loading system configuration loading override configuration from /zhome/89/0/38697/mxtest/mctest/../mccodelib/mcxtrace-test/McXtrace-1.x_CPU_MPICC/mccode_config.json INFO: Using directory: "1" INFO: Using existing c-file: ./Test_SX.c INFO: Using existing binary: ./Test_SX.out INFO: === INFO: Using system default number of mpirun -np processes -------------------------------------------------------------------------- By default, for Open MPI 4.0 and later, infiniband ports on a device are not used by default. The intent is to use UCX for these devices. You can override this policy by setting the btl_openib_allow_ib MCA parameter to true. Local host: n-62-29-31 Local adapter: mlx4_0 Local port: 1 -------------------------------------------------------------------------- -------------------------------------------------------------------------- WARNING: There was an error initializing an OpenFabrics device. Local host: n-62-29-31 Local device: mlx4_0 -------------------------------------------------------------------------- Simulation 'Test_SX' (/zhome/89/0/38697/xTESTS/2022-12-01/McXtrace-1.x_CPU_MPICC_1e7/Test_SX/Test_SX.instr): running on 10 nodes (master is 'n-62-29-31', MPI version 3.1). Opening input file '/zhome/89/0/38697/McXtrace/mcxtrace/1.x-dev/tools/Python/mxrun/../mccodelib/../../../data/Mo.lau' (Table_Read_Offset) Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Opening input file '/zhome/89/0/38697/McXtrace/mcxtrace/1.x-dev/tools/Python/mxrun/../mccodelib/../../../data/Mo.txt' (Table_Read_Offset) atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02356e-09 l2=4.26366e-05 x=-4.52282e-05 y=8.06938e-05 z=-2.13179e-05 kx=0.000459714 ky=-0.000456436 kz=23.1367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04161e-09 l2=2.18688e-05 x=-4.87903e-05 y=0.000248549 z=-1.09328e-05 kx=0.00101568 ky=0.000386805 kz=23.2768 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4373e-09 l2=1.66192e-05 x=-4.93049e-05 y=0.000411844 z=-8.30969e-06 kx=0.00028887 ky=0.000867373 kz=23.2934 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29042e-09 l2=2.29245e-05 x=-4.86691e-05 y=-0.000289221 z=-1.14608e-05 kx=0.000978567 ky=-0.00170381 kz=23.0309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7058e-09 l2=1.08271e-05 x=4.9706e-05 y=-0.000446298 z=-5.41635e-06 kx=0.000885927 ky=-0.000666345 kz=22.9166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27342e-09 l2=3.40941e-05 x=4.70044e-05 y=0.000249907 z=-1.70479e-05 kx=0.000120871 ky=6.74918e-05 kz=22.981 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04441e-09 l2=3.09684e-05 x=4.75422e-05 y=0.000268633 z=-1.54844e-05 kx=-0.000149727 ky=0.000128001 kz=23.2858 atomic_weight 95.94 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33712e-09 l2=5.60421e-06 x=-4.99214e-05 y=3.80232e-05 z=-2.80564e-06 kx=-0.00109801 ky=0.000502539 kz=23.2135 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56739e-09 l2=7.34185e-06 x=-4.98652e-05 y=4.48838e-05 z=-3.67089e-06 kx=0.000374873 ky=0.000356032 kz=22.951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23674e-09 l2=2.18834e-05 x=4.8788e-05 y=-0.000416333 z=-1.09434e-05 kx=0.000514215 ky=-0.00153222 kz=23.0273 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29434e-09 l2=2.71344e-05 x=4.81243e-05 y=-0.000346899 z=-1.35678e-05 kx=1.07934e-06 ky=-0.00166887 kz=22.4847 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43417e-09 l2=1.18723e-05 x=4.96464e-05 y=-0.000231532 z=-5.93694e-06 kx=3.9221e-05 ky=0.000498857 kz=22.512 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68096e-09 l2=6.74138e-06 x=-4.98863e-05 y=0.000445714 z=-3.37153e-06 kx=2.16716e-07 ky=0.00124584 kz=22.3299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78644e-09 l2=2.75442e-06 x=4.99811e-05 y=-3.58751e-05 z=-1.37763e-06 kx=-0.000214769 ky=-0.000296864 kz=22.488 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07561e-09 l2=8.90283e-06 x=-4.98017e-05 y=0.000360671 z=-4.44985e-06 kx=0.000957623 ky=0.00156901 kz=22.6866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06697e-09 l2=9.83045e-06 x=-4.9758e-05 y=-0.000133811 z=-4.91471e-06 kx=0.000477305 ky=0.000361688 kz=22.6644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46482e-09 l2=1.06924e-05 x=-4.97136e-05 y=0.000205493 z=-5.34512e-06 kx=0.000831735 ky=0.000678013 kz=23.0298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.20834e-09 l2=8.47959e-06 x=-4.98201e-05 y=-0.000329058 z=-4.24016e-06 kx=0.000342612 ky=-9.40944e-05 kz=23.0736 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39322e-09 l2=1.80281e-05 x=4.91813e-05 y=0.000477415 z=-9.0127e-06 kx=-0.000955677 ky=0.00224344 kz=23.1699 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89115e-09 l2=9.39141e-06 x=-4.97791e-05 y=3.49085e-05 z=-4.69701e-06 kx=-0.000167377 ky=-0.00104276 kz=22.9729 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16458e-08 l2=9.30464e-07 x=-4.99979e-05 y=-0.000309336 z=-4.77319e-07 kx=-0.000573188 ky=0.000275601 kz=22.6646 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71608e-09 l2=1.13379e-05 x=-4.96776e-05 y=0.000246824 z=-5.67132e-06 kx=-0.000467991 ky=0.000913053 kz=22.7644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12421e-09 l2=2.02537e-05 x=-4.89643e-05 y=0.000255808 z=-1.01253e-05 kx=0.00100163 ky=0.00158689 kz=22.8903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00351e-09 l2=1.17408e-05 x=-4.96544e-05 y=0.000474581 z=-5.86938e-06 kx=0.000688705 ky=0.00209544 kz=22.6907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34898e-09 l2=3.98033e-06 x=-4.99604e-05 y=0.000137508 z=-1.98983e-06 kx=0.000457658 ky=-0.000436673 kz=22.7527 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16507e-09 l2=1.75466e-05 x=4.92241e-05 y=0.000178926 z=-8.77525e-06 kx=0.000612886 ky=0.00139037 kz=22.3414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91199e-09 l2=2.01547e-05 x=-4.89742e-05 y=0.000221498 z=-1.0078e-05 kx=0.00011333 ky=0.00110529 kz=22.595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49861e-09 l2=1.65448e-05 x=-4.93108e-05 