-05 y=-0.000240425 z=-8.20677e-06 kx=0.00126604 ky=0.00044823 kz=23.0574 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.39587e-09 l2=7.60167e-06 x=4.98552e-05 y=0.000247451 z=-3.80524e-06 kx=0.00122364 ky=0.000680376 kz=22.4994 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11669e-09 l2=6.60605e-06 x=-4.98908e-05 y=8.79598e-05 z=-3.30414e-06 kx=-0.000256154 ky=0.0010839 kz=22.6866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70635e-09 l2=9.6679e-06 x=-4.97657e-05 y=0.000329617 z=-4.83734e-06 kx=-0.000916658 ky=0.00082677 kz=22.4324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09603e-09 l2=5.06455e-06 x=-4.99359e-05 y=0.000278546 z=-2.53293e-06 kx=-4.99217e-05 ky=0.00177578 kz=23.2351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.17558e-09 l2=4.24958e-06 x=-4.99549e-05 y=0.000268707 z=-2.12823e-06 kx=-0.00039241 ky=0.000410576 kz=23.1725 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90143e-09 l2=1.35564e-05 x=4.95383e-05 y=0.000406473 z=-6.78082e-06 kx=0.00077886 ky=0.00122628 kz=23.1465 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.53881e-09 l2=5.30313e-06 x=-4.99298e-05 y=-0.000231879 z=-2.65113e-06 kx=0.000768188 ky=-0.00094432 kz=22.4388 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43185e-09 l2=2.40653e-05 x=4.8531e-05 y=0.000438183 z=-1.20323e-05 kx=-0.000514331 ky=0.000600261 kz=23.2154 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03594e-09 l2=2.50061e-05 x=4.84111e-05 y=-0.000365634 z=-1.25057e-05 kx=0.00100014 ky=0.000182769 kz=22.6568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.43257e-09 l2=1.04486e-05 x=4.97263e-05 y=-0.000342935 z=-5.22826e-06 kx=0.00103479 ky=0.000293094 kz=23.1174 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.61569e-09 l2=1.42514e-06 x=4.9995e-05 y=0.000159777 z=-7.14777e-07 kx=-0.000974975 ky=-0.000528244 kz=23.1948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79424e-09 l2=1.30805e-05 x=-4.95702e-05 y=-0.000294214 z=-6.5435e-06 kx=-0.00106373 ky=-0.000618808 kz=22.4014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.09516e-09 l2=1.30984e-06 x=4.99957e-05 y=0.000343655 z=-6.59782e-07 kx=0.00103947 ky=0.00129708 kz=22.4714 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48833e-09 l2=1.26287e-05 x=-4.95998e-05 y=-6.32358e-05 z=-6.31521e-06 kx=-5.96787e-05 ky=-0.00023542 kz=22.6261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10515e-09 l2=2.2794e-05 x=4.86835e-05 y=0.000382354 z=-1.13993e-05 kx=0.000790681 ky=0.000809425 kz=22.8145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71744e-09 l2=2.22844e-05 x=-4.87431e-05 y=0.000352165 z=-1.11423e-05 kx=0.000384377 ky=0.00147408 kz=22.8637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39158e-09 l2=1.77043e-05 x=4.92103e-05 y=-5.84839e-05 z=-8.85295e-06 kx=5.7178e-05 ky=-8.78982e-05 kz=22.6951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19927e-09 l2=1.33619e-05 x=4.95519e-05 y=-0.000301266 z=-6.67998e-06 kx=-0.000732316 ky=3.47969e-05 kz=23.0892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10221e-09 l2=1.08565e-05 x=4.97046e-05 y=-7.86974e-05 z=-5.4278e-06 kx=-0.000453185 ky=-0.000951999 kz=22.9799 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39792e-09 l2=5.42511e-06 x=4.99263e-05 y=0.000417466 z=-2.71496e-06 kx=0.000775867 ky=0.00181213 kz=22.6702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31122e-09 l2=1.25712e-05 x=4.96031e-05 y=0.000381279 z=-6.28893e-06 kx=0.00123525 ky=0.0010275 kz=22.8631 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03195e-09 l2=1.93159e-05 x=-4.90581e-05 y=-0.000249135 z=-9.66046e-06 kx=-0.000931061 ky=-0.000215154 kz=22.7351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50627e-09 l2=7.24338e-06 x=4.98687e-05 y=-3.36845e-05 z=-3.62241e-06 kx=-1.68084e-05 ky=-0.000457491 kz=22.6961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05033e-09 l2=2.48745e-05 x=-4.84281e-05 y=0.000143085 z=-1.24395e-05 kx=-0.000787965 ky=0.00136345 kz=22.3377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07187e-09 l2=3.10783e-05 x=4.75236e-05 y=0.000108305 z=-1.55414e-05 kx=0.000835558 ky=-0.00074008 kz=22.4182 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03321e-09 l2=3.56734e-05 x=4.67105e-05 y=0.000258945 z=-1.78372e-05 kx=-2.53712e-05 ky=0.000593971 kz=22.9081 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.065e-09 l2=9.80225e-06 x=-4.97591e-05 y=0.000456027 z=-4.90294e-06 kx=-0.000586796 ky=3.28674e-06 kz=22.7163 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15312e-09 l2=2.45462e-05 x=-4.84707e-05 y=1.61862e-06 z=-1.22728e-05 kx=0.00040986 ky=-0.00052287 kz=22.3065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02409e-09 l2=4.51184e-05 x=4.46216e-05 y=0.000219539 z=-2.25602e-05 kx=0.000237717 ky=0.000383647 kz=22.9923 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05292e-09 l2=1.20083e-05 x=4.96384e-05 y=-0.000494441 z=-6.00374e-06 kx=-0.000425729 ky=-0.00144599 kz=22.613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0979e-09 l2=1.84426e-05 x=4.9142e-05 y=-0.000421688 z=-9.22402e-06 kx=0.00101277 ky=-0.00194429 kz=23.0519 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20218e-09 l2=2.75865e-05 x=4.80593e-05 y=0.000357598 z=-1.37964e-05 kx=0.00119658 ky=0.00107654 kz=22.8234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23678e-09 l2=1.85645e-05 x=4.91309e-05 y=-0.000282838 z=-9.28293e-06 kx=3.35428e-05 ky=-0.00016152 kz=22.4141 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79505e-09 l2=7.70442e-06 x=4.98514e-05 y=0.000170685 z=-3.85429e-06 kx=0.000532193 ky=0.00110863 kz=22.3361 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69187e-09 l2=2.2841e-05 x=4.86787e-05 y=0.000461582 z=-1.14203e-05 kx=-0.000465631 ky=0.000543493 kz=22.9148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00527e-09 l2=1.84132e-05 x=-4.91454e-05 y=-1.80692e-05 z=-9.20566e-06 kx=0.000664812 ky=-0.000328614 kz=22.7933 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28424e-09 l2=1.80391e-05 x=-4.91801e-05 y=-0.000396529 z=-9.01918e-06 kx=0.000468082 ky=-0.0013562 kz=22.4678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66898e-09 l2=2.52492e-05 x=4.838e-05 y=0.000376324 z=-1.26259e-05 kx=0.000239987 ky=-2.38524e-05 kz=22.9082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71159e-09 l2=1.2529e-05 x=-4.9606e-05 y=0.000176543 z=-6.26622e-06 kx=-0.000390387 ky=-7.42331e-05 kz=22.4328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24276e-09 l2=2.0323e-05 x=4.8957e-05 y=0.000375369 z=-1.01606e-05 kx=-0.000693311 ky=0.00131632 kz=22.3487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14066e-09 l2=2.63848e-05 x=4.82286e-05 y=-0.000279167 z=-1.3192e-05 kx=-0.000459563 ky=-0.00036695 kz=22.8581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37138e-09 l2=1.98361e-05 x=-4.90067e-05 y=-0.000312262 z=-9.91821e-06 kx=0.000233154 ky=0.000419287 kz=22.5735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.52642e-09 l2=7.39043e-06 x=4.98634e-05 y=-0.000410579 z=-3.69615e-06 kx=-0.000150629 ky=-0.00034359 kz=22.8555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13534e-09 l2=1.29908e-05 x=-4.95766e-05 y=-6.5692e-05 z=-6.49456e-06 kx=0.000647518 ky=-0.00118979 kz=22.7437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46493e-09 l2=1.36256e-05 x=4.95335e-05 y=0.000341678 z=-6.81536e-06 kx=0.000844508 ky=9.46741e-05 kz=23.216 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00755e-09 l2=9.21644e-06 x=-4.97873e-05 y=-7.34482e-05 z=-4.60751e-06 kx=0.000559397 ky=-0.000216812 kz=23.0202 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.53192e-09 l2=6.86441e-06 x=-4.98821e-05 y=-5.14067e-05 z=-3.43413e-06 kx=-0.000300073 ky=-0.00021147 kz=22.6471 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48467e-09 l2=1.14665e-05 x=-4.96703e-05 y=-2.93251e-05 z=-5.73435e-06 kx=-0.000160617 ky=-0.00108931 kz=22.5312 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37851e-09 l2=1.36997e-05 x=-4.95288e-05 y=2.347e-05 z=-6.84923e-06 kx=0.000615625 ky=0.00105558 kz=22.9356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.1429e-09 l2=1.20567e-05 x=-4.96356e-05 y=0.00030205 z=-6.02845e-06 kx=0.000677193 ky=-0.000111066 kz=22.7746 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37397e-09 l2=2.4079e-05 x=-4.85287e-05 y=-0.000267509 z=-1.20417e-05 kx=-0.00071084 ky=0.000188935 kz=23.2163 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36647e-09 l2=4.03805e-06 x=-4.99592e-05 y=0.000454601 z=-2.02156e-06 kx=-0.000856232 ky=0.00174247 kz=23.0936 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00334e-09 l2=2.18903e-05 x=-4.87876e-05 y=0.000406436 z=-1.09451e-05 kx=0.000281387 ky=0.00192494 kz=23.199 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43888e-09 l2=1.96804e-05 x=4.90225e-05 y=-0.000224716 z=-9.83994e-06 kx=-0.000470123 ky=-0.000400833 kz=23.2985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0015e-09 l2=2.50273e-05 x=-4.84087e-05 y=0.000125223 z=-1.25148e-05 kx=-0.000279361 ky=-0.000730557 kz=23.1511 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14405e-09 l2=7.18428e-06 x=-4.98709e-05 y=0.000472542 z=-3.59254e-06 kx=0.000307042 ky=0.00166416 kz=22.8067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.19667e-09 l2=7.49884e-06 x=4.98594e-05 y=0.00037834 z=-3.74935e-06 kx=-0.00053382 ky=0.00137306 kz=22.8568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26079e-09 l2=1.47578e-05 x=-4.94529e-05 y=0.000203512 z=-7.37747e-06 kx=0.00096379 ky=0.00146662 kz=22.9087 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19001e-09 l2=2.91241e-05 x=4.78328e-05 y=9.59729e-05 z=-1.45622e-05 kx=-0.000215646 ky=-0.000590911 kz=22.7445 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21835e-09 l2=1.81465e-05 x=4.91699e-05 y=-0.000377074 z=-9.07434e-06 kx=0.000227052 ky=-0.001488 kz=22.8841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.41014e-09 l2=8.33064e-06 x=4.98263e-05 y=-0.000395499 z=-4.16683e-06 kx=0.000137557 ky=-0.00103 kz=22.8798 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.68705e-09 l2=7.9453e-06 x=4.98419e-05 y=-0.00033486 z=-3.97537e-06 kx=0.000629467 ky=-0.000840549 kz=22.8371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14333e-09 l2=1.66778e-05 x=4.93e-05 y=0.000401559 z=-8.33939e-06 kx=-0.000271165 ky=0.00172777 kz=22.7989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80483e-09 l2=1.91594e-05 x=-4.90734e-05 y=0.000429429 z=-9.58309e-06 kx=-0.00113854 ky=0.00190516 kz=22.4657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61699e-09 l2=1.39432e-05 x=-4.95119e-05 y=0.000301533 z=-6.97071e-06 kx=0.000793587 ky=-0.000113512 kz=23.2443 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01479e-09 l2=1.85198e-05 x=4.91348e-05 y=0.000211409 z=-9.26234e-06 kx=0.000882346 ky=-0.000602466 kz=22.7032 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29958e-09 l2=1.316e-05 x=4.95651e-05 y=0.000310495 z=-6.58142e-06 kx=0.000355489 ky=0.00123589 kz=22.3949 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.5973e-09 l2=4.34089e-06 x=-4.99529e-05 y=0.000473769 z=-2.17652e-06 kx=-0.00106255 ky=0.00161969 kz=23.276 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28873e-09 l2=2.04126e-05 x=4.89474e-05 y=0.000187547 z=-1.02065e-05 kx=-0.000179749 ky=0.000256726 kz=22.672 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27114e-09 l2=3.06828e-05 x=4.75889e-05 y=-4.855e-05 z=-1.53407e-05 kx=-0.000611812 ky=0.000551042 kz=22.8827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58505e-09 l2=1.33979e-05 x=-4.95491e-05 y=-7.07202e-05 z=-6.70167e-06 kx=-0.00088668 ky=0.00097824 kz=22.8178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3176e-09 l2=2.20193e-05 x=4.87729e-05 y=-0.000116501 z=-1.10105e-05 kx=6.67458e-05 ky=0.000588826 kz=22.995 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23786e-09 l2=2.57218e-05 x=4.83174e-05 y=2.66013e-06 z=-1.28631e-05 kx=0.000732002 ky=0.000449846 kz=22.759 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7567e-09 l2=1.64559e-05 x=4.93186e-05 y=0.000171003 z=-8.22818e-06 kx=-0.000293764 ky=0.000576287 kz=22.5872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88367e-09 l2=2.35301e-05 x=-4.85966e-05 y=0.000278949 z=-1.17649e-05 kx=0.0005221 ky=0.00162294 kz=22.3907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54593e-09 l2=2.07017e-05 x=-4.89169e-05 y=0.000259073 z=-1.0352e-05 kx=-0.000177245 ky=0.000624811 kz=22.9397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43346e-09 l2=2.0473e-05 x=-4.89408e-05 y=-1.83738e-05 z=-1.02385e-05 kx=-0.000574817 ky=-0.000944736 kz=22.381 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24906e-09 l2=2.04897e-05 x=-4.89391e-05 y=0.000172168 z=-1.02466e-05 kx=-0.000504449 ky=7.7087e-05 kz=22.9384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87559e-09 l2=1.30177e-05 x=4.95744e-05 y=0.000383521 z=-6.51214e-06 kx=0.00105072 ky=-0.000232269 kz=22.3946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68392e-09 l2=8.73018e-06 x=-4.98091e-05 y=0.000303515 z=-4.36724e-06 kx=-0.00060652 ky=0.000145493 kz=23.0592 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14441e-09 l2=1.83261e-05 x=-4.91533e-05 y=-0.000188953 z=-9.16353e-06 kx=5.53534e-05 ky=0.00054583 kz=22.5083 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1904e-09 l2=1.5914e-05 x=-4.93632e-05 y=-0.000228828 z=-7.95582e-06 kx=0.000798097 ky=0.000550162 kz=22.5079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.66553e-09 l2=4.65587e-06 x=-4.99458e-05 y=0.000140498 z=-2.3328e-06 kx=-0.00093613 ky=0.00141452 kz=23.0009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72013e-09 l2=1.20332e-05 x=4.96369e-05 y=-0.000285284 z=-6.01653e-06 kx=-0.000413774 ky=-0.00110142 kz=22.5651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47503e-09 l2=1.23768e-05 x=4.96155e-05 y=-0.000420676 z=-6.19048e-06 kx=0.000618772 ky=-3.14814e-05 kz=23.0288 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32308e-09 l2=3.45059e-05 x=-4.69298e-05 y=-0.000470033 z=-1.72522e-05 kx=0.000663448 ky=-0.000676551 kz=23.0274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.32909e-09 l2=1.07881e-05 x=-4.97085e-05 y=0.000468845 z=-5.39434e-06 kx=0.000614419 ky=0.00121764 kz=22.6733 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05593e-09 l2=3.29912e-05 x=4.72008e-05 y=-5.15395e-05 z=-1.6496e-05 kx=-6.19822e-05 ky=0.000659294 kz=22.3738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42511e-09 l2=5.55581e-06 x=-4.99227e-05 y=0.000442338 z=-2.78073e-06 kx=-0.00095712 ky=0.00195169 kz=22.6004 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20669e-09 l2=1.91991e-05 x=4.90698e-05 y=-8.40582e-05 z=-9.60107e-06 kx=0.000429713 ky=-0.000429701 kz=22.3636 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.31766e-09 l2=4.95085e-06 x=4.99388e-05 y=-0.000231794 z=-2.47635e-06 kx=-0.000341627 ky=-0.000277089 kz=23.1512 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20801e-09 l2=1.84271e-05 x=-4.91437e-05 y=0.0004654 z=-9.21529e-06 kx=-0.000525716 ky=0.00079755 kz=22.6646 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.27512e-09 l2=3.33809e-06 x=-4.99722e-05 y=-6.06778e-05 z=-1.67261e-06 kx=-0.000424185 ky=-0.000695159 kz=22.9333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61652e-09 l2=9.38475e-06 x=4.97793e-05 y=4.33328e-05 z=-4.69432e-06 kx=0.000511984 ky=0.000755512 kz=22.4446 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96943e-09 l2=1.78458e-05 x=-4.91977e-05 y=-0.000348879 z=-8.92314e-06 kx=0.000336338 ky=0.00030282 kz=22.8027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.00556e-09 l2=3.86058e-06 x=-4.99627e-05 y=-0.000361596 z=-1.93385e-06 kx=-0.000724956 ky=0.000304422 kz=23.1914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48543e-09 l2=1.70241e-05 x=-4.92704e-05 y=-3.31659e-05 z=-8.5122e-06 kx=0.000269309 ky=1.52886e-05 kz=22.4594 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18005e-09 l2=3.77517e-05 x=4.62997e-05 y=0.000253386 z=-1.88781e-05 kx=0.000824778 ky=-2.26977e-05 kz=23.2818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73874e-09 l2=1.05646e-05 x=4.97204e-05 y=5.02852e-05 z=-5.28187e-06 kx=-0.000586621 ky=-8.23837e-05 kz=22.4184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11008e-09 l2=1.22711e-05 x=4.96222e-05 y=-6.58907e-05 z=-6.13623e-06 kx=4.71128e-05 ky=0.000530269 kz=22.4838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53281e-09 l2=1.48997e-05 x=-4.9442e-05 y=0.000220186 z=-7.4508e-06 kx=-9.1525e-05 ky=-0.000613778 kz=22.6237 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51325e-09 l2=1.05173e-05 x=-4.97229e-05 y=-0.000164873 z=-5.25782e-06 kx=0.000730277 ky=0.000146066 kz=23.1476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30189e-08 l2=1.78244e-06 x=4.99922e-05 y=-0.000304373 z=-8.97921e-07 kx=8.96842e-05 ky=-0.00126039 kz=23.2743 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39866e-09 l2=2.4234e-05 x=4.85101e-05 y=-0.000299344 z=-1.21161e-05 kx=-0.000732776 ky=-0.00131194 kz=22.7237 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00472e-09 l2=1.75679e-05 x=4.92227e-05 y=-0.000439004 z=-8.78331e-06 kx=-0.00052433 ky=-0.00147543 kz=22.4913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12912e-09 l2=1.01659e-05 x=-4.9741e-05 y=-0.000112906 z=-5.08507e-06 kx=-0.000484513 ky=-0.000229255 kz=22.4286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57341e-09 l2=1.84643e-05 x=-4.914e-05 y=0.000486393 z=-9.2352e-06 kx=-0.00108351 ky=0.0015202 kz=23.2952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1111e-09 l2=2.86164e-05 x=4.79087e-05 y=0.000324473 z=-1.43104e-05 kx=0.000748431 ky=0.000338401 kz=22.3419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18137e-09 l2=4.12812e-05 x=4.55416e-05 y=0.000159233 z=-2.06401e-05 kx=-0.000543923 ky=-0.000508859 kz=23.2508 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.02819e-09 l2=7.10814e-06 x=4.98738e-05 y=0.000127492 z=-3.5536e-06 kx=-0.000912874 ky=-0.000584419 kz=23.0231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18894e-09 l2=1.59686e-05 x=-4.93586e-05 y=0.000230866 z=-7.98431e-06 kx=0.000276387 ky=-0.000369383 kz=23.0679 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23802e-09 l2=1.24308e-05 x=-4.96125e-05 y=-0.000426483 z=-6.21404e-06 kx=0.000933809 ky=-0.000927144 kz=23.2999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.58396e-09 l2=1.12579e-05 x=-4.96824e-05 y=0.000301714 z=-5.62986e-06 kx=0.000400934 ky=0.000102389 kz=22.7939 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24235e-09 l2=2.00935e-05 x=4.89805e-05 y=-0.000306603 z=-1.00465e-05 kx=-0.000413147 ky=-0.00153124 kz=22.875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40102e-09 l2=1.696e-05 x=4.92756e-05 y=-8.35016e-05 z=-8.48146e-06 kx=0.00034003 ky=0.000538021 kz=22.4904 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09066e-09 l2=3.60452e-05 x=-4.66392e-05 y=-0.000180086 z=-1.80229e-05 kx=0.000108108 ky=0.000278431 kz=22.9809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23498e-09 l2=2.30157e-05 x=-4.86574e-05 y=0.000315896 z=-1.15101e-05 kx=-0.000792673 ky=0.00137599 kz=23.2076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78904e-09 l2=1.23223e-05 x=-4.96193e-05 y=2.36682e-05 z=-6.15982e-06 kx=0.00101063 ky=3.76327e-07 kz=22.6022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87977e-09 l2=1.19857e-05 x=4.96394e-05 y=0.000417301 z=-5.99587e-06 kx=0.000974144 ky=0.000664153 kz=23.2889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15665e-09 l2=1.39789e-05 x=4.95094e-05 y=0.000317701 z=-6.98907e-06 kx=-0.000662114 ky=0.00017516 kz=22.694 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91354e-09 l2=1.68259e-05 x=-4.9287e-05 y=-0.000348938 z=-8.41576e-06 kx=-0.000852481 ky=-5.97799e-05 kz=22.4137 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74901e-09 l2=2.04446e-05 x=-4.89442e-05 y=0.000430616 z=-1.02226e-05 kx=0.000260404 ky=0.000197766 kz=22.8395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32444e-09 l2=2.02472e-05 x=-4.89643e-05 y=0.00030263 z=-1.01254e-05 kx=-0.000545461 ky=0.000280632 kz=22.579 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60876e-09 l2=1.51e-05 x=-4.9427e-05 y=6.94326e-05 z=-7.54964e-06 kx=0.000529111 ky=0.000524064 kz=22.8071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0685e-09 l2=2.61908e-05 x=4.82549e-05 y=-0.000460127 z=-1.30955e-05 kx=-0.000218862 ky=-0.00111717 kz=23.0422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25436e-09 l2=1.64056e-05 x=4.93223e-05 y=-0.000489644 z=-8.20654e-06 kx=0.00119144 ky=-0.000510496 kz=22.6676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30806e-09 l2=1.98927e-05 x=-4.90009e-05 y=-2.15698e-05 z=-9.94664e-06 kx=0.000175874 ky=1.01513e-05 kz=23.2644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11098e-09 l2=1.02262e-05 x=-4.9738e-05 y=0.000383891 z=-5.11326e-06 kx=0.00018574 ky=0.00201734 kz=23.2275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74124e-09 l2=9.16016e-06 x=-4.979e-05 y=0.000295322 z=-4.57925e-06 kx=0.000774361 ky=0.000149975 kz=22.7062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.07686e-09 l2=3.25387e-06 x=-4.99736e-05 y=0.000196599 z=-1.62926e-06 kx=-0.000127199 ky=0.00113966 kz=22.7044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91288e-09 l2=2.54361e-05 x=-4.83559e-05 y=-0.000110468 z=-1.27184e-05 kx=0.000277197 ky=0.000364742 kz=23.0549 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12853e-09 l2=1.83342e-05 x=-4.91527e-05 y=-7.16514e-05 z=-9.16718e-06 kx=0.000221655 ky=-1.07441e-05 kz=22.4869 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31516e-09 l2=2.48005e-05 x=4.84376e-05 y=-7.3795e-05 z=-1.2403e-05 kx=0.000977501 ky=-0.000431797 kz=22.6311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0237e-09 l2=1.1001e-05 x=-4.96967e-05 y=0.000235706 z=-5.49949e-06 kx=0.00068477 ky=0.0001169 kz=22.5879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.69509e-09 l2=9.28024e-06 x=4.97842e-05 y=-0.000321187 z=-4.64331e-06 kx=0.000830571 ky=-0.00108636 kz=22.4779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12081e-09 l2=1.61591e-05 x=4.93429e-05 y=-7.92371e-05 z=-8.08041e-06 kx=0.000135071 ky=0.000452623 kz=22.5553 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30385e-09 l2=5.95326e-06 x=-4.99115e-05 y=-0.000282835 z=-2.97509e-06 kx=0.000998998 ky=-0.000870895 kz=22.7041 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11713e-09 l2=1.60995e-05 x=4.93475e-05 y=0.000380677 z=-8.05251e-06 kx=0.00103388 ky=0.00149903 kz=23.248 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03318e-09 l2=1.33411e-05 x=-4.95529e-05 y=0.000258642 z=-6.67373e-06 kx=-0.000985809 ky=0.00113906 kz=22.6883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.81741e-09 l2=3.07606e-06 x=4.99763e-05 y=0.000303922 z=-1.5409e-06 kx=0.000659782 ky=0.0012834 kz=22.5755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57153e-09 l2=5.70509e-06 x=-4.99185e-05 y=-3.67102e-05 z=-2.85494e-06 kx=-0.000726849 ky=0.000759267 kz=22.5897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04872e-09 l2=1.0244e-05 x=4.97371e-05 y=0.000479714 z=-5.12135e-06 kx=-0.000528377 ky=0.000358655 kz=22.4522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.66724e-09 l2=1.12766e-05 x=4.96812e-05 y=-0.000336466 z=-5.63993e-06 kx=0.000129037 ky=-0.00083916 kz=22.8181 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09602e-09 l2=8.33852e-06 x=4.98258e-05 y=-0.000211374 z=-4.17178e-06 kx=0.00091241 ky=-9.56068e-05 kz=23.0804 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.57185e-09 l2=8.58873e-06 x=-4.98154e-05 y=-0.00034387 z=-4.29695e-06 kx=-0.000139878 ky=8.45188e-05 kz=23.058 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33149e-09 l2=9.38784e-06 x=-4.97791e-05 y=2.9976e-05 z=-4.69763e-06 kx=-0.00114257 ky=0.000936627 kz=22.384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.432e-09 l2=2.16166e-05 x=-4.88177e-05 y=0.000287088 z=-1.08103e-05 kx=-0.000636629 ky=0.000673787 kz=23.0575 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52262e-09 l2=1.05392e-05 x=4.97217e-05 y=-0.000202515 z=-5.2692e-06 kx=-0.000521834 ky=-0.00118404 kz=22.8257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36759e-09 l2=1.16687e-05 x=4.96582e-05 y=0.000493897 z=-5.83768e-06 kx=0.00118845 ky=0.00203062 kz=22.4572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55857e-09 l2=4.44651e-06 x=-4.99505e-05 y=4.22275e-05 z=-2.2253e-06 kx=-0.000566985 ky=0.000607326 kz=22.3307 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16816e-09 l2=1.57803e-05 x=-4.9374e-05 y=0.000264118 z=-7.88851e-06 kx=0.00100059 ky=0.000178592 kz=22.3039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.079e-09 l2=1.82405e-05 x=4.91608e-05 y=0.000329896 z=-9.12342e-06 kx=0.00121228 ky=3.49129e-05 kz=22.7356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03673e-09 l2=1.71959e-05 x=-4.92555e-05 y=0.000105977 z=-8.59704e-06 kx=0.000672491 ky=0.00134547 kz=22.9242 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98006e-09 l2=4.89169e-06 x=-4.99402e-05 y=-0.000125104 z=-2.44794e-06 kx=-0.000281816 ky=-0.000803923 kz=23.0405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76435e-09 l2=1.41395e-05 x=-4.9498e-05 y=5.67656e-05 z=-7.06884e-06 kx=0.00082182 ky=8.35272e-05 kz=22.8833 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31536e-09 l2=1.20708e-05 x=-4.96343e-05 y=-0.000112371 z=-6.03756e-06 kx=-0.00068919 ky=-0.000751147 kz=23.1257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92769e-09 l2=2.01613e-05 x=4.8973e-05 y=-0.000107136 z=-1.00839e-05 kx=0.00105846 ky=-0.000863239 kz=22.8161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85268e-09 l2=9.24135e-06 x=-4.97862e-05 y=0.000406127 z=-4.6213e-06 kx=0.000370242 ky=0.00105875 kz=22.8495 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4e-09 l2=1.74549e-05 x=-4.92326e-05 y=0.000464127 z=-8.72788e-06 kx=0.000110681 ky=0.000582574 kz=22.5456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7093e-09 l2=1.52543e-05 x=4.94148e-05 y=0.000333256 z=-7.62891e-06 kx=0.000423891 ky=0.00072919 kz=23.1505 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89004e-09 l2=1.33068e-05 x=4.95555e-05 y=0.000470556 z=-6.65443e-06 kx=4.75341e-05 ky=0.00201368 kz=22.3794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2081e-09 l2=2.03531e-05 x=4.89539e-05 y=4.59018e-05 z=-1.01755e-05 kx=-0.000790967 ky=0.00100612 kz=22.7197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02884e-09 l2=1.44574e-05 x=4.94747e-05 y=0.00037372 z=-7.22951e-06 kx=0.000134716 ky=0.00154839 kz=22.9464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.31646e-09 l2=7.90929e-06 x=4.98433e-05 y=0.000407596 z=-3.95762e-06 kx=0.000842653 ky=1.40477e-05 kz=23.0936 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22741e-09 l2=1.05239e-05 x=4.97225e-05 y=0.000455585 z=-5.26158e-06 kx=-0.000438548 ky=0.000216172 kz=22.4302 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72549e-09 l2=1.47357e-05 x=4.94541e-05 y=-0.000350414 z=-7.3697e-06 kx=0.00046586 ky=0.0001568 kz=22.8869 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08195e-09 l2=1.98965e-05 x=-4.90008e-05 y=-1.49707e-05 z=-9.94705e-06 kx=0.000802607 ky=-0.000976105 kz=22.3939 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41511e-09 l2=1.49485e-05 x=4.94385e-05 y=-0.000256942 z=-7.47376e-06 kx=-0.000544813 ky=-0.000162216 kz=22.3848 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30721e-09 l2=2.5938e-05 x=-4.82891e-05 y=-0.00014711 z=-1.29689e-05 kx=0.000373736 ky=-0.00109647 kz=23.2126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55351e-09 l2=8.8073e-06 x=4.98057e-05 y=-4.23641e-05 z=-4.40544e-06 kx=0.000460822 ky=-0.000189755 kz=22.5437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.76403e-09 l2=6.93882e-07 x=-4.99988e-05 y=0.000463661 z=-3.48066e-07 kx=0.000351367 ky=0.00115954 kz=23.1986 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.31077e-09 l2=4.93226e-06 x=-4.99391e-05 y=3.46233e-05 z=-2.46958e-06 kx=-0.00083902 ky=0.000406731 kz=23.2898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32951e-09 l2=7.37981e-06 x=4.98637e-05 y=7.24678e-05 z=-3.69217e-06 kx=0.000510341 ky=0.00110907 kz=23.0518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36747e-09 l2=2.84985e-05 x=4.79262e-05 y=-0.000162581 z=-1.42519e-05 kx=0.000919482 ky=-0.000410815 kz=22.9738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08134e-09 l2=1.78818e-05 x=-4.91946e-05 y=-0.000225577 z=-8.93939e-06 kx=0.000947351 ky=-0.00124211 kz=22.4437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01387e-09 l2=2.06986e-05 x=-4.89167e-05 y=-1.5135e-05 z=-1.03525e-05 kx=-0.00120146 ky=0.000594331 kz=22.3331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43782e-09 l2=1.01133e-05 x=4.97437e-05 y=0.000333786 z=-5.059e-06 kx=0.000511229 ky=0.00165051 kz=22.9693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83167e-09 l2=8.4107e-06 x=-4.98229e-05 y=-4.59319e-06 z=-4.20635e-06 kx=-3.78575e-05 ky=0.000646308 kz=23.175 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.45338e-09 l2=6.64747e-06 x=-4.98897e-05 y=0.000148587 z=-3.32419e-06 kx=0.0008067 ky=2.23801e-06 kz=22.6939 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22579e-09 l2=1.21661e-05 x=4.96288e-05 y=-0.000144747 z=-6.08238e-06 kx=-0.000578562 ky=-0.000918276 kz=22.3546 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82096e-09 l2=8.91213e-06 x=-4.98011e-05 y=-1.43744e-05 z=-4.45854e-06 kx=-0.000477467 ky=-0.00105902 kz=22.4147 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29254e-09 l2=1.76573e-05 x=-4.92147e-05 y=0.000238059 z=-8.82811e-06 kx=0.000547118 ky=0.000725112 kz=22.9353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16283e-09 l2=1.97103e-05 x=4.90196e-05 y=0.000474029 z=-9.85423e-06 kx=-0.000712184 ky=0.00209754 kz=22.8296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65823e-09 l2=1.05131e-05 x=-4.97231e-05 y=-0.00023302 z=-5.25633e-06 kx=0.000469753 ky=-0.000945064 kz=22.5809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.76404e-09 l2=3.28337e-06 x=-4.99731e-05 y=0.000474694 z=-1.64602e-06 kx=-0.000653358 ky=0.000413441 kz=22.4891 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.47541e-09 l2=8.87054e-06 x=4.98031e-05 y=0.00020506 z=-4.43598e-06 kx=-0.000472608 ky=1.25426e-05 kz=23.0293 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.37645e-09 l2=6.47564e-06 x=-4.98952e-05 y=-3.19588e-05 z=-3.23809e-06 kx=0.000419873 ky=-0.00110462 kz=22.8827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25543e-09 l2=1.25885e-05 x=4.96021e-05 y=0.00015132 z=-6.29663e-06 kx=0.000793684 ky=-0.00056914 kz=22.6298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.17661e-09 l2=3.49996e-06 x=4.99696e-05 y=-0.000314823 z=-1.75228e-06 kx=-0.000820893 ky=-0.00170529 kz=22.9642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20638e-09 l2=3.06727e-05 x=4.75906e-05 y=0.000445722 z=-1.53354e-05 kx=-0.00072352 ky=0.0019982 kz=22.705 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16852e-09 l2=2.70662e-05 x=-4.81341e-05 y=0.000460783 z=-1.35331e-05 kx=0.000303044 ky=0.000107931 kz=23.1688 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86654e-09 l2=1.65611e-05 x=-4.93094e-05 y=-0.000196229 z=-8.28327e-06 kx=-0.000839971 ky=0.000123234 kz=23.1921 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21195e-09 l2=1.34277e-05 x=4.95474e-05 y=0.000435011 z=-6.71342e-06 kx=-0.000476908 ky=0.000729278 kz=22.7608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.36533e-09 l2=7.33517e-06 x=4.98655e-05 y=0.000486862 z=-3.66857e-06 kx=-0.000325625 ky=4.84627e-05 kz=23.2004 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04357e-09 l2=9.74809e-06 x=4.97618e-05 y=0.000160794 z=-4.87566e-06 kx=0.000492723 ky=0.00023745 kz=22.3684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16368e-09 l2=1.59146e-05 x=4.93627e-05 y=1.31642e-05 z=-7.95885e-06 kx=0.000441071 ky=-0.000394606 kz=22.9993 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61503e-09 l2=2.24616e-05 x=-4.87222e-05 y=-0.000322862 z=-1.12333e-05 kx=-0.000809432 ky=0.00016515 kz=23.3068 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.8687e-09 l2=2.34616e-05 x=4.86043e-05 y=2.24336e-05 z=-1.17331e-05 kx=0.000644703 ky=-0.000580018 kz=22.66 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.50469e-09 l2=1.48624e-05 x=4.94448e-05 y=0.000284867 z=-7.43322e-06 kx=0.00035293 ky=0.000937127 kz=22.8179 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.47835e-09 l2=6.7881e-06 x=-4.98846e-05 y=0.000291032 z=-3.39791e-06 kx=-0.00098371 ky=0.000585801 kz=23.0768 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36689e-09 l2=1.91666e-05 x=-4.90734e-05 y=0.000162029 z=-9.58274e-06 kx=0.000568976 ky=0.0014885 kz=22.6877 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.57054e-09 l2=7.02419e-06 x=-4.98766e-05 y=-0.000291485 z=-3.5146e-06 kx=-0.000333959 ky=-0.00119301 kz=22.9523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04953e-09 l2=2.8836e-05 x=-4.7876e-05 y=0.000368504 z=-1.44194e-05 kx=-0.000388652 ky=5.05546e-05 kz=22.7614 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20217e-09 l2=2.13791e-05 x=-4.88444e-05 y=0.000261999 z=-1.0689e-05 kx=0.000537485 ky=0.000251631 kz=22.7275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01871e-09 l2=1.51481e-05 x=4.94227e-05 y=0.000136494 z=-7.57723e-06 kx=0.00120764 ky=8.03218e-05 kz=22.3274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11096e-09 l2=3.38511e-05 x=4.70483e-05 y=-0.000127763 z=-1.69261e-05 kx=8.02942e-06 ky=0.000487683 kz=22.434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44542e-09 l2=7.10231e-06 x=4.98738e-05 y=-0.000168118 z=-3.5514e-06 kx=-0.00021859 ky=0.000742604 kz=22.9091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22851e-09 l2=2.3042e-05 x=-4.86551e-05 y=0.000149285 z=-1.15199e-05 kx=0.000799965 ky=-0.000132044 kz=23.1881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08219e-09 l2=3.25737e-05 x=-4.72737e-05 y=-0.000109196 z=-1.6286e-05 kx=0.000656616 ky=-0.000509556 kz=22.626 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68435e-09 l2=9.88383e-06 x=4.97554e-05 y=6.6865e-06 z=-4.94108e-06 kx=-0.000757157 ky=-0.000419816 kz=22.4811 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65438e-09 l2=1.24812e-05 x=-4.96091e-05 y=-0.000413285 z=-6.24145e-06 kx=-2.20899e-05 ky=-0.00188209 kz=22.4899 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33517e-09 l2=1.65667e-05 x=4.93089e-05 y=0.000255401 z=-8.28687e-06 kx=0.00106316 ky=-2.29522e-05 kz=22.362 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27197e-09 