y=-8.71468e-05 z=-8.27438e-06 kx=-0.000580487 ky=-0.000294596 kz=22.8277 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.064e-09 l2=2.42974e-05 x=-4.85011e-05 y=-0.000286749 z=-1.21518e-05 kx=-0.00122006 ky=-0.000928055 kz=22.643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03032e-08 l2=1.47955e-06 x=4.99946e-05 y=-0.000302641 z=-7.4387e-07 kx=-0.000483976 ky=-0.000571839 kz=22.9014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.91022e-09 l2=3.68744e-06 x=-4.99661e-05 y=-7.56921e-06 z=-1.84522e-06 kx=0.000440349 ky=-0.000910726 kz=22.916 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31713e-09 l2=1.88152e-05 x=-4.91069e-05 y=-9.44147e-05 z=-9.40929e-06 kx=-0.000470143 ky=0.000111697 kz=22.7258 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6162e-09 l2=2.06275e-05 x=-4.89251e-05 y=0.000394651 z=-1.03133e-05 kx=0.000573533 ky=-4.70859e-05 kz=22.3529 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07753e-09 l2=1.85921e-05 x=-4.91283e-05 y=0.000141219 z=-9.29678e-06 kx=-7.97246e-05 ky=0.00101242 kz=23.0554 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02911e-09 l2=2.82564e-05 x=4.79622e-05 y=-0.000289878 z=-1.41298e-05 kx=0.000521325 ky=-0.00158205 kz=22.329 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2746e-09 l2=2.04016e-05 x=-4.89489e-05 y=-0.00017122 z=-1.01996e-05 kx=0.0008387 ky=0.000186615 kz=22.3472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87877e-09 l2=6.20866e-06 x=4.99037e-05 y=-0.000291721 z=-3.10369e-06 kx=-0.000714898 ky=-0.00126428 kz=22.635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27276e-09 l2=2.68021e-05 x=-4.81714e-05 y=-0.000151278 z=-1.33997e-05 kx=0.00093528 ky=-0.00020577 kz=22.9769 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.38516e-09 l2=4.82449e-06 x=4.99419e-05 y=-0.000439956 z=-2.41122e-06 kx=-0.00102896 ky=-0.00138929 kz=23.1493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21809e-09 l2=2.80175e-05 x=4.79974e-05 y=-6.96512e-05 z=-1.401e-05 kx=0.000299174 ky=-0.00107746 kz=22.8818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28665e-09 l2=2.51028e-05 x=4.83989e-05 y=0.000302422 z=-1.2553e-05 kx=0.000472055 ky=-0.000320798 kz=23.2774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.96687e-09 l2=5.24816e-06 x=-4.99312e-05 y=-0.000151209 z=-2.62675e-06 kx=-0.000316069 ky=0.000528531 kz=22.7836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07727e-09 l2=1.88419e-05 x=4.91043e-05 y=0.000295422 z=-9.42285e-06 kx=0.000621964 ky=0.00144484 kz=22.4031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85898e-09 l2=7.23528e-06 x=-4.9869e-05 y=-0.000386903 z=-3.61928e-06 kx=-9.35251e-05 ky=-0.000355667 kz=22.7417 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11407e-09 l2=1.97765e-05 x=-4.90129e-05 y=0.000101449 z=-9.88723e-06 kx=0.00075486 ky=-0.000600352 kz=23.0747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1988e-09 l2=1.66639e-05 x=-4.9301e-05 y=0.00010183 z=-8.33243e-06 kx=4.45042e-05 ky=0.000803789 kz=22.5072 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.34754e-09 l2=2.60994e-06 x=4.99829e-05 y=0.000170987 z=-1.30918e-06 kx=0.00116482 ky=0.00103022 kz=22.9879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25703e-09 l2=1.24059e-05 x=-4.96138e-05 y=0.000309521 z=-6.20379e-06 kx=-8.82093e-05 ky=0.00085341 kz=22.4002 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.891e-09 l2=2.09629e-05 x=-4.88896e-05 y=0.000391365 z=-1.04809e-05 kx=0.000717804 ky=0.00191532 kz=22.6374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66484e-09 l2=9.69485e-06 x=4.97644e-05 y=-0.000386149 z=-4.84932e-06 kx=0.000491336 ky=-0.000938826 kz=22.9328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67455e-09 l2=2.7955e-05 x=4.80061e-05 y=-0.000218541 z=-1.39806e-05 kx=0.00108491 ky=-0.00137252 kz=22.9845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10698e-09 l2=1.08865e-05 x=4.9703e-05 y=-6.97037e-05 z=-5.44314e-06 kx=-0.000303403 ky=-0.00122908 kz=22.4948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.29527e-09 l2=5.7667e-06 x=-4.99168e-05 y=-7.38927e-05 z=-2.88601e-06 kx=-0.000694606 ky=0.000416101 kz=22.9823 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18819e-09 l2=2.17375e-05 x=-4.8804e-05 y=-4.2974e-05 z=-1.08719e-05 kx=-0.00122264 ky=-0.000201727 kz=23.2164 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.75903e-09 l2=5.8832e-06 x=-4.99135e-05 y=0.000406639 z=-2.94429e-06 kx=-0.000377722 ky=0.00123137 kz=23.2556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.42349e-09 l2=1.45589e-05 x=-4.94676e-05 y=4.27672e-05 z=-7.27972e-06 kx=0.000432696 ky=0.000524788 kz=22.6756 atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56268e-09 l2=1.60625e-05 x=4.93507e-05 y=3.94924e-05 z=-8.03314e-06 kx=0.000511465 ky=0.00125119 kz=23.2863 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00221e-09 l2=8.75374e-06 x=4.98083e-05 y=0.000208981 z=-4.37552e-06 kx=-0.000854156 ky=0.000131707 kz=22.9328 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01819e-09 l2=2.16949e-05 x=-4.88094e-05 y=-0.000497898 z=-1.08472e-05 kx=0.000369733 ky=-0.000112415 kz=23.225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01479e-09 l2=2.18547e-05 x=-4.87909e-05 y=0.000114238 z=-1.09302e-05 kx=-0.00108531 ky=-0.00080606 kz=22.4228 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46016e-09 l2=8.71946e-06 x=-4.98095e-05 y=3.61723e-05 z=-4.36322e-06 kx=-0.0010343 ky=0.00109093 kz=22.7852 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49973e-09 l2=2.77432e-05 x=-4.80381e-05 y=-0.000156618 z=-1.38702e-05 kx=0.000989357 ky=-0.000971457 kz=22.4791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07953e-09 l2=2.02344e-05 x=-4.89655e-05 y=-0.000482129 z=-1.01192e-05 kx=-0.000699463 ky=-0.00122463 kz=23.3074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.193e-09 l2=1.09394e-05 x=4.96998e-05 y=0.000309701 z=-5.47264e-06 kx=0.000844453 ky=0.00104664 kz=22.8034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04545e-09 l2=2.57608e-05 x=4.83131e-05 y=0.000315847 