l2=2.51978e-05 x=-4.83866e-05 y=-0.000488245 z=-1.26003e-05 kx=-0.000345935 ky=-0.00139986 kz=22.9971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00711e-09 l2=3.99016e-05 x=-4.58476e-05 y=-0.000193493 z=-1.99508e-05 kx=0.000224208 ky=0.000577047 kz=22.4483 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.51368e-09 l2=1.36751e-05 x=-4.95302e-05 y=-0.000493243 z=-6.84084e-06 kx=-0.000950789 ky=-0.0013993 kz=23.1874 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01083e-09 l2=2.40952e-05 x=-4.85266e-05 y=-0.000429696 z=-1.20498e-05 kx=-0.000793729 ky=-0.00129878 kz=22.5192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.6117e-09 l2=5.2764e-06 x=4.99306e-05 y=-0.000289325 z=-2.63847e-06 kx=-0.000948031 ky=-0.00132383 kz=23.2275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3845e-09 l2=1.57735e-05 x=4.93743e-05 y=-0.000453591 z=-7.88679e-06 kx=-0.000288855 ky=-0.00151415 kz=22.436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02214e-09 l2=2.13957e-05 x=-4.88424e-05 y=0.000461713 z=-1.06976e-05 kx=0.000365775 ky=0.000697236 kz=22.5879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03005e-09 l2=2.1219e-05 x=-4.88615e-05 y=-0.000491957 z=-1.06103e-05 kx=-0.000115605 ky=-0.00113162 kz=22.368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.94886e-09 l2=1.21645e-05 x=-4.96289e-05 y=-0.00024509 z=-6.08314e-06 kx=0.000271351 ky=-0.00127848 kz=22.3192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.64821e-09 l2=2.64007e-06 x=-4.99827e-05 y=9.15407e-05 z=-1.32287e-06 kx=0.000229138 ky=0.00111035 kz=23.2402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42398e-09 l2=1.14665e-05 x=-4.96704e-05 y=-2.14655e-05 z=-5.73319e-06 kx=0.000347716 ky=-0.000528675 kz=22.9354 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14844e-09 l2=5.91827e-06 x=4.99124e-05 y=-7.00269e-05 z=-2.96085e-06 kx=0.000297621 ky=-0.000494777 kz=23.1062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14461e-09 l2=2.21742e-05 x=-4.87549e-05 y=-0.000434198 z=-1.109e-05 kx=-0.00110428 ky=-0.000979202 kz=22.9355 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12424e-09 l2=3.14104e-05 x=-4.74696e-05 y=-0.000222821 z=-1.57058e-05 kx=-6.71224e-06 ky=0.000161939 kz=22.9305 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04346e-09 l2=1.79635e-05 x=-4.91871e-05 y=-0.000351067 z=-8.98068e-06 kx=0.000720284 ky=-0.000500041 kz=22.6226 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23478e-09 l2=7.92069e-06 x=-4.9843e-05 y=0.000476846 z=-3.96115e-06 kx=0.000138282 ky=0.00181441 kz=22.4597 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29853e-09 l2=1.74023e-05 x=4.92376e-05 y=0.000176866 z=-8.69967e-06 kx=-0.00101192 ky=0.00142776 kz=23.3084 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.62368e-09 l2=6.75274e-06 x=-4.9886e-05 y=-0.000241737 z=-3.37941e-06 kx=-0.000329095 ky=-0.000985633 kz=22.7076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10636e-09 l2=1.8952e-05 x=4.90935e-05 y=0.000140609 z=-9.47966e-06 kx=0.00121333 ky=0.000575754 kz=22.7664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25176e-09 l2=2.1452e-05 x=4.88364e-05 y=9.69348e-06 z=-1.07255e-05 kx=-0.000543293 ky=-0.00082931 kz=23.0309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.72178e-09 l2=1.40007e-06 x=4.99951e-05 y=-0.000457846 z=-7.03813e-07 kx=0.00108328 ky=-0.000222205 kz=22.4244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06876e-09 l2=1.38654e-05 x=4.95168e-05 y=-0.000366478 z=-6.93542e-06 kx=0.000981794 ky=-0.000569988 kz=22.3629 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20245e-09 l2=1.92328e-05 x=4.90664e-05 y=0.000222535 z=-9.61851e-06 kx=0.000698497 ky=0.0014485 kz=22.6341 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04211e-09 l2=1.62216e-05 x=-4.93377e-05 y=0.000108661 z=-8.1125e-06 kx=-0.000537282 ky=0.000216834 kz=22.3451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90757e-09 l2=7.08776e-06 x=-4.98742e-05 y=-0.000485339 z=-3.54636e-06 kx=-0.000691868 ky=-0.00219477 kz=22.6115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52801e-09 l2=1.73992e-05 x=-4.92372e-05 y=-0.000438934 z=-8.70177e-06 kx=-0.000649284 ky=-0.000567678 kz=22.8732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.30825e-09 l2=9.93391e-06 x=4.9753e-05 y=-0.000231364 z=-4.96729e-06 kx=-0.000591629 ky=0.000149724 kz=22.3377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56034e-09 l2=1.64042e-05 x=4.93225e-05 y=-0.000312294 z=-8.20471e-06 kx=0.000864437 ky=-0.0012558 kz=23.2103 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08291e-09 l2=1.74735e-05 x=-4.92308e-05 y=-0.000408912 z=-8.73766e-06 kx=-0.000175658 ky=-0.000491918 kz=22.8288 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1084e-09 l2=3.38702e-05 x=-4.70444e-05 y=0.000178865 z=-1.69369e-05 kx=-0.00061259 ky=0.00152417 kz=22.6689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17593e-09 l2=1.81902e-05 x=-4.91656e-05 y=-3.84921e-05 z=-9.09755e-06 kx=-0.00085686 ky=-0.000612358 kz=22.8522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26755e-09 l2=3.04331e-05 x=4.76289e-05 y=0.000210872 z=-1.5216e-05 kx=-0.000568517 ky=-7.43812e-05 kz=23.2035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32309e-09 l2=8.32932e-06 x=-4.98264e-05 y=-0.000299773 z=-4.16495e-06 kx=0.000406699 ky=-0.00160989 kz=23.2562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07982e-09 l2=1.20459e-05 x=4.9636e-05 y=-1.43651e-05 z=-6.02356e-06 kx=3.48545e-05 ky=-0.000752552 kz=22.9086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.66524e-09 l2=3.79127e-06 x=-4.99642e-05 y=0.000276537 z=-1.89972e-06 kx=-0.000349181 ky=0.00141441 kz=23.2972 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0673e-09 l2=8.49494e-06 x=-4.98193e-05 y=0.000319639 z=-4.24903e-06 kx=-0.000235792 ky=0.0005896 kz=22.3122 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10974e-09 l2=2.09904e-05 x=4.88857e-05 y=-0.000170386 z=-1.04982e-05 kx=0.00114489 ky=-0.000200899 kz=22.3855 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.5336e-09 l2=9.11589e-06 x=-4.97917e-05 y=-0.000111156 z=-4.56147e-06 kx=-0.00101625 ky=-0.000843745 kz=22.451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29105e-09 l2=9.03911e-06 x=-4.97953e-05 y=0.000458725 z=-4.52068e-06 kx=-0.000219588 ky=0.000562028 kz=22.5897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52538e-09 l2=1.09846e-05 x=-4.96973e-05 y=-0.000117812 z=-5.49491e-06 kx=-0.000842537 ky=-0.000987636 kz=22.5992 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15409e-09 l2=1.58793e-05 x=4.93656e-05 y=0.000114472 z=-7.94077e-06 kx=0.000256801 ky=-0.000200466 kz=22.3593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.036e-09 l2=1.88124e-05 x=4.91077e-05 y=-0.000170834 z=-9.40516e-06 kx=-0.000706907 ky=0.000135093 kz=22.4034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00261e-09 l2=2.39205e-05 x=-4.85482e-05 y=-0.000390473 z=-1.19621e-05 kx=-0.000656247 ky=-0.00119817 kz=22.5938 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.19981e-09 l2=1.56287e-05 x=4.93856e-05 y=-0.00017327 z=-7.81657e-06 kx=0.000530244 ky=-0.000824092 kz=23.0442 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43245e-09 l2=1.88163e-05 x=4.91066e-05 y=-0.000249458 z=-9.41103e-06 kx=0.00100912 ky=-0.000367981 kz=23.1116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35491e-09 l2=2.09143e-05 x=4.88939e-05 y=0.000231713 z=-1.04603e-05 kx=0.00114689 ky=6.86324e-06 kz=22.7346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42053e-09 l2=1.1435e-05 x=-4.96719e-05 y=0.000413059 z=-5.71962e-06 kx=-0.000653123 ky=-0.000185003 kz=23.1432 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45843e-09 l2=5.72208e-06 x=4.99182e-05 y=0.000419408 z=-2.86112e-06 kx=-0.000293718 ky=0.00164127 kz=22.6608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37909e-09 l2=1.93955e-05 x=-4.90504e-05 y=0.000165512 z=-9.69976e-06 kx=-0.000612722 ky=0.00147864 kz=22.7215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26395e-09 l2=1.60562e-05 x=4.93509e-05 y=-0.00043061 z=-8.03144e-06 kx=0.0012662 ky=-0.000400474 kz=23.2571 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28729e-09 l2=1.68098e-05 x=-4.92889e-05 y=-1.99361e-05 z=-8.40407e-06 kx=0.000679158 ky=0.000218147 kz=23.0295 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63057e-09 l2=9.46285e-06 x=-4.97758e-05 y=-3.80539e-05 z=-4.73199e-06 kx=0.000340584 ky=0.00053415 kz=22.619 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12159e-09 l2=1.36405e-05 x=4.95327e-05 y=0.000362412 z=-6.82223e-06 kx=0.000437429 ky=0.000405407 kz=23.2872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.72842e-09 l2=2.80509e-06 x=-4.99804e-05 y=0.00025948 z=-1.40259e-06 kx=0.000606312 ky=0.000771011 kz=22.8955 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02054e-09 l2=2.10968e-05 x=-4.88744e-05 y=0.000176204 z=-1.05507e-05 kx=-0.000862004 ky=0.0006139 kz=23.0927 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57756e-09 l2=2.11731e-05 x=4.88667e-05 y=0.000466039 z=-1.05868e-05 kx=-0.000232443 ky=0.000269969 kz=22.8206 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24326e-09 l2=2.67216e-05 x=-4.81824e-05 y=-8.66132e-05 z=-1.336e-05 kx=0.0006764 ky=-0.000290216 kz=23.0664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59324e-09 l2=1.39328e-05 x=4.95122e-05 y=-0.000428554 z=-6.96853e-06 kx=0.000614191 ky=-0.000833883 kz=22.8127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13187e-09 l2=1.48108e-05 x=4.94488e-05 y=0.000499991 z=-7.40513e-06 kx=-0.000398796 ky=0.000514016 kz=23.1013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52598e-09 l2=1.02125e-05 x=4.97386e-05 y=-0.00035708 z=-5.1076e-06 kx=0.000272718 ky=0.000227768 kz=23.1374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10101e-09 l2=1.69423e-05 x=4.92768e-05 y=-0.000455585 z=-8.47434e-06 kx=0.00119669 ky=-0.00023627 kz=22.3834 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49406e-09 l2=1.85803e-05 x=-4.91296e-05 y=-0.00016597 z=-9.29018e-06 kx=0.000319368 ky=0.000499882 kz=22.4606 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25167e-09 l2=1.87582e-05 x=-4.91129e-05 y=-0.000277073 z=-9.37821e-06 kx=0.000706654 ky=-0.000550956 kz=23.0726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0706e-09 l2=9.43374e-06 x=4.97772e-05 y=-0.00025837 z=-4.71557e-06 kx=-0.000847612 ky=-0.000487127 kz=22.9788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.76606e-09 l2=1.16085e-06 x=4.99967e-05 y=0.000190237 z=-5.80291e-07 kx=-0.000933758 ky=0.00150588 kz=23.1613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36843e-09 l2=2.25673e-05 x=4.87106e-05 y=-0.000493384 z=-1.1283e-05 kx=-0.000641515 ky=-0.000562039 kz=23.0496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21457e-09 l2=1.36379e-05 x=-4.95331e-05 y=-0.000230698 z=-6.81854e-06 kx=0.000468172 ky=-0.000801986 kz=22.5213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05275e-09 l2=2.62921e-05 x=-4.82411e-05 y=-7.39801e-05 z=-1.31462e-05 kx=0.000185565 ky=-0.000716807 kz=22.3051 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03137e-09 l2=6.96537e-06 x=4.98785e-05 y=-5.56186e-05 z=-3.48609e-06 kx=0.0010892 ky=-0.000749185 kz=22.7067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78762e-09 l2=1.2516e-05 x=-4.96067e-05 y=0.000302156 z=-6.26084e-06 kx=-0.000891209 ky=0.00181243 kz=22.9144 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27012e-09 l2=1.73898e-05 x=4.92383e-05 y=0.000245009 z=-8.69538e-06 kx=-8.50155e-05 ky=0.0013693 kz=22.9299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83584e-09 l2=1.15786e-05 x=4.96635e-05 y=-0.000107646 z=-5.79261e-06 kx=0.00110466 ky=-0.000651295 kz=23.115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27266e-09 l2=2.08747e-05 x=4.88983e-05 y=-0.000489951 z=-1.04393e-05 kx=0.000590548 ky=-0.00023149 kz=22.9791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67358e-09 l2=1.14929e-05 x=-4.96688e-05 y=-0.000123836 z=-5.74681e-06 kx=0.00023067 ky=0.00051963 kz=22.7517 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0603e-09 l2=1.97081e-05 x=-4.90189e-05 y=0.000361764 z=-9.85722e-06 kx=-0.00121848 ky=0.00101892 kz=22.5915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68515e-09 l2=1.62823e-05 x=4.93327e-05 y=0.000295522 z=-8.14296e-06 kx=0.000448057 ky=0.000482382 kz=22.9217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09984e-09 l2=2.69593e-05 x=4.81492e-05 y=8.1263e-06 z=-1.3479e-05 kx=-0.000532262 ky=-0.000382339 kz=22.4916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03362e-09 l2=2.35544e-05 x=4.85932e-05 y=0.000108706 z=-1.17782e-05 kx=0.000245392 ky=0.00127982 kz=22.9472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04643e-09 l2=1.50067e-05 x=-4.94336e-05 y=4.01127e-05 z=-7.50555e-06 kx=-0.000772356 ky=0.000684735 kz=23.1542 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74128e-09 l2=1.11036e-05 x=-4.96912e-05 y=6.15999e-05 z=-5.55043e-06 kx=0.00103493 ky=0.000379997 kz=23.0889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36056e-09 l2=1.74183e-05 x=4.92361e-05 y=-0.000428941 z=-8.7082e-06 kx=-0.000768368 ky=-0.00208548 kz=23.3014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35047e-09 l2=1.84262e-05 x=4.91438e-05 y=-0.000257215 z=-9.21482e-06 kx=0.000482529 ky=-0.000293678 kz=22.6693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04214e-09 l2=2.11729e-05 x=4.88667e-05 y=0.000146594 z=-1.05864e-05 kx=-0.000246778 ky=0.000222801 kz=23.0225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26773e-09 l2=2.64108e-05 x=4.82245e-05 y=-8.12778e-05 z=-1.32072e-05 kx=0.000551224 ky=-0.000660795 kz=22.6741 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62774e-09 l2=1.55139e-05 x=4.93946e-05 y=0.000392214 z=-7.75854e-06 kx=0.000358766 ky=0.000663866 kz=23.0404 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43701e-09 l2=1.28106e-05 x=-4.95881e-05 y=-6.92034e-05 z=-6.406e-06 kx=1.16573e-05 ky=0.000291288 kz=22.4988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13428e-09 l2=1.14249e-05 x=4.96729e-05 y=-8.68749e-05 z=-5.71101e-06 kx=-0.00092039 ky=0.000263097 kz=22.7662 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02638e-09 l2=2.16179e-05 x=-4.88173e-05 y=-0.000485236 z=-1.08119e-05 kx=-0.00111916 ky=-0.00219203 kz=22.7424 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66122e-09 l2=7.12388e-06 x=-4.98729e-05 y=0.000370085 z=-3.56456e-06 kx=-0.000830929 ky=0.000345798 kz=23.2125 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04217e-09 l2=3.49611e-05 x=4.68441e-05 y=-0.000197807 z=-1.74833e-05 kx=0.00106389 ky=0.000168179 kz=22.9555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18337e-09 l2=3.46165e-05 x=-4.69084e-05 y=0.000191479 z=-1.73101e-05 kx=-0.000625172 ky=0.000659309 kz=23.3077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30292e-09 l2=1.44852e-05 x=-4.9473e-05 y=0.000414524 z=-7.24154e-06 kx=0.000782685 ky=0.00107269 kz=22.6033 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62431e-09 l2=7.85816e-06 x=4.98455e-05 y=-0.000122026 z=-3.93056e-06 kx=7.67652e-05 ky=-0.00122998 kz=22.5225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45018e-09 l2=5.84037e-06 x=4.99146e-05 y=-0.000171896 z=-2.92267e-06 kx=0.000790572 ky=-0.000111275 kz=22.4502 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26639e-09 l2=2.86076e-05 x=4.79101e-05 y=-0.000369067 z=-1.43059e-05 kx=0.000708764 ky=-0.00123621 kz=22.9979 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44139e-09 l2=9.04809e-06 x=4.97951e-05 y=-0.000391026 z=-4.52319e-06 kx=-0.000734421 ky=-0.00123619 kz=23.1959 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28733e-09 l2=2.36078e-05 x=-4.85862e-05 y=0.000170644 z=-1.18072e-05 kx=-0.00122404 ky=-0.00067678 kz=22.6404 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90326e-09 l2=1.22623e-05 x=4.96228e-05 y=0.000158657 z=-6.13182e-06 kx=-0.000128393 ky=0.000929096 kz=22.6699 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6927e-09 l2=1.03002e-05 x=4.97342e-05 y=9.57275e-05 z=-5.1507e-06 kx=-0.000119262 ky=-0.000670312 kz=22.621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28189e-09 l2=2.39597e-05 x=-4.85438e-05 y=-2.24894e-06 z=-1.19805e-05 kx=8.29675e-07 ky=0.000513061 kz=23.1969 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.69495e-09 l2=3.20755e-06 x=-4.99743e-05 y=0.000345737 z=-1.60721e-06 kx=-0.000498731 ky=0.00177679 kz=22.9661 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.67007e-09 l2=1.82437e-06 x=-4.99917e-05 y=-0.000267424 z=-9.15525e-07 kx=-0.000230821 ky=-0.00162843 kz=22.8344 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25444e-09 l2=2.19862e-05 x=-4.87771e-05 y=-0.00025009 z=-1.09928e-05 kx=0.000692333 ky=-0.000332187 kz=22.7723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06435e-09 l2=9.89595e-06 x=-4.97545e-05 y=6.99491e-05 z=-4.94991e-06 kx=-0.000649043 ky=0.00112853 kz=23.1071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03751e-09 l2=1.39405e-05 x=4.95121e-05 y=0.000324648 z=-6.96893e-06 kx=-0.000857205 ky=-0.000389215 kz=23.059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0451e-09 l2=3.93533e-05 x=-4.59662e-05 y=-0.000122965 z=-1.96761e-05 kx=0.000550469 ky=0.000733897 kz=23.2883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10297e-09 l2=3.79805e-05 