z=-1.28793e-05 kx=-0.000795581 ky=0.00034824 kz=22.912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05343e-09 l2=3.12147e-05 x=-4.75022e-05 y=-0.000259837 z=-1.56069e-05 kx=0.00047623 ky=3.81547e-05 kz=23.3003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13379e-09 l2=3.31216e-05 x=-4.71784e-05 y=-0.000497202 z=-1.65601e-05 kx=0.000603792 ky=-0.00102017 kz=22.9235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05885e-09 l2=2.10344e-05 x=-4.88818e-05 y=0.000187329 z=-1.05164e-05 kx=0.000640508 ky=0.000278191 kz=22.9372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09709e-09 l2=1.18713e-05 x=4.96466e-05 y=0.000155324 z=-5.93533e-06 kx=-0.00040314 ky=-0.000166109 kz=22.8377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55156e-09 l2=1.37245e-05 x=4.95266e-05 y=-0.000156525 z=-6.8654e-06 kx=0.00109889 ky=-0.00044299 kz=23.0787 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23288e-09 l2=5.01456e-06 x=-4.99371e-05 y=-0.000455696 z=-2.50849e-06 kx=-4.07619e-05 ky=-0.000869012 kz=23.1387 Single_crystal: Mo.lau structure a=3.147 b=3.147 c=3.147 aa=90 bb=90 cc=90 V0=31.1667 Single_crystal: sample: Read 1480 reflections from file 'Mo.lau' Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51774e-09 l2=1.15965e-05 x=4.96625e-05 y=0.000382133 z=-5.80147e-06 kx=0.00113005 ky=0.000815685 kz=22.797 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.81872e-09 l2=9.49508e-06 x=-4.97742e-05 y=0.000170637 z=-4.74937e-06 kx=-0.000190576 ky=-4.79489e-05 kz=22.72 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00846e-09 l2=2.14041e-05 x=-4.88408e-05 y=0.000215202 z=-1.07051e-05 kx=-0.00118454 ky=0.00142028 kz=23.1541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05266e-09 l2=1.93055e-05 x=-4.90591e-05 y=-0.000499733 z=-9.65507e-06 kx=-0.000859883 ky=-0.00151501 kz=23.2296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09147e-09 l2=2.49406e-05 x=4.84202e-05 y=-0.000340812 z=-1.24703e-05 kx=-0.00025815 ky=-0.000596194 kz=22.8671 atomic_weight 95.94 Single_crystal: Rebinning material data (Mo.txt) for faster tracing... WARNING: (Table_Rebin): Rebinning table from Mo.txt would exceed 1M rows. Skipping. Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48065e-09 l2=2.35011e-05 x=-4.86002e-05 y=0.000493479 z=-1.17495e-05 kx=0.000840932 ky=0.00148653 kz=22.5207 Single_crystal: sample: Vc=31.1667 [Angs] sigma_abs= (mu/rho)*4.96 [barn] sigma_inc=0.08 [barn] reflections=Mo.lau Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18481e-09 l2=1.36843e-05 x=-4.95299e-05 y=-0.000464 z=-6.84135e-06 kx=0.000651703 ky=-0.00138946 kz=22.8192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47935e-09 l2=1.05634e-05 x=-4.97201e-05 y=0.000467727 z=-5.28453e-06 kx=-0.00095134 ky=0.000132941 kz=22.5144 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04246e-09 l2=1.36583e-05 x=-4.95315e-05 y=0.000434306 z=-6.82989e-06 kx=-8.84114e-05 ky=0.000516792 kz=22.9616 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01598e-09 l2=2.18275e-05 x=-4.87941e-05 y=-3.66007e-05 z=-1.09158e-05 kx=-0.000706138 ky=0.000699974 kz=23.2276 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19443e-09 l2=2.14329e-05 x=-4.88386e-05 y=0.000364122 z=-1.07152e-05 kx=0.000865883 ky=0.00168599 kz=23.0502 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22373e-09 l2=2.40317e-05 x=-4.85351e-05 y=0.000321168 z=-1.20158e-05 kx=0.000343819 ky=9.61118e-05 kz=23.1656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43479e-09 l2=3.74403e-06 x=-4.9965e-05 y=0.00012195 z=-1.8714e-06 kx=0.000616102 ky=0.00141157 kz=23.0457 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24056e-09 l2=1.04643e-05 x=4.97255e-05 y=-0.000246032 z=-5.23452e-06 kx=0.000572721 ky=-0.000990008 kz=22.9063 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37849e-09 l2=4.46142e-06 x=4.99503e-05 y=0.000171972 z=-2.23025e-06 kx=-0.00051863 ky=0.000805122 kz=22.4531 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2496e-09 l2=1.46039e-05 x=4.94642e-05 y=0.000188936 z=-7.30148e-06 kx=-0.000505943 ky=-0.000712622 kz=23.212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58174e-09 l2=2.40115e-05 x=-4.85376e-05 y=-0.00041138 z=-1.20057e-05 kx=0.000405242 ky=-0.000508901 kz=23.2944 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12325e-08 l2=4.12265e-06 x=-4.99578e-05 y=3.93709e-05 z=-2.06512e-06 kx=0.000833035 ky=-0.000171187 kz=22.8285 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44505e-09 l2=1.37522e-05 x=-4.95253e-05 y=8.55401e-05 z=-6.87471e-06 kx=0.000950336 ky=-0.0001006 kz=22.4507 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.01662e-09 l2=7.46899e-06 x=4.98606e-05 y=-0.000256676 z=-3.73447e-06 kx=-0.00094255 ky=-0.00104214 kz=23.1573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16011e-09 l2=1.77715e-05 x=4.92041e-05 y=0.000202019 z=-8.88716e-06 kx=0.00039445 ky=-0.000330938 kz=23.1412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02202e-09 l2=3.15199e-05 x=-4.7452e-05 y=7.9543e-05 z=-1.57589e-05 kx=0.00072322 ky=-0.000611997 kz=22.4056 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62907e-09 l2=1.65113e-05 x=-4.93142e-05 y=-0.000397088 z=-8.25471e-06 kx=0.00080343 ky=-0.000780206 kz=22.9041 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13488e-09 l2=2.71782e-05 x=4.81181e-05 y=-1.11798e-05 z=-1.35896e-05 kx=-1.83303e-05 ky=-0.000199482 kz=22.64 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23409e-09 l2=1.42631e-05 x=4.94886e-05 y=0.00012705 z=-7.134e-06 kx=0.000844266 ky=-9.754e-05 kz=22.6732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24831e-09 l2=2.6651e-05 x=-4.81917e-05 y=-0.000487882 z=-1.33266e-05 kx=-0.000212092 ky=-0.000207462 kz=22.7354 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04104e-09 l2=1.44385e-05 x=-4.94763e-05 y=-5.81422e-05 z=-7.21911e-06 kx=0.000308147 ky=-0.00122629 kz=22.7812 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60053e-09 l2=3.01932e-05 x=4.7666e-05 y=7.60363e-05 z=-1.50997e-05 kx=0.00110636 ky=-5.04676e-05 