x=4.62543e-05 y=0.000432651 z=-1.89889e-05 kx=-0.000919053 ky=0.000459778 kz=22.9653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0754e-09 l2=1.01128e-05 x=-4.97437e-05 y=5.60761e-05 z=-5.05746e-06 kx=-0.00025209 ky=-0.000498622 kz=22.7747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20831e-09 l2=1.85642e-05 x=-4.91305e-05 y=-0.000385712 z=-9.28505e-06 kx=-0.00106454 ky=-0.00132453 kz=22.4389 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76347e-08 l2=1.23015e-06 x=-4.99963e-05 y=-0.00016459 z=-6.24485e-07 kx=-0.000275231 ky=-0.00125665 kz=23.2827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02057e-09 l2=2.63439e-05 x=4.8234e-05 y=0.000426305 z=-1.31721e-05 kx=-0.000156292 ky=0.00183147 kz=23.3076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.70699e-09 l2=3.22493e-06 x=4.99742e-05 y=0.000187757 z=-1.61425e-06 kx=-0.000704759 ky=-0.000490651 kz=22.459 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45475e-09 l2=1.09714e-05 x=4.96982e-05 y=-0.00033349 z=-5.48719e-06 kx=0.000353936 ky=-0.00124487 kz=22.8657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.01188e-09 l2=7.13936e-06 x=-4.98723e-05 y=1.52018e-05 z=-3.57358e-06 kx=-0.00111321 ky=-0.000522333 kz=23.207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.27222e-09 l2=1.24865e-05 x=-4.96091e-05 y=-0.000421231 z=-6.24228e-06 kx=0.000960204 ky=-0.00144682 kz=22.7556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01045e-09 l2=2.18522e-05 x=-4.8792e-05 y=0.000424078 z=-1.09253e-05 kx=0.000615571 ky=0.00161934 kz=23.2513 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06636e-09 l2=1.71435e-05 x=-4.92594e-05 y=-0.00036011 z=-8.57495e-06 kx=-0.00126311 ky=-0.000171217 kz=23.2405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05169e-09 l2=1.719e-05 x=-4.92558e-05 y=-0.000171361 z=-8.59535e-06 kx=7.21551e-05 ky=0.000335614 kz=22.4986 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05854e-09 l2=3.24011e-05 x=4.73023e-05 y=0.000425091 z=-1.62027e-05 kx=0.000807819 ky=0.00145683 kz=22.6831 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26076e-09 l2=2.7002e-05 x=4.81424e-05 y=-0.000297166 z=-1.35034e-05 kx=0.000848012 ky=-0.0016711 kz=22.617 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15016e-09 l2=2.83958e-05 x=4.79424e-05 y=0.000247554 z=-1.4197e-05 kx=-0.000721503 ky=0.000117909 kz=22.952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18189e-09 l2=1.47215e-05 x=4.94556e-05 y=-0.000362456 z=-7.35913e-06 kx=-0.00100193 ky=-0.00177999 kz=22.5822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14571e-09 l2=2.20757e-05 x=4.87661e-05 y=-0.000468324 z=-1.10403e-05 kx=0.000906094 ky=-0.0013495 kz=22.9352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08403e-09 l2=2.6391e-05 x=-4.82274e-05 y=0.000302518 z=-1.31964e-05 kx=-0.000159843 ky=0.000470003 kz=23.0893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.89843e-09 l2=9.98151e-06 x=4.97505e-05 y=-0.000414186 z=-4.99287e-06 kx=7.63364e-05 ky=0.000155458 kz=23.1686 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35857e-09 l2=1.12901e-05 x=4.96804e-05 y=-0.000359419 z=-5.64561e-06 kx=-5.95326e-05 ky=-0.000614568 kz=22.6881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29932e-09 l2=2.87441e-05 x=4.78901e-05 y=-0.000217536 z=-1.43726e-05 kx=-4.5058e-05 ky=2.11499e-05 kz=23.0481 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47374e-09 l2=2.72091e-05 x=-4.81141e-05 y=0.000348472 z=-1.36041e-05 kx=0.000561339 ky=0.000930856 kz=22.868 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28369e-09 l2=1.05723e-05 x=-4.97196e-05 y=0.000342875 z=-5.28915e-06 kx=-0.00109345 ky=-0.00033597 kz=22.8689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30866e-09 l2=1.32162e-05 x=-4.95612e-05 y=0.000396725 z=-6.61129e-06 kx=-0.00116309 ky=0.00170447 kz=22.7031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13321e-09 l2=2.74845e-05 x=4.80749e-05 y=-0.000298358 z=-1.37416e-05 kx=-0.000591307 ky=0.000315154 kz=23.0657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76209e-09 l2=8.26224e-06 x=4.98291e-05 y=-0.000358548 z=-4.13196e-06 kx=-1.88092e-05 ky=-0.000281662 kz=22.6515 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32422e-09 l2=9.057e-06 x=-4.97947e-05 y=-0.00023076 z=-4.52782e-06 kx=0.000605662 ky=-0.000916941 kz=22.5607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.16251e-09 l2=2.84948e-06 x=-4.99798e-05 y=8.31171e-05 z=-1.42704e-06 kx=-0.00010099 ky=-0.000953693 kz=23.0765 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11575e-09 l2=1.5474e-05 x=-4.93976e-05 y=-0.000245029 z=-7.73907e-06 kx=-0.000700481 ky=-0.00128046 kz=22.9104 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42831e-09 l2=3.15331e-05 x=4.74497e-05 y=-9.6748e-05 z=-1.5766e-05 kx=-0.000613901 ky=-0.000573307 kz=22.8038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74091e-08 l2=1.46787e-06 x=-4.99948e-05 y=0.00015638 z=-7.411e-07 kx=0.00070791 ky=0.00109828 kz=22.9719 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02481e-09 l2=2.3165e-05 x=4.86404e-05 y=-0.000326381 z=-1.15818e-05 kx=-0.000572118 ky=-0.00109148 kz=23.3003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46685e-09 l2=1.00318e-05 x=-4.9748e-05 y=-8.61552e-05 z=-5.01487e-06 kx=0.000815867 ky=-0.000348822 kz=23.1957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93194e-09 l2=5.26947e-06 x=4.99307e-05 y=0.000285111 z=-2.63347e-06 kx=-0.00103348 ky=-0.00036529 kz=23.1345 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28841e-09 l2=9.71261e-06 x=4.97637e-05 y=0.000279937 z=-4.85783e-06 kx=0.000175221 ky=0.00169376 kz=22.7881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20812e-09 l2=2.67264e-05 x=-4.81814e-05 y=0.000149162 z=-1.33634e-05 kx=0.000193138 ky=4.97963e-05 kz=23.0358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00366e-09 l2=2.53007e-05 x=-4.83732e-05 y=-1.21874e-05 z=-1.26516e-05 kx=-0.000333765 ky=-0.000196132 kz=22.5357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.12961e-09 l2=6.24105e-06 x=-4.99027e-05 y=-0.000498918 z=-3.12259e-06 kx=7.93362e-07 ky=-0.000798792 kz=22.8712 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00618e-09 l2=1.03429e-05 x=4.97316e-05 y=-0.000368697 z=-5.17466e-06 kx=0.00123638 ky=-0.000689465 kz=22.6196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43055e-09 l2=1.80648e-05 x=4.91771e-05 y=0.000415028 z=-9.03519e-06 kx=0.000951836 ky=0.000886412 kz=22.771 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13208e-09 l2=3.24655e-05 x=4.72916e-05 y=-0.000341329 z=-1.6234e-05 kx=0.000343948 ky=-0.000100582 kz=23.1136 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38813e-09 l2=1.54595e-05 x=-4.93993e-05 y=-0.000325787 z=-7.72874e-06 kx=0.000782026 ky=0.000350135 kz=22.7101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95853e-08 l2=9.97264e-07 x=4.99977e-05 y=0.000262978 z=-5.13705e-07 kx=0.000128538 ky=0.000866778 kz=22.9005 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62633e-09 l2=1.42862e-05 x=4.94876e-05 y=-0.000381823 z=-7.1428e-06 kx=-0.000755305 ky=-0.00201332 kz=23.2801 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42965e-09 l2=1.19905e-05 x=4.96395e-05 y=-0.000378524 z=-5.99483e-06 kx=-0.000528753 ky=-0.000762234 kz=22.8239 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03596e-09 l2=1.99065e-05 x=4.89995e-05 y=0.000123294 z=-9.95339e-06 kx=-0.000164471 ky=0.000956978 kz=22.5316 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80598e-09 l2=1.85468e-05 x=-4.91329e-05 y=0.000144575 z=-9.27314e-06 kx=0.000549603 ky=-0.00056187 kz=22.7846 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24663e-09 l2=1.83576e-05 x=4.91506e-05 y=-0.000305141 z=-9.17852e-06 kx=-0.000422605 ky=-0.000298279 kz=22.7845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00443e-09 l2=2.20321e-05 x=4.8771e-05 y=-0.000203349 z=-1.10185e-05 kx=0.00091324 ky=-0.000750058 kz=22.3324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01827e-09 l2=1.29975e-05 x=4.95757e-05 y=0.000192605 z=-6.50082e-06 kx=0.000721935 ky=0.000649094 kz=22.5573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51107e-09 l2=1.40646e-05 x=4.95033e-05 y=-0.000292754 z=-7.03187e-06 kx=-0.000535856 ky=-0.00128364 kz=22.4358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24006e-09 l2=3.26048e-05 x=4.72671e-05 y=0.000447317 z=-1.63054e-05 kx=0.00117082 ky=0.00189762 kz=23.0522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76714e-09 l2=9.04281e-06 x=4.97954e-05 y=0.000429221 z=-4.52081e-06 kx=-0.000684007 ky=-0.000132129 kz=22.9621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57568e-09 l2=1.52676e-05 x=4.94142e-05 y=-0.000492124 z=-7.63307e-06 kx=-0.000707381 ky=-0.00172008 kz=22.6754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0283e-09 l2=1.82158e-05 x=4.91632e-05 y=7.57675e-05 z=-9.11039e-06 kx=0.000927524 ky=-0.000937834 kz=22.8971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11647e-09 l2=2.63737e-05 x=4.82295e-05 y=0.000412502 z=-1.31889e-05 kx=0.000715148 ky=0.00162884 kz=23.0382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.36939e-09 l2=9.99653e-06 x=4.97495e-05 y=-0.000313774 z=-5.00128e-06 kx=0.000820484 ky=-0.000808377 kz=22.3697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63385e-09 l2=1.67028e-05 x=4.92974e-05 y=-0.000329543 z=-8.35424e-06 kx=0.000957604 ky=3.55733e-05 kz=23.0818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41872e-09 l2=2.35017e-05 x=-4.86001e-05 y=0.000329908 z=-1.175e-05 kx=0.000705637 ky=0.000120088 kz=22.6253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47733e-09 l2=1.58189e-05 x=-4.93707e-05 y=0.000108246 z=-7.90949e-06 kx=0.00032271 ky=-0.00056163 kz=22.4259 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09644e-09 l2=9.0309e-06 x=-4.97959e-05 y=0.000339252 z=-4.51537e-06 kx=0.000525849 ky=0.000892636 kz=23.2384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14569e-09 l2=3.34806e-05 x=4.71145e-05 y=0.000308712 z=-1.67411e-05 kx=9.65783e-05 ky=0.00107471 kz=22.9847 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04963e-09 l2=3.96372e-05 x=-4.59048e-05 y=0.000497323 z=-1.98189e-05 kx=9.80764e-05 ky=0.00157062 kz=22.8593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01534e-09 l2=1.85353e-05 x=-4.91335e-05 y=-0.000491461 z=-9.26936e-06 kx=-0.000566793 ky=-0.000282974 kz=23.1372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01249e-09 l2=9.48096e-06 x=-4.97747e-05 y=-0.000377339 z=-4.74198e-06 kx=-0.000457927 ky=-0.000380646 kz=22.8291 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07047e-09 l2=2.13025e-05 x=-4.88524e-05 y=0.000338791 z=-1.0652e-05 kx=-7.19146e-05 ky=0.000142233 kz=22.6386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21659e-09 l2=6.1936e-06 x=4.9904e-05 y=0.000181734 z=-3.09863e-06 kx=0.000547886 ky=0.0014797 kz=22.4742 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08384e-09 l2=2.5648e-05 x=-4.83278e-05 y=-0.000436041 z=-1.2824e-05 kx=0.000244555 ky=-0.000261057 kz=23.2357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43138e-09 l2=1.69979e-06 x=-4.99928e-05 y=4.28266e-05 z=-8.53427e-07 kx=-0.00104972 ky=0.000339585 kz=22.6332 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.0955e-09 l2=2.25903e-06 x=-4.99873e-05 y=0.000231582 z=-1.13652e-06 kx=-0.00112217 ky=-0.000449652 kz=22.814 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12512e-09 l2=4.71701e-06 x=-4.99445e-05 y=-0.000296077 z=-2.35721e-06 kx=0.000862002 ky=-0.000921859 kz=23.1525 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18873e-09 l2=1.03856e-05 x=4.97297e-05 y=-2.29413e-05 z=-5.19331e-06 kx=-4.36636e-05 ky=-0.000654205 kz=22.388 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31328e-09 l2=7.68277e-06 x=-4.98524e-05 y=4.57712e-05 z=-3.84056e-06 kx=0.000682548 ky=0.000577629 kz=22.9547 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29684e-09 l2=7.98407e-06 x=4.98404e-05 y=6.78574e-05 z=-3.99324e-06 kx=0.000253363 ky=0.00062088 kz=22.5488 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46821e-09 l2=1.07508e-05 x=4.97103e-05 y=-0.000291438 z=-5.37646e-06 kx=0.000140945 ky=-0.000673306 kz=22.7778 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47268e-09 l2=1.95749e-05 x=4.90323e-05 y=0.00019961 z=-9.79074e-06 kx=0.00118484 ky=-8.42695e-05 kz=22.7547 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40572e-09 l2=2.50238e-05 x=-4.84097e-05 y=-0.000106131 z=-1.25113e-05 kx=0.000644588 ky=-0.000719307 kz=23.0261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.25558e-09 l2=3.76869e-06 x=4.99644e-05 y=0.000102309 z=-1.88842e-06 kx=0.00113376 ky=-0.000322792 kz=23.1505 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0138e-09 l2=1.52297e-05 x=-4.94171e-05 y=2.58634e-05 z=-7.6132e-06 kx=0.00102006 ky=0.000641582 kz=23.1862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.98073e-09 l2=1.06074e-05 x=-4.9718e-05 y=-0.000411684 z=-5.30664e-06 kx=-0.000425685 ky=-0.0015595 kz=22.6393 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11491e-09 l2=9.21499e-06 x=-4.97874e-05 y=-0.000474387 z=-4.60662e-06 kx=0.000642535 ky=-0.000799886 kz=22.3591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22907e-09 l2=1.01306e-05 x=4.97427e-05 y=-0.000144093 z=-5.06761e-06 kx=0.000781979 ky=0.000573328 kz=23.093 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67433e-09 l2=8.061e-06 x=-4.98372e-05 y=0.000252268 z=-4.03401e-06 kx=-0.000971061 ky=0.000300264 kz=22.2997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17674e-09 l2=1.94913e-05 x=4.90412e-05 y=-1.22255e-05 z=-9.74593e-06 kx=-0.000138084 ky=0.000195295 kz=22.6422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18024e-09 l2=2.38009e-05 x=-4.85628e-05 y=6.05186e-05 z=-1.19032e-05 kx=-0.00105289 ky=-0.000676829 kz=23.1275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61602e-09 l2=8.51715e-06 x=4.98182e-05 y=0.000375758 z=-4.26184e-06 kx=0.00112139 ky=0.000714766 kz=22.7454 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98758e-09 l2=1.40179e-05 x=4.95065e-05 y=3.14615e-05 z=-7.00925e-06 kx=-0.000313818 ky=0.00104209 kz=22.5886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12986e-09 l2=1.02884e-05 x=-4.97349e-05 y=0.00022094 z=-5.14387e-06 kx=0.000647366 ky=0.000457686 kz=23.0431 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36335e-09 l2=1.43541e-05 x=4.94826e-05 y=0.000114668 z=-7.1759e-06 kx=-0.000849469 ky=0.00121444 kz=22.7631 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29752e-09 l2=3.3631e-05 x=4.70885e-05 y=-0.000122154 z=-1.68143e-05 kx=-0.000892065 ky=0.000616259 kz=22.7436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50259e-09 l2=1.62728e-05 x=-4.93337e-05 y=0.000132183 z=-8.13674e-06 kx=0.000197205 ky=0.000836958 kz=22.767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13593e-09 l2=1.08392e-05 x=-4.97054e-05 y=-5.19818e-05 z=-5.42199e-06 kx=-0.000606245 ky=-0.000648434 kz=22.4314 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.04204e-09 l2=9.35507e-06 x=4.97809e-05 y=0.00047592 z=-4.67851e-06 kx=-0.00025432 ky=-5.01431e-05 kz=23.2173 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10657e-09 l2=3.33511e-05 x=-4.71373e-05 y=0.000335955 z=-1.66768e-05 kx=-0.000337292 ky=0.000851444 kz=22.9101 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43202e-09 l2=2.86052e-05 x=-4.79106e-05 y=0.000187052 z=-1.43044e-05 kx=-0.000529789 ky=0.00105237 kz=23.0808 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03301e-09 l2=1.40036e-05 x=4.95075e-05 y=-0.000180372 z=-7.00237e-06 kx=-0.000204592 ky=-0.000898253 kz=22.5392 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50765e-09 l2=1.03796e-05 x=4.973e-05 y=-0.000166787 z=-5.19091e-06 kx=0.000161188 ky=-0.00134344 kz=23.0889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97603e-09 l2=7.6865e-06 x=-4.98522e-05 y=-0.000475612 z=-3.84405e-06 kx=8.78896e-05 ky=-0.00133145 kz=22.8233 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06672e-09 l2=8.40603e-06 x=-4.9823e-05 y=-0.000104731 z=-4.20489e-06 kx=-0.000610378 ky=0.000135941 kz=22.5782 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88981e-09 l2=7.58346e-06 x=-4.98562e-05 y=0.00014742 z=-3.79064e-06 kx=0.000909894 ky=0.00118213 kz=22.3212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07748e-09 l2=1.93578e-05 x=4.9054e-05 y=0.0001016 z=-9.68146e-06 kx=0.000928519 ky=0.000457449 kz=22.6395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01006e-09 l2=3.82283e-05 x=4.62017e-05 y=0.000134741 z=-1.91164e-05 kx=0.000890462 ky=0.000503021 kz=22.7093 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.24141e-09 l2=1.47916e-05 x=4.94499e-05 y=-0.000386534 z=-7.39957e-06 kx=0.00100675 ky=-0.000613336 kz=23.0302 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51428e-09 l2=7.81996e-06 x=4.98468e-05 y=0.000133832 z=-3.91271e-06 kx=0.000898489 ky=0.00120147 kz=22.6882 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78284e-09 l2=1.42615e-05 x=4.94889e-05 y=0.000245676 z=-7.13279e-06 kx=0.000525934 ky=0.00149468 kz=22.7064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20719e-09 l2=1.87722e-05 x=4.91116e-05 y=0.000320018 z=-9.38473e-06 kx=-0.000928847 ky=0.000303913 kz=22.9261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25272e-09 l2=1.39473e-05 x=-4.95113e-05 y=-0.000173001 z=-6.97511e-06 kx=-0.000375693 ky=0.000502506 kz=22.6711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16908e-09 l2=2.15236e-05 x=-4.88277e-05 y=-0.000432837 z=-1.07648e-05 kx=-0.00109618 ky=-0.000524091 kz=22.3906 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57266e-09 l2=1.8776e-05 x=4.91111e-05 y=0.000186851 z=-9.38784e-06 kx=-0.000446286 ky=0.000776867 kz=23.0968 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03915e-09 l2=3.19295e-05 x=-4.73822e-05 y=-0.000482731 z=-1.59676e-05 kx=-0.00111345 ky=-0.000620881 kz=22.961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47716e-08 l2=1.1484e-06 x=-4.99968e-05 y=-0.00024178 z=-5.86957e-07 kx=-0.000168004 ky=-0.00130886 kz=22.5279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51434e-09 l2=3.0129e-05 x=4.76769e-05 y=-6.71328e-05 z=-1.50652e-05 kx=-3.2494e-05 ky=-0.00105085 kz=23.2224 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24708e-09 l2=1.7524e-05 x=4.92263e-05 y=0.000456525 z=-8.76344e-06 kx=0.000378991 ky=0.00114451 kz=22.7107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.20595e-09 l2=3.46636e-06 x=-4.99699e-05 y=-4.10593e-05 z=-1.73781e-06 kx=-0.00116272 ky=-0.000586892 kz=23.0036 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18537e-09 l2=2.11666e-05 x=-4.88674e-05 y=0.000412618 z=-1.05833e-05 kx=0.000289887 ky=0.001038 kz=23.2523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.90812e-09 l2=8.91094e-06 x=4.98013e-05 y=0.000479128 z=-4.45579e-06 kx=-0.000525413 ky=0.00213486 kz=23.1569 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25488e-09 l2=7.81952e-06 x=4.98468e-05 y=0.000154887 z=-3.913e-06 kx=0.000953598 ky=-0.00013651 kz=22.519 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43025e-09 l2=2.57308e-05 x=4.83161e-05 y=5.62559e-05 z=-1.28682e-05 kx=0.000994549 ky=-0.000371428 kz=22.9767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22838e-09 l2=7.95453e-06 x=-4.98416e-05 y=-0.000315091 z=-3.97889e-06 kx=-0.000231571 ky=-0.000680007 kz=22.4872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28822e-09 l2=4.52863e-06 x=4.99488e-05 y=-9.32509e-05 z=-2.26389e-06 kx=-0.000490069 ky=-0.00111971 kz=22.8459 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81775e-09 l2=2.147e-05 x=4.88339e-05 y=-0.000446321 z=-1.07374e-05 kx=0.00068489 ky=-0.00195732 kz=22.9698 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40274e-09 l2=1.56951e-05 x=-4.93804e-05 y=-0.000314443 z=-7.84833e-06 kx=-3.78408e-05 ky=-0.00141189 kz=23.0685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.08051e-09 l2=1.25769e-05 x=-4.96031e-05 y=0.000236838 z=-6.28961e-06 kx=-6.35483e-05 ky=-0.000555628 kz=22.8071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08549e-09 l2=2.55552e-05 x=-4.83398e-05 y=0.000426913 z=-1.27786e-05 kx=-0.000223079 ky=-6.73363e-05 kz=22.6345 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64138e-09 l2=1.55678e-05 x=-4.93908e-05 y=-0.00036174 z=-7.7832e-06 kx=0.000701754 ky=-0.00100348 kz=22.9057 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53779e-09 l2=1.67756e-05 x=-4.92917e-05 y=0.000120795 z=-8.38777e-06 kx=0.000379064 ky=0.000883219 kz=22.9884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98333e-09 l2=1.02893e-05 x=-4.97347e-05 y=-0.000493299 z=-5.14575e-06 kx=-5.77862e-05 ky=-0.000817212 kz=22.3452 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20181e-09 l2=2.6493e-05 x=-4.8214e-05 y=-0.000122006 z=-1.32454e-05 kx=0.000797594 ky=-0.000939488 kz=22.3419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19855e-09 l2=1.70832e-05 x=4.92654e-05 y=0.000115424 z=-8.5405e-06 kx=-0.000799529 ky=0.000503279 kz=22.9864 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49629e-09 l2=1.70414e-05 x=4.92688e-05 y=0.000278752 z=-8.52107e-06 kx=-0.000170121 ky=0.000104267 kz=22.412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08706e-09 l2=2.1083e-05 x=4.88762e-05 y=-0.000373061 z=-1.05425e-05 kx=0.000221175 ky=-0.0013434 kz=22.9671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11085e-09 l2=2.52256e-05 x=4.83827e-05 y=-4.44237e-05 z=-1.26151e-05 kx=0.000828791 ky=-3.23316e-05 kz=22.9162 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20631e-09 l2=1.97565e-05 x=4.90148e-05 y=2.01665e-05 z=-9.87774e-06 kx=-0.00052904 ky=-0.000317201 kz=23.1946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00023e-09 l2=2.59786e-05 x=-4.82836e-05 y=-0.000366736 z=-1.29892e-05 kx=0.000274019 ky=-0.00082966 kz=22.3401 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78025e-09 l2=1.49012e-05 x=-4.94415e-05 y=-0.000160408 z=-7.45399e-06 kx=-0.00114546 ky=-0.000885513 kz=22.5544 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03054e-09 l2=1.49012e-05 x=-4.94419e-05 y=0.000281697 z=-7.4517e-06 kx=-2.90289e-05 ky=-0.000229549 kz=23.1077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03685e-09 l2=3.12914e-05 x=4.74887e-05 y=-0.000340846 z=-1.56478e-05 kx=0.000784829 ky=-0.00035304 kz=22.9324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67097e-09 l2=1.55641e-05 x=4.93909e-05 y=-0.000401761 z=-7.7825e-06 kx=-0.000179059 ky=-0.000464352 kz=23.0496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45246e-09 l2=9.90625e-06 x=-4.97543e-05 y=-0.000187914 z=-4.95215e-06 kx=0.000767124 ky=0.000150009 kz=22.4175 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55523e-09 l2=2.05559e-05 x=4.89325e-05 y=6.28679e-05 z=-1.02784e-05 kx=-0.000160698 ky=0.00103212 kz=22.4737 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86321e-09 l2=1.08258e-05 x=4.97064e-05 y=-0.000443701 z=-5.41222e-06 kx=-0.000738022 ky=-0.000654776 kz=22.4319 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00131e-09 l2=1.32035e-05 x=4.95625e-05 y=-0.00022127 z=-6.60116e-06 kx=-0.000490968 ky=-0.000820485 kz=22.5449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=0 l2=0 x=5.00002e-05 y=4.96593e-05 z=4.43805e-10 kx=-0.000204278 ky=-0.00102553 kz=23.0146 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35521e-09 l2=1.24019e-05 x=4.96139e-05 y=-0.00031718 z=-6.20413e-06 kx=0.000905348 ky=-0.000108094 kz=22.3548 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2838e-09 l2=1.22054e-05 x=-4.96261e-05 y=0.00035376 z=-6.10461e-06 kx=-0.000583367 ky=0.00184563 kz=22.5311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11382e-09 l2=2.45686e-05 x=-4.8467e-05 y=-0.000295058 z=-1.22873e-05 kx=-0.00113339 ky=-0.00134716 kz=22.8691 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29567e-09 l2=3.29428e-05 x=4.72087e-05 y=-0.000124544 z=-1.64738e-05 kx=0.000829044 ky=-0.00143358 kz=23.0198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07048e-09 l2=2.36701e-05 x=-4.85788e-05 y=-0.000456098 z=-1.18375e-05 kx=-0.000881641 ky=-9.13811e-05 kz=22.9178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01197e-09 l2=2.24708e-05 x=4.87209e-05 y=7.59976e-05 z=-1.1238e-05 kx=0.000953658 ky=-0.000425192 kz=22.3883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3183e-09 l2=6.7044e-06 x=4.98875e-05 y=-0.000392216 z=-3.3541e-06 kx=0.000343916 ky=-0.00117634 kz=23.0762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07521e-09 l2=1.20111e-05 x=4.96379e-05 y=0.000411288 z=-6.00793e-06 kx=0.00083671 ky=0.00129357 kz=22.4825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41395e-09 l2=1.61925e-05 x=4.93404e-05 y=-0.000471448 z=-8.09623e-06 kx=-0.000323628 ky=-0.000564302 kz=22.3649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57097e-09 l2=7.85362e-06 x=4.98455e-05 y=0.00022192 z=-3.92975e-06 kx=0.000989175 ky=0.000541527 kz=22.8503 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07164e-09 l2=1.30515e-05 x=-4.95724e-05 y=-0.000417309 z=-6.52652e-06 kx=-0.000107502 ky=-0.00153336 kz=22.5965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00387e-09 l2=2.84623e-05 x=-4.79325e-05 y=-0.000441636 z=-1.42303e-05 kx=0.000672535 ky=-0.0016363 kz=23.0766 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1893e-09 l2=3.12811e-05 x=-4.74913e-05 y=0.000296565 z=-1.56401e-05 kx=0.000514091 ky=0.00125054 kz=22.8847 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32835e-09 l2=9.61222e-06 x=4.97685e-05 y=-0.000100291 z=-4.80819e-06 kx=0.000415564 ky=0.00072305 kz=22.4933 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11835e-09 l2=3.50885e-05 x=4.6821e-05 y=0.000180214 z=-1.75453e-05 kx=0.000240891 ky=0.000837013 kz=23.2742 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78966e-09 l2=1.52586e-05 x=-4.94149e-05 y=-0.000105449 z=-7.62832e-06 kx=0.000867864 ky=-0.000132938 kz=22.749 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0413e-09 l2=1.11092e-05 x=-4.96905e-05 y=0.00023279 z=-5.55696e-06 kx=-0.000614726 ky=-0.000602685 kz=22.7369 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6554e-09 l2=1.5026e-05 x=-4.94325e-05 y=0.000357044 z=-7.51327e-06 kx=0.000251953 ky=0.00153357 kz=23.0147 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15225e-09 l2=1.78296e-05 x=4.91991e-05 y=-0.000263667 z=-8.9144e-06 kx=-0.000453036 ky=-0.00154814 kz=23.3086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03887e-09 l2=1.94483e-05 x=4.90455e-05 y=0.000415222 z=-9.72409e-06 kx=-0.000268289 ky=0.000593337 kz=22.9151 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.96203e-09 l2=6.932e-06 x=4.98799e-05 y=0.0002554 z=-3.46736e-06 kx=-0.00028793 ky=0.00031732 kz=23.1779 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05835e-09 l2=2.82945e-05 x=4.79567e-05 y=0.000140782 z=-1.41488e-05 kx=0.000492885 ky=4.98255e-05 kz=22.6073 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24667e-09 l2=1.86806e-05 x=4.91203e-05 y=-1.26607e-05 z=-9.33925e-06 kx=-0.000779985 ky=0.000471012 kz=22.9896 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50114e-09 l2=2.0642e-05 x=4.89234e-05 y=-0.000150828 z=-1.03215e-05 kx=-0.000130374 ky=-0.000991638 kz=22.8482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74586e-09 l2=9.2815e-06 x=-4.97843e-05 y=0.000147108 z=-4.6413e-06 kx=0.000147628 ky=0.00130606 kz=22.6045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01117e-09 l2=2.5027e-05 x=-4.84083e-05 y=-0.000417634 z=-1.25166e-05 kx=-0.00122776 ky=0.000130286 kz=22.9913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65469e-09 l2=1.29718e-05 x=-4.95775e-05 y=0.000296231 z=-6.48759e-06 kx=-0.000388974 ky=0.00154034 kz=22.9651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03573e-09 l2=4.52993e-05 x=-4.4575e-05 y=0.00013584 z=-2.26521e-05 kx=-0.00101875 ky=0.00105013 kz=22.9991 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.69015e-09 l2=1.00602e-05 x=4.97466e-05 y=-0.00036385 z=-5.03047e-06 kx=-0.000449685 ky=0.000292415 kz=22.8334 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.1445e-09 l2=6.06415e-06 x=-4.99081e-05 y=5.63496e-05 z=-3.0334e-06 kx=0.000113539 ky=0.000849513 kz=22.7389 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21287e-09 l2=1.69284e-05 x=-4.92781e-05 y=0.00040931 z=-8.46693e-06 kx=-0.000952958 ky=-7.33438e-05 kz=22.388 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10515e-09 l2=6.18042e-06 x=4.99043e-05 y=-0.0002955 z=-3.09245e-06 kx=0.000754304 ky=-0.00167448 kz=22.3187 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22736e-09 l2=3.47176e-05 x=4.68898e-05 y=-0.000282615 z=-1.73606e-05 kx=0.000549392 ky=-0.000862811 kz=22.3177 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50109e-09 l2=1.53499e-05 x=4.94074e-05 y=-0.000155691 z=-7.67694e-06 kx=0.000586494 ky=-0.00143778 kz=22.9637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35382e-09 l2=2.07431e-05 x=-4.89129e-05 y=-0.00017031 z=-1.03712e-05 kx=0.000491671 ky=-0.00132192 kz=23.0736 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01517e-09 l2=1.4809e-05 x=-4.9449e-05 y=7.16707e-06 z=-7.40326e-06 kx=0.000809053 ky=0.000826463 kz=22.8677 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33028e-09 l2=8.36149e-06 x=4.98251e-05 y=-0.000334163 z=-4.17962e-06 kx=-0.000804866 ky=-0.00034014 kz=22.4396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32176e-09 l2=1.76215e-05 x=-4.92176e-05 y=0.000246903 z=-8.81214e-06 kx=-0.00032727 ky=0.000449333 kz=22.8714 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10887e-09 l2=2.55712e-05 x=-4.83374e-05 y=0.000102326 z=-1.27877e-05 kx=-0.000718786 ky=0.000324444 kz=23.2116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17888e-09 l2=1.94458e-06 x=-4.99906e-05 y=0.000439451 z=-9.71438e-07 kx=0.000866775 ky=0.00138773 kz=22.3419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91807e-09 l2=9.08408e-06 x=4.97932e-05 y=-0.000299913 z=-4.54468e-06 kx=0.000784811 ky=-0.00128519 kz=23.1866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72006e-09 l2=9.98293e-06 x=-4.97503e-05 y=5.38983e-05 z=-4.99265e-06 kx=-0.000149632 ky=-0.000625983 kz=23.1704 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17621e-09 l2=7.73276e-06 x=-4.98505e-05 y=-0.000161381 z=-3.86638e-06 kx=0.000500916 ky=-0.00063361 kz=23.0161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49644e-09 l2=1.08381e-05 x=4.97055e-05 y=0.000172332 z=-5.42017e-06 kx=0.000179733 ky=0.00145612 kz=22.7039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01647e-09 l2=1.81881e-05 x=-4.91659e-05 y=-0.000380594 z=-9.09588e-06 kx=-0.000625244 ky=-0.00182131 kz=23.142 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07333e-09 l2=2.12631e-05 x=4.88564e-05 y=-0.000199246 z=-1.06336e-05 kx=0.000711389 ky=1.91879e-05 kz=22.929 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64981e-09 l2=1.83117e-05 x=-4.91547e-05 y=0.000490714 z=-9.15679e-06 kx=-6.2033e-05 ky=2.5946e-05 kz=22.367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04001e-09 l2=1.60931e-05 x=-4.93483e-05 y=1.90525e-05 z=-8.04743e-06 kx=-0.000156829 ky=0.000838253 kz=23.2089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22941e-09 l2=1.73327e-05 x=-4.92434e-05 y=-0.000257785 z=-8.66654e-06 kx=0.000187412 ky=-0.00071691 kz=22.3044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67556e-09 l2=7.08126e-06 x=4.98747e-05 y=-0.000155924 z=-3.54054e-06 kx=-0.000657288 ky=-0.000395849 kz=22.9605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.03423e-09 l2=5.63052e-06 x=-4.99207e-05 y=0.000353844 z=-2.8189e-06 kx=-0.000731801 ky=1.41408e-05 kz=22.556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35885e-09 l2=2.72823e-05 x=4.8103e-05 y=7.18262e-05 z=-1.36433e-05 kx=0.000702237 ky=0.00081506 kz=23.2246 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30015e-09 l2=1.89481e-05 x=-4.90939e-05 y=-0.000321637 z=-9.47692e-06 kx=-0.00102753 ky=-0.00108842 kz=22.8307 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44066e-09 l2=2.17374e-05 x=4.8805e-05 y=-0.000161355 z=-1.08675e-05 kx=-0.000881667 ky=0.000100194 kz=22.6578 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36856e-09 l2=1.453e-05 x=4.94693e-05 y=-0.00022191 z=-7.26705e-06 kx=0.000633319 ky=-0.00127985 kz=23.3032 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25803e-09 l2=1.36352e-05 x=4.95331e-05 y=-0.000109581 z=-6.81848e-06 kx=0.000126345 ky=-0.00038267 kz=22.8946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68741e-09 l2=1.70158e-05 x=-4.92709e-05 y=0.00024268 z=-8.50943e-06 kx=-0.000316718 ky=-0.000360738 kz=22.5059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56309e-09 l2=1.76323e-05 x=4.92168e-05 y=-0.000114336 z=-8.8166e-06 kx=-0.00015826 ky=-0.000816072 kz=23.0934 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71476e-09 l2=1.02588e-05 x=4.97364e-05 y=-0.000272914 z=-5.12934e-06 kx=-0.000403552 ky=-0.00137308 kz=22.3566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39153e-09 l2=1.39544e-05 x=4.95109e-05 y=0.000315965 z=-6.979e-06 kx=0.000279614 ky=0.0013152 kz=22.9656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15289e-09 l2=2.50983e-05 x=4.83993e-05 y=-0.000318122 z=-1.25526e-05 kx=0.00108719 ky=-0.0016776 kz=22.8593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01097e-09 l2=2.51271e-05 x=4.83957e-05 y=-1.07255e-05 z=-1.2565e-05 kx=0.000459009 ky=0.000341695 kz=23.0031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23459e-09 l2=7.8328e-06 x=4.98464e-05 y=0.000472945 z=-3.91695e-06 kx=-2.92258e-05 ky=0.000363476 kz=23.0462 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15953e-09 l2=1.9727e-05 x=-4.90175e-05 y=0.000149129 z=-9.86433e-06 kx=-0.000122754 ky=-0.000170486 kz=22.6029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73344e-09 l2=1.40985e-05 x=-4.95004e-05 y=-4.63071e-05 z=-7.05238e-06 kx=-0.0010426 ky=-0.000551324 kz=23.023 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.38678e-09 l2=3.40575e-06 x=4.99711e-05 y=-5.79721e-05 z=-1.70576e-06 kx=8.79357e-05 ky=0.00101275 kz=23.1357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21942e-09 l2=2.88755e-05 x=-4.787e-05 y=-0.000114525 z=-1.44393e-05 kx=-0.000470243 ky=0.000355504 kz=23.1093 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.70391e-09 l2=3.08359e-06 x=-4.99763e-05 y=9.65906e-05 z=-1.54384e-06 kx=0.000375532 ky=-0.000544043 kz=23.1012 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04183e-09 l2=1.37422e-05 x=4.95256e-05 y=0.00027088 z=-6.87213e-06 kx=0.000241728 ky=0.000689858 kz=23.2695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11539e-09 l2=2.05456e-05 x=4.89333e-05 y=-0.000366382 z=-1.02739e-05 kx=0.000240689 ky=2.21992e-05 kz=22.4962 