kz=23.2094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0542e-09 l2=2.50119e-05 x=-4.84108e-05 y=0.000240234 z=-1.25068e-05 kx=-0.00016095 ky=-0.000385895 kz=22.4794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6577e-09 l2=4.5942e-06 x=-4.99472e-05 y=0.000223674 z=-2.29815e-06 kx=-9.9163e-05 ky=0.000128636 kz=22.4262 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.54947e-09 l2=5.91829e-06 x=-4.99124e-05 y=0.000159913 z=-2.96441e-06 kx=-0.00113775 ky=0.00111497 kz=22.8037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37145e-09 l2=3.17607e-05 x=4.74119e-05 y=-0.000325876 z=-1.58795e-05 kx=-0.000763645 ky=-0.000381106 kz=23.259 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63033e-09 l2=2.90401e-05 x=4.78452e-05 y=-0.000347751 z=-1.45218e-05 kx=0.000460018 ky=-0.00104709 kz=22.8326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29056e-09 l2=1.28958e-05 x=-4.95823e-05 y=-2.57969e-05 z=-6.45059e-06 kx=-0.000923364 ky=0.000686853 kz=22.4286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42427e-09 l2=1.69337e-05 x=4.92781e-05 y=-0.00020947 z=-8.46688e-06 kx=-0.000333171 ky=-0.00161817 kz=23.2982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10046e-09 l2=3.28726e-05 x=-4.72221e-05 y=-0.000407568 z=-1.6435e-05 kx=0.000881305 ky=-0.00100186 kz=22.4046 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.43943e-09 l2=3.15569e-06 x=4.99752e-05 y=-3.94425e-05 z=-1.58267e-06 kx=0.000275574 ky=0.00094099 kz=22.9382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13194e-09 l2=2.13708e-05 x=4.88448e-05 y=0.000468479 z=-1.0687e-05 kx=0.000510217 ky=0.000802141 kz=23.2326 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35927e-09 l2=8.90255e-06 x=4.98017e-05 y=0.000416776 z=-4.4512e-06 kx=-0.000587417 ky=0.00193443 kz=23.2513 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44597e-09 l2=2.4113e-05 x=4.85246e-05 y=0.00035106 z=-1.20582e-05 kx=0.000442202 ky=0.00148928 kz=22.3784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02629e-09 l2=1.36388e-05 x=4.95326e-05 y=-0.000279979 z=-6.82135e-06 kx=0.000663607 ky=-0.000249623 kz=23.1605 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.27875e-09 l2=1.1807e-05 x=4.96505e-05 y=0.000181096 z=-5.90462e-06 kx=-0.000245499 ky=0.000879239 kz=23.2109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3151e-09 l2=1.65817e-05 x=4.9308e-05 y=5.21614e-05 z=-8.29121e-06 kx=-0.000137494 ky=3.35312e-05 kz=23.3099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29265e-09 l2=2.17053e-05 x=-4.88083e-05 y=0.00032407 z=-1.08524e-05 kx=0.000442463 ky=0.000706352 kz=23.1429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5901e-09 l2=6.08187e-06 x=4.99077e-05 y=-0.000171647 z=-3.04082e-06 kx=-0.000879375 ky=0.000131414 kz=23.015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2266e-09 l2=1.92955e-05 x=4.90608e-05 y=-0.000131423 z=-9.64672e-06 kx=-0.0007546 ky=-0.000749765 kz=22.4581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03682e-09 l2=3.10176e-05 x=-4.75336e-05 y=-4.77721e-06 z=-1.55111e-05 kx=-0.000822397 ky=-0.000755341 kz=22.4115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.87555e-09 l2=3.77023e-06 x=4.99647e-05 y=-0.000103035 z=-1.88762e-06 kx=-0.000642803 ky=-0.00011679 kz=22.4414 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17312e-09 l2=6.06194e-06 x=-4.9908e-05 y=-3.09639e-05 z=-3.0331e-06 kx=-0.000692519 ky=0.00095585 kz=22.3863 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13506e-09 l2=1.84472e-05 x=4.91415e-05 y=0.000461689 z=-9.22684e-06 kx=0.00126068 ky=0.000857282 kz=23.2787 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10551e-09 l2=7.04723e-06 x=4.98756e-05 y=0.000132627 z=-3.52656e-06 kx=0.00108432 ky=0.00105538 kz=22.6279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58518e-09 l2=1.06138e-05 x=4.97176e-05 y=0.000406602 z=-5.30781e-06 kx=4.86186e-05 ky=0.00036492 kz=22.6935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14171e-09 l2=1.27654e-05 x=4.95912e-05 y=0.000391861 z=-6.38255e-06 kx=-0.000569765 ky=0.000441232 kz=22.9108 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.48842e-09 l2=7.61578e-06 x=4.98549e-05 y=-0.000452644 z=-3.8101e-06 kx=0.000210278 ky=-0.000486022 kz=22.3792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02903e-09 l2=1.77355e-05 x=-4.9207e-05 y=-0.000103511 z=-8.87047e-06 kx=-0.00103092 ky=-0.00114011 kz=22.9074 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0763e-09 l2=8.0759e-06 x=4.98368e-05 y=-0.000372845 z=-4.0386e-06 kx=-0.000174375 ky=-0.000865279 kz=22.7164 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18944e-09 l2=1.78264e-05 x=4.91997e-05 y=-0.000201198 z=-8.91247e-06 kx=-0.000836397 ky=0.000214804 kz=22.8653 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13662e-09 l2=9.40908e-06 x=-4.97783e-05 y=0.000474774 z=-4.70476e-06 kx=0.000159787 ky=0.00101798 kz=22.5996 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35723e-09 l2=1.60395e-05 x=4.93524e-05 y=0.000216539 z=-8.02268e-06 kx=0.0010178 ky=0.000468129 kz=22.5582 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.16355e-09 l2=9.73709e-06 x=-4.97627e-05 y=0.000151086 z=-4.86858e-06 kx=0.000701233 ky=0.000156998 kz=22.6138 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.90227e-09 l2=4.66803e-06 x=4.84206e-05 y=-0.000238427 z=-1.24686e-05 kx=4.55622 ky=-1.5037 kz=21.8692 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0654e-09 l2=3.21989e-05 x=4.73372e-05 y=0.000270868 z=-1.61004e-05 kx=0.000193327 ky=0.00108329 kz=23.1764 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.64783e-09 l2=6.75936e-06 x=-4.98857e-05 y=-0.000118643 z=-3.3812e-06 kx=-9.00603e-05 ky=-7.89914e-05 kz=22.7201 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.71252e-09 l2=5.99501e-06 x=4.99102e-05 y=-0.000184041 z=-2.99942e-06 kx=2.53704e-05 ky=-0.000774317 kz=22.4651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16292e-09 l2=2.07732e-05 x=-4.89091e-05 y=-0.000390406 z=-1.03885e-05 kx=-0.000633944 ky=-0.000366756 kz=22.5493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35157e-09 l2=8.11765e-06 x=4.9835e-05 y=0.00028781 z=-4.05948e-06 kx=-9.43811e-06 ky=9.28475e-06 kz=22.8638 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30453e-09 l2=7.58266e-06 x=4.98562e-05 y=4.89442e-06 z=-3.79034e-06 kx=-0.000757028 ky=0.000413614 kz=22.9622 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23735e-09 l2=1.98234e-05 x=-4.90074e-05 y=-0.000285144 z=-9.91465e-06 kx=-0.00108173 ky=-0.00165116 kz=23.0087 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14657e-09 l2=1.78836e-05 x=-4.91939e-05 y=-0.000477386 z=-8.94312e-06 kx=-0.000355096 ky=-0.00085225 kz=22.8194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05649e-09 l2=1.79325e-05 x=-4.91896e-05 y=-4.10141e-05 z=-8.96646e-06 kx=0.000154859 ky=0.000406982 kz=22.9019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74169e-09 l2=1.78906e-05 x=4.91938e-05 y=0.000127176 z=-8.94433e-06 kx=-0.00084463 ky=-9.2664e-05 kz=22.7139 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26976e-09 l2=1.49539e-05 x=4.9438e-05 y=3.79702e-05 z=-7.4771e-06 kx=-0.000213824 ky=0.000510744 kz=22.3217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18226e-09 l2=5.76042e-06 x=-4.9917e-05 y=2.16496e-05 z=-2.88154e-06 kx=-0.000330189 ky=0.000690072 kz=22.4721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39726e-09 l2=1.95158e-05 x=4.90386e-05 y=0.000307152 z=-9.75927e-06 kx=0.000316562 ky=0.000744229 kz=22.4576 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17086e-09 l2=1.04094e-05 x=4.97283e-05 y=-2.22622e-05 z=-5.20682e-06 kx=0.000694088 ky=-0.000136732 kz=22.5106 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39885e-08 l2=2.11062e-07 x=4.99999e-05 y=-0.000370465 z=-1.17923e-07 kx=0.000182695 ky=-0.00101759 kz=22.9516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02858e-09 l2=2.76666e-05 x=-4.80489e-05 y=0.000354629 z=-1.38321e-05 kx=0.000806192 ky=0.000296604 kz=23.0982 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07154e-09 l2=1.26398e-05 x=4.95991e-05 y=0.00037063 z=-6.32e-06 kx=-0.00020852 ky=0.00162751 kz=22.5423 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05341e-09 l2=1.03835e-05 x=-4.97297e-05 y=-2.2059e-05 z=-5.19325e-06 kx=-0.000452947 ky=0.000176608 kz=23.198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2931e-09 l2=6.58487e-06 x=-4.98916e-05 y=8.09709e-05 z=-3.29239e-06 kx=0.000319531 ky=-0.000737217 kz=23.0518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18463e-09 l2=3.54871e-05 x=-4.67467e-05 y=-0.00021144 z=-1.77423e-05 kx=0.000944991 ky=-0.00135858 kz=23.2272 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1025e-09 l2=3.57112e-05 x=4.67034e-05 y=0.000461999 z=-1.78558e-05 kx=-0.000168554 ky=0.00202397 kz=23.0612 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81761e-09 l2=1.24185e-05 x=-4.96132e-05 y=0.000262 z=-6.20943e-06 kx=0.000334007 ky=0.000530318 kz=23.2044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68531e-09 l2=1.07497e-05 x=-4.97105e-05 y=-0.000184634 z=-5.37467e-06 kx=0.000491833 ky=-0.000416001 kz=23.2988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25829e-09 l2=1.06824e-05 x=-4.9714e-05 y=0.000244481 z=-5.3416e-06 kx=0.000110463 ky=0.00145114 kz=23.2774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41957e-09 l2=1.54804e-05 x=4.9397e-05 y=2.34311e-05 z=-7.74354e-06 kx=0.0012001 ky=-0.000371236 kz=22.3586 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19519e-09 l2=2.64589e-05 x=-4.82179e-05 y=-0.000209226 z=-1.32313e-05 kx=-0.00060646 ky=-0.00132059 kz=22.9231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02861e-09 l2=3.02322e-05 x=-4.76609e-05 y=0.000302946 z=-1.51152e-05 kx=0.000667146 ky=0.000404117 kz=22.9709 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.37495e-09 l2=8.87484e-06 x=4.9803e-05 y=-0.000453691 z=-4.43709e-06 kx=-0.000920942 ky=-0.000619986 kz=22.7116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.21502e-09 l2=6.22905e-06 x=-4.9903e-05 y=-0.000149348 z=-3.11569e-06 kx=-2.5512e-05 ky=-0.000453934 kz=22.6757 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7193e-09 l2=3.56652e-06 x=4.99682e-05 y=-0.000442721 z=-1.78517e-06 kx=0.000479976 ky=-0.000458553 kz=22.929 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28195e-09 l2=2.19359e-05 x=-4.87824e-05 y=-0.000377502 z=-1.09684e-05 kx=9.689e-05 ky=-0.000845921 kz=23.2223 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.92216e-09 l2=9.3815e-06 x=4.97798e-05 y=4.45981e-05 z=-4.69355e-06 kx=-7.63352e-05 ky=-0.000867835 kz=22.7418 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27748e-09 l2=1.90937e-05 x=4.90805e-05 y=-0.000487298 z=-9.54606e-06 kx=-0.0006718 ky=-0.000375143 kz=22.9019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09498e-09 l2=2.40696e-05 x=4.85301e-05 y=0.000495252 z=-1.20355e-05 kx=5.79585e-05 ky=0.00107289 kz=22.4157 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.8905e-09 l2=4.80563e-06 x=4.99423e-05 y=-0.000488766 z=-2.40614e-06 kx=0.00061706 ky=-0.000217716 kz=22.3214 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49287e-09 l2=8.36005e-06 x=4.98249e-05 y=0.000359926 z=-4.1824e-06 kx=0.000757975 ky=0.0011062 kz=23.1641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77693e-09 l2=7.00608e-06 x=-4.98772e-05 y=0.000257383 z=-3.5034e-06 kx=0.000235739 ky=-0.000303086 kz=22.4572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11069e-09 l2=1.25657e-05 x=4.96041e-05 y=-0.000487334 z=-6.28201e-06 kx=-0.000887591 ky=-0.0021427 kz=23.1081 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.53028e-09 l2=3.84441e-06 x=4.9963e-05 y=8.88634e-05 z=-1.9263e-06 kx=0.00105043 ky=0.000769656 kz=22.5194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54461e-09 l2=1.60641e-05 x=-4.93506e-05 y=-5.15289e-06 z=-8.03361e-06 kx=-0.000365921 ky=0.000129371 kz=22.5185 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52384e-09 l2=1.17416e-05 x=4.96541e-05 y=0.000482051 z=-5.87272e-06 kx=0.000539506 ky=0.000421228 kz=23.0205 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3139e-09 