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16461e-09 l2=2.56802e-05 x=4.83232e-05 y=0.000298417 z=-1.28412e-05 kx=0.000222641 ky=0.000626053 kz=22.7639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5879e-09 l2=7.17413e-06 x=-4.98713e-05 y=0.000224657 z=-3.58853e-06 kx=0.000152082 ky=0.00154168 kz=22.8096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17195e-09 l2=1.16669e-05 x=-4.96586e-05 y=-0.000267928 z=-5.83378e-06 kx=0.000125451 ky=-0.000464285 kz=22.6412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49447e-09 l2=1.32082e-05 x=-4.95621e-05 y=0.000266203 z=-6.60429e-06 kx=0.000247091 ky=-0.000453239 kz=22.7019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.8564e-09 l2=1.21055e-05 x=-4.96327e-05 y=-9.93948e-05 z=-6.0525e-06 kx=0.000773729 ky=-0.000394382 kz=22.9747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70712e-09 l2=2.03711e-05 x=-4.89514e-05 y=-0.000393808 z=-1.01881e-05 kx=-0.000795815 ky=-0.000942762 kz=22.7377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07541e-09 l2=2.69343e-05 x=-4.81523e-05 y=-7.28969e-05 z=-1.34678e-05 kx=-3.54118e-05 ky=-0.000326042 kz=23.0294 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.12644e-09 l2=7.20778e-06 x=-4.98701e-05 y=0.000496114 z=-3.60486e-06 kx=0.000272943 ky=0.000236204 kz=22.9255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01199e-09 l2=2.42044e-05 x=4.85127e-05 y=-0.000282706 z=-1.21054e-05 kx=0.00122223 ky=-0.00124314 kz=22.402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.00497e-09 l2=7.63461e-06 x=4.98544e-05 y=0.000462322 z=-3.81815e-06 kx=-0.000767943 ky=0.000683994 kz=23.153 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27992e-09 l2=1.93483e-05 x=-4.90549e-05 y=-4.50334e-05 z=-9.67684e-06 kx=-0.000941026 ky=5.8117e-05 kz=22.7257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41748e-09 l2=1.59328e-05 x=4.93615e-05 y=-0.000199166 z=-7.9666e-06 kx=-0.000239979 ky=-8.22551e-05 kz=22.6435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32685e-09 l2=8.80397e-06 x=-4.98061e-05 y=-0.000462541 z=-4.40088e-06 kx=0.000814477 ky=9.45306e-06 kz=22.957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77544e-09 l2=8.59072e-06 x=4.9815e-05 y=-0.00015999 z=-4.29854e-06 kx=0.00103104 ky=-0.000703988 kz=22.4099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.57721e-09 l2=4.7706e-06 x=4.99432e-05 y=0.000100045 z=-2.38517e-06 kx=-0.000652711 ky=0.000454252 kz=22.9133 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14819e-09 l2=7.37273e-06 x=4.98639e-05 y=2.53506e-05 z=-3.68742e-06 kx=0.000222235 ky=0.000824954 kz=23.1008 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25504e-09 l2=2.77214e-05 x=4.80403e-05 y=3.27201e-05 z=-1.38622e-05 kx=0.000434966 ky=-0.00104329 kz=23.172 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51273e-09 l2=3.0452e-05 x=4.76254e-05 y=-0.000242065 z=-1.52273e-05 kx=0.000260111 ky=-0.0011573 kz=23.0382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.92464e-09 l2=1.27339e-05 x=-4.95933e-05 y=0.000388209 z=-6.36687e-06 kx=0.000714081 ky=0.00105543 kz=22.6949 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26156e-09 l2=1.81678e-05 x=-4.91684e-05 y=-0.000246573 z=-9.08259e-06 kx=0.000915919 ky=0.000431649 kz=23.158 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57701e-09 l2=2.2668e-05 x=-4.86983e-05 y=-0.000215841 z=-1.13364e-05 kx=-0.000747553 ky=-0.00107748 kz=22.968 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14881e-09 l2=9.74292e-06 x=4.97624e-05 y=0.000487203 z=-4.87009e-06 kx=-0.000895957 ky=-1.82269e-05 kz=22.8678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.26881e-09 l2=6.12063e-06 x=-4.99062e-05 y=0.000488856 z=-3.06464e-06 kx=-0.00125105 ky=0.00047125 kz=23.174 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.10372e-09 l2=3.20133e-06 x=4.99745e-05 y=0.000294418 z=-1.60217e-06 kx=-0.000474286 ky=0.000300094 kz=22.6356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11004e-09 l2=2.30748e-05 x=4.86502e-05 y=-0.000416786 z=-1.15405e-05 kx=0.00120605 ky=-0.000134472 kz=22.9371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59119e-09 l2=1.46868e-05 x=-4.94579e-05 y=-0.000218474 z=-7.3442e-06 kx=-1.26514e-05 ky=-6.36948e-06 kz=22.3289 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16609e-09 l2=2.38128e-05 x=-4.85623e-05 y=-0.000211464 z=-1.19049e-05 kx=0.000942527 ky=0.000444933 kz=22.3781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60908e-09 l2=1.65696e-05 x=-4.93093e-05 y=2.75287e-05 z=-8.28364e-06 kx=0.000897249 ky=0.000282283 kz=22.4395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.91194e-09 l2=1.28776e-05 x=4.95841e-05 y=0.000163679 z=-6.43866e-06 kx=-0.000738161 ky=0.00147682 kz=23.0853 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26969e-09 l2=1.24837e-05 x=-4.9609e-05 y=-0.000154614 z=-6.24205e-06 kx=0.00020707 ky=-0.000417494 kz=22.7501 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02854e-09 l2=2.87197e-05 x=4.78938e-05 y=-4.2253e-05 z=-1.436e-05 kx=-0.000173755 ky=0.000357666 kz=23.2599 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17291e-09 l2=2.65653e-05 x=-4.82034e-05 y=0.000131392 z=-1.32839e-05 kx=-0.000327704 ky=-0.000124184 kz=22.5186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.45168e-09 l2=5.62976e-06 x=4.99208e-05 y=-0.000345713 z=-2.81533e-06 kx=-0.000351972 ky=0.000323818 kz=22.6263 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20033e-09 l2=1.65707e-05 x=4.93091e-05 y=7.39502e-05 z=-8.28462e-06 kx=-0.000626171 ky=0.000571247 kz=23.2025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0584e-09 l2=2.12558e-05 x=4.88578e-05 y=0.000107845 z=-1.06273e-05 kx=-0.000555152 ky=-0.000742558 kz=23.2893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.72665e-09 l2=1.77535e-06 x=-4.99922e-05 y=-0.000393377 z=-8.91802e-07 kx=-0.000351023 ky=-0.000375628 kz=23.0548 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03255e-09 l2=1.86981e-05 x=-4.91184e-05 y=-0.000200436 z=-9.34881e-06 kx=0.000349997 ky=-0.00120779 kz=23.0299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64661e-09 l2=9.04631e-06 x=-4.9795e-05 y=9.37551e-05 z=-4.52449e-06 kx=-0.000234834 ky=-0.000463848 kz=22.9457 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44075e-09 l2=1.33995e-05 x=4.95489e-05 y=0.000148133 z=-6.70288e-06 kx=0.00109818 ky=-0.000318088 kz=22.6871 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58068e-09 l2=1.71414e-05 x=4.926e-05 y=0.000471199 z=-8.57183e-06 kx=0.000145315 ky=0.00143737 kz=23.0458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62113e-09 l2=1.02401e-05 x=4.97371e-05 y=0.000380888 z=-5.12182e-06 kx=0.000437779 ky=0.00156973 kz=23.1409 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58643e-09 l2=3.54999e-06 x=-4.99686e-05 y=-0.000291057 z=-1.77503e-06 kx=0.000563713 ky=0.000454567 kz=22.4213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08436e-09 l2=1.13775e-05 x=-4.96754e-05 y=3.57286e-05 z=-5.68888e-06 kx=0.000193848 ky=0.000744849 kz=22.969 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40811e-09 l2=1.97453e-05 x=-4.90153e-05 y=0.000210034 z=-9.87577e-06 kx=-0.00109798 ky=-4.59392e-05 kz=22.3673 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5381e-09 l2=8.54998e-06 x=-4.98171e-05 y=0.000103474 z=-4.27581e-06 kx=0.000432872 ky=0.000654999 kz=22.7318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.30336e-09 l2=9.08927e-06 x=-4.9793e-05 y=0.000444002 z=-4.54789e-06 kx=-0.000748991 ky=0.00211247 kz=23.3062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.54787e-09 l2=9.66432e-06 x=-4.97662e-05 y=0.000457973 z=-4.83248e-06 kx=0.000438661 ky=0.00178313 kz=22.8332 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33166e-09 l2=2.48291e-05 x=4.84348e-05 y=-0.000279345 z=-1.24136e-05 kx=-0.000749292 ky=-0.00123521 kz=23.1467 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29638e-09 l2=2.39947e-05 x=4.85395e-05 y=-0.000436445 z=-1.19977e-05 kx=-0.000167387 ky=-0.000995377 kz=23.1707 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00466e-09 l2=1.82624e-05 x=4.9159e-05 y=9.16435e-05 z=-9.13285e-06 kx=0.000532358 ky=-0.000674617 kz=22.3873 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80882e-09 l2=1.52568e-05 x=-4.94144e-05 y=-7.54625e-05 z=-7.63165e-06 kx=-0.00107124 ky=-0.00125451 kz=22.4475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16198e-09 l2=5.95961e-06 x=-4.99112e-05 y=5.64573e-05 z=-2.98048e-06 kx=0.000185365 ky=-0.000967458 kz=22.5318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15041e-09 l2=7.52166e-06 x=-4.98586e-05 y=0.000255169 z=-3.75989e-06 kx=0.000906053 ky=0.000629578 kz=22.4007 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15995e-09 l2=1.40782e-05 x=-4.95024e-05 y=0.000230461 z=-7.03797e-06 kx=0.000774133 ky=-0.000270511 kz=22.5518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4823e-09 l2=1.01671e-05 x=4.9741e-05 y=-0.000357173 z=-5.08475e-06 kx=-1.42271e-05 ky=-0.00148594 kz=22.9461 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.85711e-09 l2=5.68764e-06 x=4.99191e-05 y=-0.000364682 z=-2.84786e-06 kx=0.000983178 ky=-0.00171735 kz=23.1792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5149e-09 l2=1.63131e-05 x=4.93303e-05 y=-0.000401289 z=-8.15742e-06 kx=5.83423e-05 ky=3.82796e-05 kz=22.5731 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82248e-08 l2=1.77004e-06 x=-4.99924e-05 y=-0.000411073 z=-8.9221e-07 kx=0.000868102 ky=-0.00138707 kz=22.5755 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59018e-09 l2=1.35308e-05 x=4.95403e-05 y=-0.000187586 z=-6.76645e-06 kx=0.000129233 ky=-0.00076199 kz=23.2798 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66869e-09 l2=8.42681e-06 x=4.98221e-05 y=-3.43932e-05 z=-4.21582e-06 kx=0.000716743 ky=-0.000976071 kz=22.6026 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70219e-09 l2=4.67733e-06 x=4.99452e-05 y=0.000383007 z=-2.34209e-06 kx=0.000937331 ky=7.18632e-05 kz=22.5593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00831e-09 l2=1.76779e-05 x=-4.92127e-05 y=-0.000103671 z=-8.83909e-06 kx=0.000179308 ky=0.00071273 kz=22.8886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4723e-09 l2=1.86299e-05 x=-4.91251e-05 y=4.93839e-05 z=-9.31415e-06 kx=0.000711944 ky=-0.000995565 kz=22.5685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16551e-09 l2=1.5678e-05 x=-4.93816e-05 y=-2.48925e-05 z=-7.84068e-06 kx=-0.000515599 ky=-0.000909023 kz=23.2702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.20264e-09 l2=5.34761e-06 x=-4.99285e-05 y=-3.03449e-05 z=-2.67696e-06 kx=-0.000713691 ky=-0.000446554 kz=22.9024 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.26841e-09 l2=2.84388e-06 x=4.99798e-05 y=-0.000347291 z=-1.42824e-06 kx=0.00100789 ky=-0.000166245 kz=23.2429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.36985e-09 l2=1.30086e-05 x=-4.95755e-05 y=-0.000329623 z=-6.50527e-06 kx=0.000321705 ky=-0.000992713 kz=22.9722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19752e-09 l2=3.32119e-05 x=4.71627e-05 y=0.000485787 z=-1.66048e-05 kx=-0.000868806 ky=0.000302812 kz=23.0702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0419e-09 l2=3.10182e-05 x=-4.75344e-05 y=-0.000289663 z=-1.55084e-05 kx=0.000603763 ky=-0.00144652 kz=22.872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5477e-09 l2=2.14148e-05 x=-4.88407e-05 y=0.000162498 z=-1.0706e-05 kx=0.000996418 ky=0.00124994 kz=22.6794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65373e-09 l2=1.18221e-05 x=4.96492e-05 y=-0.000447484 z=-5.91384e-06 kx=0.00088524 ky=0.000104433 kz=22.3338 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01916e-09 l2=9.81196e-06 x=4.97586e-05 y=0.000289363 z=-4.90928e-06 kx=0.00106034 ky=0.00111235 kz=23.0352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75275e-09 l2=1.36039e-05 x=4.95351e-05 y=7.04588e-06 z=-6.80442e-06 kx=0.000731481 ky=-0.000844099 kz=23.0761 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15024e-09 l2=1.64568e-05 x=4.93181e-05 y=0.00043627 z=-8.23091e-06 kx=0.00088236 ky=0.000841802 kz=22.5487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25638e-09 l2=1.90741e-05 x=4.90821e-05 y=0.00046019 z=-9.53773e-06 kx=3.49514e-05 ky=0.000801868 kz=23.1391 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.22465e-09 l2=8.54113e-06 x=-4.98172e-05 y=-0.000191653 z=-4.27465e-06 kx=-0.00114644 ky=0.000326732 kz=23.0781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65764e-09 l2=2.71211e-05 x=-4.81256e-05 y=-0.000313521 z=-1.35636e-05 kx=-0.00106901 ky=-0.00107034 kz=23.0925 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35481e-09 l2=1.52981e-05 x=-4.94113e-05 y=-0.000310507 z=-7.65232e-06 kx=-0.000941659 ky=0.00023901 kz=22.4774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72006e-09 l2=1.05843e-05 x=-4.97193e-05 y=0.000489597 z=-5.29202e-06 kx=0.000455951 ky=0.000932631 kz=22.3534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.33722e-09 l2=5.51957e-06 x=-4.9924e-05 y=1.16718e-05 z=-2.76059e-06 kx=0.000840866 ky=0.000313494 kz=22.6065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16616e-09 l2=1.74454e-05 x=-4.9233e-05 y=0.000478062 z=-8.72518e-06 kx=-0.000899325 ky=0.00125636 kz=23.2634 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25387e-09 l2=1.96072e-05 x=4.90291e-05 y=0.000306597 z=-9.80658e-06 kx=0.00112082 ky=0.00115866 kz=23.1842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3161e-09 l2=1.78244e-05 x=-4.91998e-05 y=-0.000421305 z=-8.91088e-06 kx=0.000917897 ky=-0.00202925 kz=23.0465 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55199e-09 l2=1.57171e-05 x=4.93783e-05 y=-0.000291666 z=-7.86174e-06 kx=0.00112727 ky=-0.000865507 kz=22.8461 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.52075e-09 l2=1.55023e-06 x=-4.99941e-05 y=-0.000335318 z=-7.76816e-07 kx=0.000936198 ky=-0.000894115 kz=22.7097 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1636e-09 l2=1.33517e-05 x=-4.95521e-05 y=0.000234997 z=-6.67902e-06 kx=-0.00119014 ky=0.00135994 kz=22.8975 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.80645e-09 l2=2.2545e-06 x=4.99874e-05 y=-1.36875e-05 z=-1.12745e-06 kx=-0.000553641 ky=0.000560365 kz=23.0476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25787e-09 l2=2.15358e-05 x=-4.88267e-05 y=-0.000175975 z=-1.07693e-05 kx=-0.000353221 ky=-0.000452101 kz=23.0368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21632e-09 l2=2.81165e-05 x=-4.79834e-05 y=-0.00036071 z=-1.40579e-05 kx=0.000478589 ky=-0.00032867 kz=23.0605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11752e-09 l2=7.17301e-06 x=4.98713e-05 y=0.000341471 z=-3.58681e-06 kx=-0.000336466 ky=0.00128253 kz=22.3927 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04398e-09 l2=1.19377e-05 x=4.96427e-05 y=0.000393003 z=-5.9677e-06 kx=-0.000759912 ky=0.00122766 kz=22.7064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20904e-09 l2=2.5067e-05 x=-4.84037e-05 y=-0.000173185 z=-1.25345e-05 kx=-0.000203099 ky=-0.000792665 kz=22.9726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18599e-09 l2=3.62851e-05 x=4.6593e-05 y=-7.23553e-05 z=-1.81422e-05 kx=-0.000478875 ky=-0.000854454 kz=22.8966 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24949e-09 l2=1.05053e-05 x=-4.97232e-05 y=-6.12146e-05 z=-5.25502e-06 kx=-0.000821267 ky=-0.000492877 kz=23.186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34861e-09 l2=1.40914e-05 x=-4.95012e-05 y=0.000462634 z=-7.04659e-06 kx=-0.000106231 ky=0.000613124 kz=22.3934 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37388e-09 l2=1.72392e-05 x=4.92511e-05 y=0.000125505 z=-8.62272e-06 kx=0.00113392 ky=0.00095515 kz=23.0049 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.26111e-09 l2=7.16644e-06 x=-4.98715e-05 y=-0.00033374 z=-3.58717e-06 kx=-0.00059957 ky=-0.000898246 kz=22.6671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01662e-09 l2=1.20229e-05 x=-4.96371e-05 y=0.000414746 z=-6.01508e-06 kx=-0.00122737 ky=-8.23722e-05 kz=23.2123 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27011e-09 l2=1.03845e-05 x=-4.97295e-05 y=8.40173e-05 z=-5.1951e-06 kx=-0.0010188 ky=-0.000173479 kz=22.8318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48961e-09 l2=9.12891e-06 x=-4.97912e-05 y=-9.87309e-05 z=-4.56636e-06 kx=-0.000529123 ky=0.000783444 kz=22.7999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0634e-09 l2=2.24856e-05 x=-4.87193e-05 y=-0.000149409 z=-1.12452e-05 kx=-0.00087043 ky=0.000247394 kz=22.4468 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51544e-09 l2=3.1731e-05 x=4.74163e-05 y=0.000436631 z=-1.58664e-05 kx=6.36985e-05 ky=0.000715716 kz=22.7443 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6604e-09 l2=1.44703e-05 x=4.94739e-05 y=3.40213e-05 z=-7.23549e-06 kx=-0.000234599 ky=3.88971e-05 kz=23.1301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43391e-09 l2=2.04289e-05 x=4.89458e-05 y=-0.000442692 z=-1.02148e-05 kx=-0.000162469 ky=-0.00129192 kz=22.8009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01512e-09 l2=2.46212e-05 x=4.84607e-05 y=0.0003018 z=-1.23121e-05 kx=0.000451165 ky=0.000547612 kz=22.3774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93797e-09 l2=8.64434e-06 x=-4.98128e-05 y=0.000470837 z=-4.32421e-06 kx=-0.000484951 ky=0.00176064 kz=22.5658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17051e-09 l2=3.44804e-05 x=4.69338e-05 y=9.97192e-05 z=-1.72412e-05 kx=0.000174956 ky=0.00112014 kz=22.7855 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44361e-09 l2=1.09745e-05 x=-4.9698e-05 y=-0.000274722 z=-5.48919e-06 kx=-0.000326643 ky=-0.00115667 kz=22.4197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01475e-09 l2=1.34614e-05 x=-4.95446e-05 y=4.69859e-05 z=-6.7339e-06 kx=-0.00125967 ky=7.55802e-05 kz=23.2768 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.65356e-09 l2=4.74555e-06 x=-4.99437e-05 y=0.000452298 z=-2.37754e-06 kx=-0.00112088 ky=0.00141394 kz=22.9119 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13714e-09 l2=2.04243e-05 x=-4.89465e-05 y=0.000142199 z=-1.0211e-05 kx=0.00081581 ky=-0.000473644 kz=22.6776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34334e-09 l2=8.11065e-06 x=-4.98354e-05 y=-0.00046937 z=-4.05497e-06 kx=0.000468486 ky=-0.000755893 kz=22.6113 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18161e-09 l2=5.36461e-06 x=-4.9928e-05 y=-0.000356503 z=-2.68491e-06 kx=-0.000685781 ky=-0.000771632 kz=22.5671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79631e-09 l2=1.03682e-05 x=-4.97305e-05 y=-0.000403399 z=-5.18651e-06 kx=-0.000698649 ky=-0.00136144 kz=23.1896 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.99714e-09 l2=1.75652e-05 x=-4.92226e-05 y=0.000328175 z=-8.78493e-06 kx=-0.00061083 ky=0.000455011 kz=22.4998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03656e-09 l2=3.24415e-05 x=-4.7296e-05 y=-0.000380379 z=-1.62211e-05 kx=9.64271e-05 ky=-0.000928035 kz=22.5784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.84986e-09 l2=3.54587e-06 x=-4.99685e-05 y=-0.000333632 z=-1.77685e-06 kx=-0.00112668 ky=-0.000260438 kz=22.5996 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0601e-09 l2=1.76342e-05 x=-4.92165e-05 y=-0.000225287 z=-8.81792e-06 kx=-0.000140504 ky=-0.00114449 kz=22.436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53382e-09 l2=2.0996e-05 x=4.88857e-05 y=-0.000215249 z=-1.04985e-05 kx=-0.000115151 ky=0.000227846 kz=22.8389 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.31244e-09 l2=5.30879e-06 x=-4.99296e-05 y=-0.000404484 z=-2.65499e-06 kx=0.000479372 ky=-0.00139596 kz=22.4576 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33056e-09 l2=1.65663e-05 x=-4.93092e-05 y=0.000297157 z=-8.28403e-06 kx=-0.000101662 ky=0.000424671 kz=22.9212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.60239e-09 l2=1.12592e-05 x=4.96823e-05 y=-8.97587e-05 z=-5.6301e-06 kx=-0.000369579 ky=-0.000382355 kz=23.306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00363e-09 l2=2.1252e-05 x=-4.88575e-05 y=0.000142641 z=-1.06284e-05 kx=-0.000874779 ky=0.00114155 kz=22.9382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98079e-09 l2=1.23793e-05 x=-4.96152e-05 y=0.00042632 z=-6.19303e-06 kx=-0.00112173 ky=0.00160213 kz=23.0892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62506e-09 l2=1.62736e-06 x=4.99934e-05 y=-5.36053e-05 z=-8.12538e-07 kx=-0.000897606 ky=-0.00107316 kz=22.9445 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.74915e-09 l2=1.86776e-06 x=-4.99913e-05 y=0.000107081 z=-9.3795e-07 kx=-0.000775397 ky=-0.000525447 kz=22.8676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16925e-09 l2=3.82127e-05 x=4.62051e-05 y=0.000245793 z=-1.91084e-05 kx=0.000743374 ky=0.000181506 kz=22.861 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2208e-09 l2=1.85441e-05 x=4.91329e-05 y=0.000437658 z=-9.27241e-06 kx=-0.00012482 ky=0.000196253 kz=22.6265 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32411e-09 l2=1.82028e-05 x=-4.91652e-05 y=0.000374141 z=-9.10003e-06 kx=0.000922819 ky=0.000249344 kz=22.5772 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1827e-09 l2=4.67995e-06 x=-4.99451e-05 y=0.000277414 z=-2.34294e-06 kx=-0.00107451 ky=-0.000206749 kz=22.6422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49298e-09 l2=1.58928e-05 x=4.93648e-05 y=-0.000432644 z=-7.94618e-06 kx=-0.000439786 ky=-0.00170066 kz=22.4786 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88986e-09 l2=2.16386e-05 x=4.88155e-05 y=0.000236047 z=-1.08205e-05 kx=0.000130362 ky=3.50138e-05 kz=22.8357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24289e-09 l2=8.44131e-06 x=-4.98216e-05 y=0.000449867 z=-4.22241e-06 kx=-0.000286444 ky=0.00207376 kz=22.5984 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01716e-09 l2=2.65332e-05 x=4.82076e-05 y=-0.000370299 z=-1.32687e-05 kx=0.000720531 ky=-0.000909287 kz=22.6155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.9271e-09 l2=1.48575e-05 x=4.94453e-05 y=-8.09283e-06 z=-7.4288e-06 kx=-0.000410983 ky=0.000564182 kz=22.7193 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01524e-09 l2=2.11208e-05 x=4.88726e-05 y=-0.000152134 z=-1.05587e-05 kx=-0.00103357 ky=9.42627e-05 kz=23.1822 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81667e-09 l2=2.0634e-05 x=-4.89244e-05 y=0.000377676 z=-1.03169e-05 kx=0.000452352 ky=0.00173688 kz=22.7894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12892e-09 l2=2.0683e-05 x=4.89188e-05 y=-0.000391371 z=-1.03429e-05 kx=0.000372499 ky=-0.0019248 kz=22.8033 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02545e-09 l2=2.28141e-05 x=-4.86819e-05 y=-0.000209814 z=-1.1406e-05 kx=0.00075643 ky=-0.00060536 kz=23.2595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38248e-09 l2=1.3794e-05 x=-4.95219e-05 y=9.85052e-05 z=-6.89936e-06 kx=-0.000745627 ky=0.00125254 kz=22.3793 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34637e-09 l2=1.38278e-05 x=-4.95198e-05 y=3.5025e-05 z=-6.91456e-06 kx=1.10721e-05 ky=0.000828437 kz=22.4944 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21067e-08 l2=2.10194e-06 x=-4.99891e-05 y=-0.000215066 z=-1.05801e-06 kx=-0.000456215 ky=-0.000161464 kz=23.1083 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.82304e-09 l2=3.55798e-06 x=-4.99684e-05 y=6.88663e-05 z=-1.78409e-06 kx=-0.000536607 ky=0.000946623 kz=22.4913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77844e-09 l2=2.05358e-05 x=-4.89343e-05 y=-0.000385443 z=-1.027e-05 kx=-0.000551613 ky=-0.00112057 kz=22.6545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02494e-09 l2=4.51193e-05 x=-4.46222e-05 y=1.07094e-05 z=-2.25589e-05 kx=0.000636782 ky=0.00065444 kz=22.7025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64249e-09 l2=1.38302e-05 x=4.95196e-05 y=-0.000282913 z=-6.91576e-06 kx=-7.23684e-05 ky=-0.000882352 kz=22.3476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51334e-09 l2=2.02245e-05 x=-4.89671e-05 y=-0.000398864 z=-1.01121e-05 kx=0.000409649 ky=-0.00150488 kz=22.6198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3159e-09 l2=3.83331e-06 x=4.99633e-05 y=0.00049437 z=-1.91701e-06 kx=-0.000136847 ky=0.000288292 kz=22.7721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44637e-09 l2=6.57175e-06 x=4.98919e-05 y=-0.000288512 z=-3.28885e-06 kx=0.000795566 ky=-0.00094089 kz=22.6522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03807e-09 l2=2.40574e-05 x=-4.85317e-05 y=0.000157138 z=-1.2029e-05 kx=0.000118778 ky=-0.000169604 kz=22.5077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.26979e-09 l2=7.1216e-06 x=-4.98731e-05 y=0.000460654 z=-3.56475e-06 kx=-0.000826634 ky=0.00106103 kz=22.649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.18946e-09 l2=9.10508e-06 x=4.97926e-05 y=-0.000258376 z=-4.5532e-06 kx=-0.000667065 ky=-0.00174785 kz=23.1122 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91896e-09 l2=8.42782e-06 x=4.98222e-05 y=0.000490184 z=-4.21437e-06 kx=-0.000222452 ky=0.00114429 kz=22.472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.22979e-09 l2=8.57389e-06 x=-4.9816e-05 y=-0.000444701 z=-4.28729e-06 kx=0.000345434 ky=-0.00204771 kz=22.5495 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68763e-09 l2=1.89669e-05 x=-4.90926e-05 y=6.52413e-05 z=-9.48392e-06 kx=0.000175501 ky=0.00106453 kz=22.5095 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.65909e-09 l2=9.8721e-06 x=4.9756e-05 y=-0.000201785 z=-4.93634e-06 kx=-0.000487922 ky=-0.000835711 kz=23.2941 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68007e-09 l2=1.60916e-05 x=-4.93486e-05 y=-0.000492611 z=-8.0463e-06 kx=0.000152791 ky=-0.000262525 kz=22.7802 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86538e-09 l2=1.76732e-05 x=4.92126e-05 y=0.000180592 z=-8.84016e-06 kx=0.00124688 ky=-0.000400555 kz=23.1506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3606e-09 l2=2.13109e-05 x=-4.8851e-05 y=-0.000164649 z=-1.06586e-05 kx=-0.00112981 ky=0.000731132 kz=22.5912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00014e-09 l2=1.22498e-05 x=4.96235e-05 y=-0.000253222 z=-6.12568e-06 kx=0.000137637 ky=-0.000438034 kz=22.6435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.28769e-09 l2=4.69022e-06 x=-4.99451e-05 y=0.00020091 z=-2.34947e-06 kx=-0.000325183 ky=0.000698506 kz=22.7669 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01544e-09 l2=2.55468e-05 x=4.83406e-05 y=0.000231808 z=-1.27753e-05 kx=0.000665696 ky=0.00119914 kz=22.7255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07776e-09 l2=1.38776e-05 x=4.95163e-05 y=0.00045245 z=-6.93884e-06 kx=-0.00022301 ky=0.000408109 kz=22.3838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02594e-09 l2=3.3522e-05 x=4.71073e-05 y=0.000245761 z=-1.67611e-05 kx=-0.000203347 ky=0.000660181 kz=22.5678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15993e-09 l2=2.49603e-05 x=4.84175e-05 y=0.00022013 z=-1.24808e-05 kx=2.47285e-05 ky=7.72338e-05 kz=23.0363 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09e-09 l2=8.0433e-06 x=4.98378e-05 y=-0.000332195 z=-4.0248e-06 kx=0.00117963 ky=0.000105996 kz=22.5435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32096e-09 l2=2.26099e-05 x=4.87056e-05 y=-0.000461138 z=-1.13047e-05 kx=-0.000442568 ky=-0.00202507 kz=22.6911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60434e-09 l2=9.63901e-06 x=4.97671e-05 y=0.000247503 z=-4.82196e-06 kx=0.000772754 ky=0.00045902 kz=23.2213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63815e-09 l2=1.70229e-05 x=-4.92703e-05 y=0.000213527 z=-8.51264e-06 kx=-0.000161174 ky=0.000154853 kz=22.723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48404e-09 l2=2.52488e-05 x=-4.83798e-05 y=-4.82397e-05 z=-1.26267e-05 kx=-0.000716639 ky=-0.000311574 kz=22.3367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24032e-09 l2=9.89695e-06 x=-4.97546e-05 y=-0.000408501 z=-4.94871e-06 kx=0.000177444 ky=-0.000296709 kz=23.1107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48522e-09 l2=1.43948e-05 x=-4.94796e-05 y=-0.00022637 z=-7.19634e-06 kx=0.000837089 ky=7.35295e-06 kz=23.1913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57915e-09 l2=3.55403e-06 x=4.99685e-05 y=0.000186202 z=-1.77603e-06 kx=-0.00079942 ky=0.000469366 kz=22.5046 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21564e-09 l2=3.50409e-05 x=4.68295e-05 y=-0.000317027 z=-1.75225e-05 kx=0.000702827 ky=-0.00147351 kz=22.6309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14135e-09 l2=1.70288e-05 x=-4.92699e-05 y=0.000470557 z=-8.51466e-06 kx=0.00013585 ky=0.00159645 kz=22.7622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00275e-09 l2=1.31904e-05 x=-4.95633e-05 y=-0.000355214 z=-6.59493e-06 kx=0.000351216 ky=-0.00151168 kz=22.5153 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38364e-09 l2=1.661e-05 x=4.93053e-05 y=-0.00028148 z=-8.30722e-06 kx=0.00070724 ky=-0.000901976 kz=23.0674 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73912e-09 l2=1.3785e-05 x=-4.95229e-05 y=-0.000192884 z=-6.89215e-06 kx=0.000545092 ky=-0.000721164 kz=22.5196 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21367e-09 l2=8.58559e-06 x=-4.98153e-05 y=0.000481049 z=-4.29434e-06 kx=-0.000427704 ky=0.000410697 kz=22.7828 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62502e-09 l2=2.80653e-05 x=-4.79903e-05 y=0.000365652 z=-1.40347e-05 kx=-0.000621039 ky=0.00166886 kz=22.9756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01272e-09 l2=2.92666e-05 x=4.78103e-05 y=0.00020477 z=-1.46357e-05 kx=0.00088497 ky=-0.000322581 kz=22.8676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69541e-09 l2=1.96018e-05 x=4.903e-05 y=-0.000279907 z=-9.80292e-06 kx=0.00054441 ky=0.000486116 kz=22.8909 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37358e-09 l2=1.80809e-05 x=4.91757e-05 y=6.00794e-05 z=-9.04302e-06 kx=0.000895029 ky=-0.000664743 kz=23.1484 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05906e-09 l2=4.06549e-05 x=-4.56819e-05 y=0.000288485 z=-2.03275e-05 kx=0.000254974 ky=0.000580288 kz=23.0039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.20497e-09 l2=1.4728e-06 x=4.99946e-05 y=-0.000400299 z=-7.42481e-07 kx=0.00112854 ky=-0.00118048 kz=22.7638 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13851e-09 l2=2.24351e-05 x=4.87256e-05 y=-0.000367082 z=-1.12177e-05 kx=-0.000173903 ky=-0.000227264 kz=22.9174 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98017e-08 l2=1.01314e-06 x=4.99976e-05 y=0.000210904 z=-5.23826e-07 kx=0.00108974 ky=0.000545912 kz=23.1329 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26371e-09 l2=1.61759e-05 x=-4.93417e-05 y=-0.000374061 z=-8.08821e-06 kx=0.000168991 ky=-0.00201196 kz=23.0441 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08475e-09 l2=2.18024e-05 x=4.87974e-05 y=-8.30749e-06 z=-1.09013e-05 kx=-0.000225535 ky=0.00101754 kz=23.0587 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75125e-09 l2=6.22761e-06 x=4.99031e-05 y=-0.000321736 z=-3.11366e-06 kx=-0.000690584 ky=-0.0012259 kz=22.6128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36013e-09 l2=1.02464e-05 x=-4.9737e-05 y=-0.000348075 z=-5.12342e-06 kx=0.000202198 ky=-0.000423559 kz=22.8319 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0152e-09 l2=4.41436e-05 x=4.4865e-05 y=0.0002345 z=-2.20721e-05 kx=-9.61672e-05 ky=0.000135476 kz=22.8684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01568e-09 l2=6.93672e-06 x=-4.98798e-05 y=0.000418198 z=-3.46729e-06 kx=0.000947964 ky=0.000577796 kz=22.7208 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.40392e-09 l2=7.10395e-06 x=4.98737e-05 y=0.00016157 z=-3.55575e-06 kx=0.00071658 ky=0.000465938 kz=22.7048 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66837e-09 l2=1.10866e-05 x=4.96918e-05 y=0.000232913 z=-5.54458e-06 kx=0.000215202 ky=0.00111687 kz=23.1858 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2042e-09 l2=3.16228e-05 x=-4.74344e-05 y=0.000185077 z=-1.5812e-05 kx=-2.19324e-05 ky=-0.000380153 kz=22.7278 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08562e-09 l2=3.039e-05 x=4.76348e-05 y=-0.000334676 z=-1.51975e-05 kx=0.000907708 ky=-0.000322605 kz=22.401 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26819e-09 l2=1.94719e-05 x=-4.90427e-05 y=-6.69371e-05 z=-9.73865e-06 kx=-0.000968022 ky=-0.000675412 kz=22.8703 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.37537e-09 l2=5.70779e-06 x=4.99185e-05 y=-0.00045235 z=-2.85834e-06 kx=0.000813113 ky=-0.000202626 kz=23.1684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34584e-09 l2=1.34747e-05 x=4.95441e-05 y=-0.000344148 z=-6.73818e-06 kx=7.7601e-05 ky=-0.00127149 kz=23.2534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33291e-09 l2=7.1467e-06 x=-4.98722e-05 y=-0.000106167 z=-3.57489e-06 kx=-0.000174867 ky=-0.00133663 kz=23.1731 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50437e-09 l2=5.55436e-06 x=4.99229e-05 y=0.000328378 z=-2.77779e-06 kx=-6.75912e-05 ky=-0.000329515 kz=22.9372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13591e-09 l2=2.03448e-05 x=-4.89549e-05 y=0.000477022 z=-1.01708e-05 kx=0.00100633 ky=0.00198412 kz=22.7862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56042e-09 l2=1.52502e-05 x=4.94156e-05 y=-0.000156516 z=-7.62367e-06 kx=-0.00104273 ky=-0.000367194 kz=23.2244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26702e-09 l2=1.52325e-05 x=-4.94167e-05 y=-0.000268304 z=-7.61659e-06 kx=0.00014061 ky=-0.00100348 kz=22.7171 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20195e-09 l2=2.79795e-05 x=-4.80031e-05 y=0.000425248 z=-1.39905e-05 kx=-7.46831e-05 ky=0.000709206 kz=22.6124 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56068e-09 l2=4.58625e-06 x=-4.99475e-05 y=0.000332318 z=-2.29232e-06 kx=0.000710664 ky=0.000259768 kz=22.4038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35688e-09 l2=2.07087e-05 x=4.89166e-05 y=0.000369046 z=-1.03537e-05 kx=-0.000646289 ky=0.000342665 kz=22.7539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34725e-09 l2=4.78647e-06 x=4.99428e-05 y=0.000355887 z=-2.39327e-06 kx=-0.000295907 ky=0.00185248 kz=23.037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21134e-09 l2=9.91757e-06 x=4.97535e-05 y=-0.000110345 z=-4.96198e-06 kx=0.000738675 ky=-0.00103858 kz=23.1286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75984e-09 l2=1.18392e-05 x=4.96486e-05 y=-1.68644e-05 z=-5.92023e-06 kx=-0.000353427 ky=-0.000687728 kz=22.8374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64955e-09 l2=1.13631e-05 x=-4.96764e-05 y=0.000259475 z=-5.68132e-06 kx=0.000485386 ky=1.29556e-05 kz=22.8644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.0225e-09 l2=1.15323e-05 x=-4.96667e-05 