l2=9.22536e-06 x=4.9787e-05 y=-5.41268e-05 z=-4.61281e-06 kx=-0.000477499 ky=-0.00106389 kz=23.1871 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54034e-09 l2=1.53808e-05 x=4.94048e-05 y=0.000331034 z=-7.69362e-06 kx=0.00111071 ky=0.000322862 kz=22.5795 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12523e-09 l2=2.45587e-05 x=-4.84684e-05 y=0.000430308 z=-1.22818e-05 kx=-0.000895628 ky=0.00104574 kz=23.0705 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22934e-09 l2=1.05243e-05 x=4.97222e-05 y=-0.000442059 z=-5.26481e-06 kx=0.000942539 ky=-0.000197386 kz=22.7145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6502e-09 l2=1.92705e-05 x=-4.90626e-05 y=-0.000128192 z=-9.63799e-06 kx=-0.000878204 ky=0.000242226 kz=22.5024 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25268e-09 l2=1.2396e-05 x=4.96146e-05 y=-0.000499153 z=-6.19695e-06 kx=-0.000761353 ky=-0.000448764 kz=22.6702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82685e-09 l2=1.1412e-05 x=-4.96736e-05 y=0.000364664 z=-5.70599e-06 kx=0.000422044 ky=0.00188871 kz=22.5342 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00102e-09 l2=1.44347e-05 x=4.94765e-05 y=-0.000138455 z=-7.2171e-06 kx=-0.000361372 ky=-9.81174e-05 kz=23.1127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98038e-09 l2=8.17928e-06 x=-4.98327e-05 y=-0.000497136 z=-4.08934e-06 kx=0.000824838 ky=-0.00035382 kz=22.8683 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05202e-09 l2=6.18891e-06 x=-4.99043e-05 y=0.000142308 z=-3.09424e-06 kx=0.000579123 ky=0.00106571 kz=23.2845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12598e-09 l2=1.63457e-05 x=4.93276e-05 y=-0.000407501 z=-8.17334e-06 kx=-3.36222e-05 ky=0.00010123 kz=22.793 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81033e-09 l2=8.27187e-06 x=4.98289e-05 y=-0.000464406 z=-4.13524e-06 kx=-0.000748374 ky=-0.00138487 kz=23.2643 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51367e-09 l2=1.77372e-05 x=4.92073e-05 y=-0.000399581 z=-8.86955e-06 kx=9.91829e-05 ky=-0.00173941 kz=23.2373 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80878e-09 l2=9.21879e-06 x=4.9787e-05 y=-1.38584e-05 z=-4.61175e-06 kx=0.000672562 ky=-0.00023093 kz=23.0792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39256e-09 l2=2.07183e-05 x=-4.89154e-05 y=-0.000351685 z=-1.03594e-05 kx=0.000235163 ky=0.0001197 kz=22.9849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91323e-09 l2=4.78146e-06 x=4.99429e-05 y=0.000485802 z=-2.3903e-06 kx=-0.000636051 ky=0.00167769 kz=22.8645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.04251e-09 l2=1.13689e-05 x=-4.96757e-05 y=3.42665e-05 z=-5.68795e-06 kx=-0.00115512 ky=0.00018797 kz=23.2135 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02776e-09 l2=9.90705e-06 x=4.9754e-05 y=0.000141509 z=-4.95566e-06 kx=0.000518352 ky=0.00119836 kz=23.0082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.46243e-09 l2=6.09031e-06 x=4.99071e-05 y=0.000326676 z=-3.04889e-06 kx=0.00114848 ky=0.00176294 kz=22.902 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63188e-09 l2=2.72036e-05 x=-4.81148e-05 y=0.000299999 z=-1.36019e-05 kx=0.000318128 ky=-0.000201732 kz=23.1434 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36415e-09 l2=1.29759e-05 x=-4.95775e-05 y=0.000436445 z=-6.48745e-06 kx=0.000538694 ky=0.00149809 kz=22.7998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23314e-09 l2=2.7274e-05 x=-4.81041e-05 y=2.12404e-05 z=-1.36394e-05 kx=-0.000826293 ky=0.000631257 kz=22.3118 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02696e-09 l2=3.01784e-05 x=4.76695e-05 y=-0.000373616 z=-1.50882e-05 kx=-0.00074337 ky=-0.000704482 kz=23.0209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33338e-09 l2=1.66797e-05 x=4.92994e-05 y=-0.000395698 z=-8.34234e-06 kx=0.00083656 ky=-0.00135863 kz=22.8524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03807e-09 l2=2.55894e-05 x=4.83353e-05 y=0.000370421 z=-1.27954e-05 kx=7.60263e-05 ky=0.000259125 kz=22.9922 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86883e-09 l2=1.00684e-05 x=4.97458e-05 y=-0.000120949 z=-5.03738e-06 kx=0.00104722 ky=-0.00139633 kz=22.9922 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93455e-09 l2=1.56612e-05 x=-4.93828e-05 y=0.000314136 z=-7.83371e-06 kx=-0.000987613 ky=0.000798756 kz=22.6013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0614e-09 l2=9.20744e-06 x=-4.97875e-05 y=0.000351181 z=-4.6063e-06 kx=-0.000934079 ky=0.00086871 kz=22.6444 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76836e-09 l2=2.00752e-05 x=4.89825e-05 y=-0.000206995 z=-1.00373e-05 kx=-0.000579475 ky=-0.00138037 kz=23.1773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12955e-09 l2=2.15964e-05 x=4.88203e-05 y=-0.000138398 z=-1.07983e-05 kx=-0.000214911 ky=0.000549779 kz=23.2209 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55028e-09 l2=1.96131e-05 x=-4.90289e-05 y=-0.000434411 z=-9.80799e-06 kx=-0.000306996 ky=-0.0003344 kz=22.3189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72808e-09 l2=7.63567e-06 x=-4.98542e-05 y=4.1925e-06 z=-3.81726e-06 kx=0.000660056 ky=-0.000597709 kz=22.8452 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71566e-09 l2=1.88619e-05 x=4.91028e-05 y=0.000349247 z=-9.43129e-06 kx=-0.000251169 ky=-1.22991e-05 kz=23.1333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19023e-09 l2=1.50326e-05 x=-4.94319e-05 y=-0.000354628 z=-7.51668e-06 kx=9.75119e-05 ky=-0.00135627 kz=22.3177 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44112e-09 l2=1.91572e-05 x=4.90745e-05 y=0.000143711 z=-9.57735e-06 kx=-0.000900004 ky=-0.000544416 kz=22.6287 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08966e-09 l2=1.21872e-05 x=4.96274e-05 y=0.000225813 z=-6.09376e-06 kx=-0.000181869 ky=0.000439026 kz=23.1944 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4937e-09 l2=1.99631e-05 x=-4.89938e-05 y=-0.000156156 z=-9.98182e-06 kx=0.000215781 ky=-0.00111697 kz=23.2231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11522e-09 l2=2.76543e-05 x=4.80498e-05 