y=-0.000305747 z=-5.76749e-06 kx=0.000315457 ky=-0.00107332 kz=23.1184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32293e-09 l2=3.74896e-06 x=-4.99649e-05 y=-0.000313248 z=-1.8758e-06 kx=-0.000304549 ky=-0.0014237 kz=23.061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0383e-09 l2=2.81209e-05 x=-4.79829e-05 y=0.000284498 z=-1.40597e-05 kx=0.000607888 ky=0.00148361 kz=22.9635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85944e-09 l2=7.8494e-06 x=4.98457e-05 y=0.000383018 z=-3.92815e-06 kx=0.000908109 ky=0.00110959 kz=22.3999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00642e-09 l2=1.52268e-05 x=-4.94171e-05 y=-4.68987e-05 z=-7.61444e-06 kx=-1.63289e-05 ky=9.28812e-05 kz=22.8429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.44044e-09 l2=6.86091e-06 x=-4.98824e-05 y=8.16684e-05 z=-3.43215e-06 kx=0.000239974 ky=-0.000284459 kz=22.9368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00949e-09 l2=2.56135e-05 x=4.83327e-05 y=-0.000365512 z=-1.28051e-05 kx=-0.000992051 ky=0.000236737 kz=22.9571 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.31263e-09 l2=1.23081e-05 x=4.962e-05 y=0.000182586 z=-6.15464e-06 kx=-0.000252545 ky=0.00148994 kz=23.1559 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19196e-09 l2=1.49096e-05 x=4.94409e-05 y=-0.000428108 z=-7.4578e-06 kx=0.0010837 ky=-0.000648516 kz=22.35 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24444e-09 l2=1.1207e-05 x=4.96849e-05 y=-0.000494553 z=-5.60701e-06 kx=0.00109012 ky=-0.000889439 kz=22.61 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.29101e-09 l2=4.60042e-06 x=-4.99472e-05 y=-1.31234e-05 z=-2.30155e-06 kx=0.000594828 ky=-7.0912e-05 kz=22.7129 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10412e-09 l2=1.98252e-05 x=-4.90075e-05 y=-0.000399239 z=-9.91419e-06 kx=-0.000487027 ky=-0.00150285 kz=22.6941 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.24351e-09 l2=9.61318e-06 x=-4.97683e-05 y=-0.000173351 z=-4.81088e-06 kx=-0.00122114 ky=-0.000503997 kz=22.781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77744e-09 l2=1.33556e-05 x=4.95521e-05 y=0.000380608 z=-6.67953e-06 kx=0.000399026 ky=0.00111824 kz=22.9148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00737e-09 l2=1.30585e-05 x=4.95722e-05 y=3.73835e-05 z=-6.52797e-06 kx=-0.000848498 ky=8.13318e-05 kz=23.2509 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20919e-09 l2=2.58738e-05 x=-4.8298e-05 y=0.000174503 z=-1.29356e-05 kx=0.000906982 ky=0.000231399 kz=23.2974 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71687e-09 l2=2.28708e-06 x=-4.99869e-05 y=-0.000319494 z=-1.14664e-06 kx=-0.000787066 ky=-0.001393 kz=22.5981 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46324e-09 l2=1.42209e-05 x=4.94922e-05 y=-0.00046957 z=-7.10909e-06 kx=-0.000957774 ky=-0.00206313 kz=22.8758 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0297e-09 l2=2.04084e-05 x=-4.89475e-05 y=0.000432046 z=-1.02061e-05 kx=-0.000644612 ky=-9.30569e-06 kz=22.9692 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19429e-09 l2=1.32364e-05 x=4.956e-05 y=8.19344e-05 z=-6.61992e-06 kx=0.00052655 ky=-0.000774708 kz=23.1149 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01651e-09 l2=3.04975e-05 x=-4.76188e-05 y=-0.000295417 z=-1.52474e-05 kx=0.000860271 ky=-0.00177549 kz=22.6395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52261e-09 l2=2.1285e-05 x=-4.88545e-05 y=-0.000146104 z=-1.0643e-05 kx=0.000136194 ky=-0.000939896 kz=22.695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.97949e-09 l2=4.95744e-06 x=4.99386e-05 y=-0.000342986 z=-2.48221e-06 kx=0.000228347 ky=-0.00126368 kz=22.8768 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03736e-09 l2=1.15885e-05 x=-4.96635e-05 y=0.00019331 z=-5.79326e-06 kx=0.000931153 ky=-0.000535089 kz=23.2539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.82546e-09 l2=8.61018e-06 x=4.98144e-05 y=0.000137729 z=-4.30781e-06 kx=0.000362445 ky=0.000731144 kz=22.3276 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1527e-09 l2=3.79749e-05 x=-4.62542e-05 y=-0.000116833 z=-1.89892e-05 kx=-0.000624079 ky=-0.00131589 kz=23.3109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24693e-09 l2=2.06653e-05 x=4.89206e-05 y=0.000385173 z=-1.03342e-05 kx=0.000432095 ky=0.00164579 kz=22.317 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70696e-09 l2=1.73513e-05 x=-4.92415e-05 y=0.000283948 z=-8.67802e-06 kx=-0.000702579 ky=0.000516773 kz=23.0893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13569e-09 l2=3.73416e-05 x=-4.6383e-05 y=-5.40085e-05 z=-1.86723e-05 kx=-0.000468679 ky=0.000868839 kz=22.4956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.57848e-09 l2=4.11766e-06 x=-4.99577e-05 y=-4.89555e-06 z=-2.06127e-06 kx=-6.67955e-05 ky=-0.000839867 kz=22.818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.20244e-09 l2=1.17488e-05 x=4.96536e-05 y=0.000485127 z=-5.8777e-06 kx=0.00101019 ky=0.000906271 kz=22.8119 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04017e-09 l2=2.7365e-05 x=4.80917e-05 y=2.22978e-05 z=-1.36828e-05 kx=-9.88325e-05 ky=0.000245595 kz=22.7825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52564e-09 l2=1.30833e-05 x=4.95706e-05 y=0.00038898 z=-6.54063e-06 kx=-0.000833843 ky=0.00149999 kz=23.0884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75793e-09 l2=1.99351e-05 x=-4.89965e-05 y=-0.000206674 z=-9.96909e-06 kx=-0.000313902 ky=-0.00145672 kz=22.7798 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41115e-09 l2=2.21457e-05 x=-4.87583e-05 y=-0.00042755 z=-1.10751e-05 kx=-0.000728781 ky=-0.00098882 kz=22.6774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88841e-09 l2=2.01182e-05 x=-4.89782e-05 y=5.10977e-05 z=-1.00583e-05 kx=0.000795458 ky=7.11408e-05 kz=22.701 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16539e-09 l2=1.84751e-05 x=4.91391e-05 y=-0.000441481 z=-9.23963e-06 kx=0.000699622 ky=-0.00189015 kz=23.0539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33068e-09 l2=2.26221e-05 x=-4.87039e-05 y=0.000409261 z=-1.13121e-05 kx=-0.000178614 ky=0.000977534 kz=22.8039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.62486e-08 l2=4.23207e-07 x=4.99996e-05 y=-0.000289605 z=-2.3628e-07 kx=0.000713388 ky=-0.000160716 kz=22.9832 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06254e-09 l2=2.2716e-05 x=4.86927e-05 y=-0.000409987 z=-1.13599e-05 kx=0.000614037 ky=-0.00137114 kz=22.752 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.63404e-09 l2=4.67283e-06 x=-4.99455e-05 y=-0.000370449 z=-2.33774e-06 kx=0.000224446 ky=-0.000463337 kz=22.8111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10282e-09 l2=1.8258e-05 x=4.91596e-05 y=0.000393461 z=-9.12957e-06 kx=1.20615e-05 ky=0.000245364 kz=22.334 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13098e-09 l2=2.65805e-05 x=-4.82013e-05 y=-0.000174426 z=-1.32915e-05 kx=-0.000297279 ky=-0.000200782 kz=22.7079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05531e-09 l2=1.21134e-05 x=4.96318e-05 y=0.000412557 z=-6.05895e-06 kx=0.000563481 ky=0.000811399 kz=23.3082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35537e-09 l2=1.87205e-05 x=4.91164e-05 y=1.33303e-05 z=-9.35976e-06 kx=-0.000534848 ky=0.000613176 kz=23.0038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64172e-09 l2=1.98349e-05 x=-4.90069e-05 y=9.91831e-05 z=-9.91759e-06 kx=0.000318697 ky=-0.000144966 kz=22.4398 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31538e-09 l2=1.02341e-05 x=4.97377e-05 y=7.5663e-05 z=-5.11585e-06 kx=-0.000829425 ky=0.000638916 kz=22.3183 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38442e-09 l2=5.33928e-06 x=4.99288e-05 y=0.000404759 z=-2.66969e-06 kx=-0.000522977 ky=0.00119651 kz=22.8748 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08718e-09 l2=1.52575e-05 x=4.94149e-05 y=0.000488016 z=-7.62782e-06 kx=-0.000692164 ky=0.000261273 kz=23.06 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01256e-09 l2=1.93616e-05 x=-4.90538e-05 y=0.00045008 z=-9.68222e-06 kx=-0.000411413 ky=0.00144645 kz=22.3903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3321e-09 l2=4.87861e-06 x=4.99405e-05 y=0.000113765 z=-2.43993e-06 kx=-1.80091e-05 ky=0.000666178 kz=22.3027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42997e-09 l2=1.61368e-05 x=4.93446e-05 y=-0.000166088 z=-8.07054e-06 kx=0.000654036 ky=-0.000916845 kz=22.9735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14868e-09 l2=1.46525e-05 x=-4.94604e-05 y=-0.000386489 z=-7.32703e-06 kx=-9.69493e-05 ky=-0.00128395 kz=23.2462 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92177e-09 l2=1.14718e-05 x=-4.96703e-05 y=0.000317043 z=-5.73479e-06 kx=0.000933058 ky=0.00142951 kz=22.5935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03067e-09 l2=2.31431e-05 x=-4.86427e-05 y=0.000173458 z=-1.1573e-05 kx=-0.000190395 ky=0.000243801 kz=22.7124 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16328e-09 l2=5.31256e-06 x=4.99294e-05 y=0.000149606 z=-2.65807e-06 kx=0.000546281 ky=0.00145009 kz=22.5195 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00319e-09 l2=3.9837e-05 x=4.58617e-05 y=0.000306023 z=-1.99186e-05 kx=-0.000234809 ky=0.000414328 kz=22.8668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03917e-09 l2=3.99434e-06 x=4.99601e-05 y=-0.000484513 z=-1.99764e-06 kx=-2.10874e-05 ky=-0.00030557 kz=22.5133 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.91645e-09 l2=7.03838e-06 x=4.98761e-05 y=-0.000419324 z=-3.52152e-06 kx=0.000167376 ky=-0.00155182 kz=22.4652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52957e-09 l2=1.52475e-05 x=4.94155e-05 y=-0.000246207 z=-7.62461e-06 kx=4.99498e-05 ky=-4.67661e-06 kz=22.3722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.36144e-09 l2=2.07055e-06 x=4.99894e-05 y=0.000101929 z=-1.03676e-06 kx=-0.000536779 ky=0.000296762 kz=22.5059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17341e-09 l2=1.79418e-05 x=-4.91891e-05 y=-5.18685e-05 z=-8.96957e-06 kx=0.000888303 ky=0.000628208 kz=22.7374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48959e-09 l2=1.35578e-05 x=-4.95385e-05 y=0.000357688 z=-6.7789e-06 kx=0.000327297 ky=0.000817412 kz=22.4892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44034e-09 l2=1.94297e-05 x=4.9047e-05 y=-0.000357657 z=-9.71712e-06 kx=0.000701689 ky=0.000130507 kz=22.5621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00147e-09 l2=1.37754e-05 x=-4.95235e-05 y=-3.10214e-05 z=-6.88828e-06 kx=0.000188659 ky=-0.000932269 kz=22.8154 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14065e-09 l2=5.92778e-06 x=4.99121e-05 y=3.03039e-05 z=-2.96523e-06 kx=0.000124677 ky=-0.000685431 kz=22.7622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11476e-09 l2=9.47975e-06 x=4.9775e-05 y=0.000193652 z=-4.74033e-06 kx=-0.000273007 ky=0.000743309 kz=22.5225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46962e-09 l2=1.357e-05 x=4.95373e-05 y=-0.000113308 z=-6.78806e-06 kx=0.00105807 ky=2.51838e-07 kz=22.4725 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25598e-09 l2=9.53276e-06 x=4.97725e-05 y=0.000189243 z=-4.76536e-06 kx=-0.000738126 ky=0.000814702 kz=22.3348 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60025e-09 l2=8.15983e-06 x=4.98332e-05 y=5.9241e-06 z=-4.08201e-06 kx=0.00060203 ky=-0.00114086 kz=23.192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5791e-09 l2=1.04654e-05 x=-4.97257e-05 y=-0.000392986 z=-5.23204e-06 kx=0.000686558 ky=-0.00100671 kz=23.1533 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1895e-09 l2=2.54686e-05 x=4.83512e-05 y=0.000483854 z=-1.27356e-05 kx=0.000327882 ky=0.00141076 kz=22.8197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17903e-09 l2=2.90174e-05 x=-4.78493e-05 y=-4.24231e-06 z=-1.45079e-05 kx=0.000656421 ky=0.000957343 kz=22.4249 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04319e-09 l2=1.41359e-05 x=4.9498e-05 y=-0.000363493 z=-7.06823e-06 kx=-0.000111059 ky=-1.12937e-05 kz=22.5279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13921e-09 l2=3.74874e-05 x=4.63538e-05 y=0.000304069 z=-1.87448e-05 kx=0.000221394 ky=0.000306214 kz=22.3011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.73881e-09 l2=8.89346e-06 x=-4.98021e-05 y=0.000452865 z=-4.44694e-06 kx=0.000544662 ky=0.00176008 kz=23.2977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11304e-09 l2=3.1331e-05 x=4.74829e-05 y=-3.79096e-05 z=-1.56656e-05 kx=-0.000240242 ky=-0.000616531 kz=22.7435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66274e-09 l2=1.06031e-05 x=4.97181e-05 y=-0.000153348 z=-5.3037e-06 kx=0.000626776 ky=-0.000881086 kz=23.1396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73493e-09 l2=5.36119e-06 x=-4.99282e-05 y=0.000443995 z=-2.67949e-06 kx=0.000885541 ky=5.8162e-05 kz=22.3808 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83573e-09 l2=1.32882e-05 x=-4.95569e-05 y=7.80959e-05 z=-6.64358e-06 kx=0.000640724 ky=0.000278711 kz=22.4659 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07007e-09 l2=2.29174e-05 x=-4.86688e-05 y=0.000282465 z=-1.14616e-05 kx=-0.00113648 ky=0.000752274 kz=22.7965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59934e-09 l2=1.93979e-05 x=-4.90504e-05 y=-0.00021974 z=-9.70015e-06 kx=-0.000172385 ky=-0.000915221 kz=22.5989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.52816e-08 l2=4.10901e-07 x=4.99997e-05 y=-0.000196319 z=-2.32169e-07 kx=-0.000426821 ky=-0.000922968 kz=23.1445 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3302e-09 l2=2.76787e-05 x=-4.80468e-05 y=0.000365973 z=-1.38398e-05 kx=0.000117917 ky=0.000839429 kz=22.524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33555e-09 l2=9.70695e-06 x=4.97638e-05 y=-0.000409916 z=-4.85606e-06 kx=0.000886856 ky=-0.00159086 kz=22.9655 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02754e-09 l2=4.02764e-06 x=4.99595e-05 y=-0.000202823 z=-2.01381e-06 kx=-0.000236069 ky=-0.00103499 kz=22.567 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89373e-09 l2=1.51786e-05 x=-4.94211e-05 y=-7.00576e-05 z=-7.58808e-06 kx=0.00100411 ky=-0.00127413 kz=23.0201 Single_crystal: sample: Error message was repeated 2026 times with absorbed x-rays. Warning: 155906 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15121 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2072 times with absorbed x-rays. Warning: 156460 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15080 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2044 times with absorbed x-rays. Warning: 156201 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15029 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2121 times with absorbed x-rays. Warning: 156357 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15184 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2114 times with absorbed x-rays. Warning: 156112 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15128 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2074 times with absorbed x-rays. Warning: 156060 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15100 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2071 times with absorbed x-rays. Warning: 156280 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 14900 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2122 times with absorbed x-rays. Warning: 155717 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15040 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2108 times with absorbed x-rays. Warning: 155682 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15229 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: psd0_I=7.95775e-10 psd0_ERR=1.1254e-13 psd0_N=5e+07 "psd0.dat" Single_crystal: sample: Error message was repeated 2076 times with absorbed x-rays. Warning: 156726 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15103 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2061 times with absorbed x-rays. Warning: 156798 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15196 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2115 times with absorbed x-rays. Warning: 155853 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15048 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: psd4pi_I=1.01869e-17 psd4pi_ERR=5.34687e-21 psd4pi_N=4.96793e+06 "psd4pi.dat" Detector: detector_I=6.85704e-19 detector_ERR=1.38502e-21 detector_N=332938 "psd1.dat" Single_crystal: sample: Error message was repeated 2100 times with absorbed x-rays. Warning: 156039 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 14855 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2114 times with absorbed x-rays. Warning: 156581 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15051 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: detector2_I=1.74914e-21 detector2_ERR=6.96392e-23 detector2_N=857 "psd2.dat" Single_crystal: sample: Error message was repeated 2041 times with absorbed x-rays. Warning: 156528 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 14889 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 2032 times with absorbed x-rays. Warning: 156165 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 15061 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). INFO: Placing instr file copy /home/nexmap/pkwi/xTESTS/2022-12-01/McXtrace-1.x_CPU_MPICC_5e7/Test_SX/Test_SX.instr in dataset 1