y=8.56927e-05 z=-1.38291e-05 kx=0.000664432 ky=0.00017051 kz=22.6946 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1567e-09 l2=2.16248e-05 x=4.88173e-05 y=-0.000175448 z=-1.08116e-05 kx=-0.00062425 ky=-0.000430227 kz=22.5371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.17376e-09 l2=3.28449e-06 x=-4.99731e-05 y=-0.000293476 z=-1.64778e-06 kx=-0.000668776 ky=-0.000100131 kz=23.1129 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37439e-09 l2=1.25699e-05 x=-4.96033e-05 y=0.000200999 z=-6.28745e-06 kx=-0.000855724 ky=0.000890599 kz=23.1178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.10702e-09 l2=5.63259e-06 x=4.99208e-05 y=-0.000348409 z=-2.817e-06 kx=-0.000391831 ky=-0.00188705 kz=22.9541 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58465e-09 l2=2.15406e-05 x=4.88269e-05 y=-7.79915e-05 z=-1.0769e-05 kx=-0.000989995 ky=0.000670001 kz=22.8194 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.65311e-09 l2=1.16981e-05 x=4.96568e-05 y=0.000155075 z=-5.85133e-06 kx=0.000438272 ky=0.000330554 kz=22.7235 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60229e-09 l2=2.14895e-05 x=-4.88321e-05 y=0.000494072 z=-1.07451e-05 kx=0.000232762 ky=0.000711609 kz=23.0642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.99593e-09 l2=1.42615e-05 x=-4.94891e-05 y=-0.000132188 z=-7.13171e-06 kx=1.55109e-05 ky=-0.00125865 kz=22.567 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.52941e-09 l2=8.46025e-06 x=4.98209e-05 y=7.95381e-05 z=-4.23088e-06 kx=-0.000233272 ky=0.0011131 kz=22.8426 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27583e-09 l2=1.29952e-05 x=-4.95759e-05 y=-0.000232303 z=-6.50012e-06 kx=-0.00086617 ky=-0.000458612 kz=22.9657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63652e-09 l2=2.00108e-05 x=4.89888e-05 y=0.000402315 z=-1.00067e-05 kx=0.000229875 ky=0.00125318 kz=22.697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45113e-09 l2=1.22406e-05 x=-4.96241e-05 y=-0.00046089 z=-6.12131e-06 kx=-0.000127361 ky=-0.00128046 kz=22.7366 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33996e-09 l2=2.46254e-05 x=4.84604e-05 y=-0.00036501 z=-1.23135e-05 kx=6.13051e-05 ky=-0.0013133 kz=22.8225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7023e-09 l2=1.97575e-05 x=4.90144e-05 y=0.000258305 z=-9.8805e-06 kx=0.000423046 ky=0.000914695 kz=22.4763 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93763e-09 l2=6.77536e-06 x=4.98852e-05 y=-0.000353453 z=-3.38784e-06 kx=-0.000374127 ky=-0.0017877 kz=23.0843 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01108e-09 l2=2.75206e-05 x=-4.80688e-05 y=0.000222842 z=-1.37631e-05 kx=-0.00103982 ky=0.000440363 kz=22.439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03059e-09 l2=2.37187e-05 x=4.8573e-05 y=0.000168494 z=-1.1861e-05 kx=0.000546292 ky=0.000394232 kz=22.9184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37869e-09 l2=3.1281e-05 x=-4.74903e-05 y=-0.000269241 z=-1.56433e-05 kx=-0.00104684 ky=-0.00177392 kz=23.2948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34682e-09 l2=1.18092e-05 x=-4.96504e-05 y=-0.000289664 z=-5.90386e-06 kx=0.000632749 ky=0.000361655 kz=22.5956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.4672e-09 l2=5.46249e-06 x=4.99253e-05 y=4.99368e-05 z=-2.73486e-06 kx=0.000845837 ky=0.00105073 kz=22.4199 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21565e-09 l2=2.60241e-05 x=-4.82772e-05 y=0.000481198 z=-1.30132e-05 kx=-0.000276186 ky=0.000225516 kz=22.6336 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.61364e-09 l2=7.18382e-06 x=-4.98711e-05 y=-0.000460127 z=-3.59114e-06 kx=0.000945302 ky=-0.00117162 kz=22.6455 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.18075e-09 l2=7.01097e-06 x=-4.98771e-05 y=-9.69291e-05 z=-3.5064e-06 kx=0.000307105 ky=0.00058601 kz=22.7642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53648e-09 l2=7.46692e-06 x=4.98603e-05 y=-0.000391832 z=-3.7365e-06 kx=0.00103477 ky=-0.00024726 kz=22.6475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14857e-09 l2=2.83395e-05 x=4.79502e-05 y=-0.000448001 z=-1.41709e-05 kx=0.000271265 ky=-0.000274713 kz=22.6715 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.25955e-09 l2=4.42719e-06 x=-4.99512e-05 y=0.000387355 z=-2.21451e-06 kx=0.000793587 ky=0.00130242 kz=23.1572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.60987e-09 l2=1.25675e-05 x=4.96035e-05 y=-0.000356538 z=-6.28667e-06 kx=0.00074334 ky=-0.000376621 kz=22.4817 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16595e-09 l2=9.12279e-06 x=4.97916e-05 y=0.000261691 z=-4.56133e-06 kx=-0.000299909 ky=0.00164944 kz=23.0977 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1339e-09 l2=1.68161e-05 x=-4.92879e-05 y=0.000366231 z=-8.40974e-06 kx=-0.00051729 ky=0.00131797 kz=22.4393 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.313e-09 l2=2.70446e-05 x=4.81375e-05 y=0.000198198 z=-1.35209e-05 kx=-0.000990168 ky=0.000169146 kz=23.1658 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11611e-09 l2=5.3582e-06 x=-4.99283e-05 y=-0.000427795 z=-2.67865e-06 kx=0.000678331 ky=-0.000934 kz=22.482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60805e-09 l2=1.21374e-05 x=4.96302e-05 y=-0.000190939 z=-6.07164e-06 kx=0.0009926 ky=-0.000648408 kz=23.1609 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30679e-09 l2=2.70379e-05 x=4.81377e-05 y=0.000164123 z=-1.35203e-05 kx=0.000354154 ky=0.000876057 kz=23.2966 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42526e-09 l2=8.05124e-06 x=4.98377e-05 y=-8.07905e-05 z=-4.02706e-06 kx=0.000332519 ky=0.000745295 kz=22.7681 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03064e-09 l2=1.3204e-05 x=4.95624e-05 y=-0.000191511 z=-6.60305e-06 kx=1.67951e-05 ky=0.000198539 kz=23.3066 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36099e-08 l2=1.16527e-06 x=4.99967e-05 y=0.000318059 z=-5.89419e-07 kx=-1.00665e-05 ky=0.000222011 kz=22.881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23661e-09 l2=3.05568e-05 x=4.76083e-05 y=-0.000293807 z=-1.52803e-05 kx=0.000640146 ky=8.56953e-05 kz=23.0475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30674e-08 l2=1.40453e-06 x=4.99952e-05 y=0.000249866 z=-7.13958e-07 kx=7.12964e-05 ky=0.0010345 kz=22.6735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05997e-09 l2=1.1281e-05 x=-4.96809e-05 y=-0.000178706 z=-5.64104e-06 kx=-1.14101e-05 ky=-0.00124023 kz=22.9773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75865e-09 l2=1.28382e-05 x=-4.95865e-05 y=-0.000151767 z=-6.41877e-06 kx=0.000555886 ky=-0.00105341 kz=23.0552 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.02897e-09 l2=1.80204e-05 x=-4.9182e-05 y=0.000448509 z=-9.00913e-06 kx=0.000985481 ky=0.00167905 kz=23.1421 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02974e-09 l2=3.01761e-05 x=4.76687e-05 y=-0.000281079 z=-1.50906e-05 kx=0.00095394 ky=-0.000418787 kz=23.1437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.55155e-09 l2=9.65993e-06 x=-4.97662e-05 y=-0.000292724 z=-4.83343e-06 kx=-0.000786133 ky=-0.00020437 kz=23.1866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12577e-09 l2=3.77516e-05 x=-4.62996e-05 y=-0.000353176 z=-1.88784e-05 kx=-0.000996826 ky=-0.00153234 kz=23.0137 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0297e-09 l2=1.38313e-05 x=-4.95195e-05 y=0.00036313 z=-6.91588e-06 kx=0.000123987 ky=0.00192111 kz=22.6309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23935e-09 l2=8.42895e-06 x=4.98221e-05 y=-6.16337e-05 z=-4.21687e-06 kx=0.00059375 ky=0.000342297 kz=23.2121 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08371e-09 l2=1.2362e-05 x=4.96167e-05 y=8.33991e-05 z=-6.18049e-06 kx=-0.000471443 ky=-0.000496625 kz=22.4844 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0286e-09 l2=1.88095e-05 x=4.91072e-05 y=-0.000279342 z=-9.40762e-06 kx=0.00107551 ky=-0.0015579 kz=22.3591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01935e-08 l2=2.173e-06 x=-4.99883e-05 y=0.000281683 z=-1.09301e-06 kx=-0.00064397 ky=-0.000302769 kz=22.782 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02296e-09 l2=3.20971e-05 x=4.73544e-05 y=-0.000458483 z=-1.60497e-05 kx=0.000295292 ky=-0.000839024 kz=22.9016 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4209e-09 l2=1.90669e-06 x=-4.99909e-05 y=-0.000384797 z=-9.538e-07 kx=0.000114967 ky=-0.000568525 kz=22.6184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81669e-09 l2=1.06586e-05 x=-4.97153e-05 y=0.000271709 z=-5.33039e-06 kx=-8.05321e-05 ky=0.00149035 kz=22.9407 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00584e-09 l2=2.59334e-05 x=-4.82894e-05 y=-0.00046828 z=-1.29677e-05 kx=-0.000229512 ky=-0.000433497 kz=22.6901 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47914e-09 l2=1.4705e-05 x=4.94565e-05 y=-0.000147434 z=-7.35446e-06 kx=0.000317802 ky=-0.000634257 kz=22.5965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95486e-09 l2=1.21025e-05 x=4.96324e-05 y=0.000297213 z=-6.0541e-06 kx=0.00085159 ky=-0.00045317 kz=22.7693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.66617e-09 l2=4.43509e-06 x=4.99509e-05 y=-0.00027038 z=-2.22015e-06 kx=0.000124314 ky=-0.00133145 kz=23.2147 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26306e-09 l2=1.86043e-05 x=-4.91273e-05 y=0.000333903 z=-9.30202e-06 kx=0.000352772 ky=0.000837814 kz=22.304 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36277e-09 l2=1.91987e-05 x=-4.90699e-05 y=-0.000385507 z=-9.60054e-06 kx=-0.000228754 ky=-0.000864271 kz=22.5641 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27854e-09 l2=9.53326e-06 x=4.97724e-05 y=-0.000203506 z=-4.76625e-06 kx=-0.000462411 ky=-0.000219897 kz=22.7315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24931e-09 l2=3.56791e-06 x=-4.99681e-05 y=-9.22094e-05 z=-1.78568e-06 kx=-0.000497435 ky=0.000151475 kz=22.6726 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37965e-09 l2=7.77327e-06 x=4.98489e-05 y=-2.08485e-05 z=-3.88511e-06 kx=-0.00102055 ky=-0.000239963 kz=23.0244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.58983e-09 l2=7.12954e-06 x=4.98728e-05 y=0.000139088 z=-3.56905e-06 kx=0.000903426 ky=0.00138912 kz=22.7111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08206e-09 l2=2.25108e-05 x=-4.87166e-05 y=0.000134578 z=-1.12567e-05 kx=-0.000383299 ky=0.000590633 kz=23.114 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45932e-09 l2=1.79119e-05 x=4.91914e-05 y=0.000255721 z=-8.95719e-06 kx=0.000244179 ky=0.00144173 kz=22.7511 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66069e-09 l2=8.36494e-06 x=4.98247e-05 y=-0.000170873 z=-4.18513e-06 kx=0.000829393 ky=-0.000707551 kz=22.5865 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.77951e-09 l2=5.9317e-06 x=4.99119e-05 y=-0.00013817 z=-2.96984e-06 kx=0.00117518 ky=-0.000132394 kz=22.5256 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35829e-09 l2=1.3312e-05 x=4.95553e-05 y=-0.000184639 z=-6.65575e-06 kx=-0.000643803 ky=-0.000138997 kz=22.5125 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.0104e-09 l2=1.1574e-05 x=-4.96641e-05 y=0.000282287 z=-5.78757e-06 kx=0.00019303 ky=-0.000355979 kz=23.1943 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.64454e-09 l2=1.20703e-05 x=-4.96347e-05 y=0.000486642 z=-6.03575e-06 kx=0.000326953 ky=0.00119856 kz=23.2792 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.49293e-09 l2=4.87635e-06 x=4.99407e-05 y=0.00034055 z=-2.4393e-06 kx=-0.00051225 ky=-0.00025246 kz=22.8399 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23357e-09 l2=1.68003e-05 x=4.92896e-05 y=0.000387591 z=-8.39953e-06 kx=-0.000582243 ky=0.0016402 kz=23.0089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01303e-09 l2=9.03096e-06 x=4.97958e-05 y=-5.19151e-05 z=-4.515e-06 kx=-0.00044637 ky=-0.000593602 kz=22.4683 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13928e-09 l2=2.47143e-05 x=4.84491e-05 y=-0.000122922 z=-1.23576e-05 kx=-5.53189e-05 ky=0.00052329 kz=22.5776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54719e-09 l2=2.00571e-05 x=-4.89845e-05 y=-0.000268955 z=-1.00272e-05 kx=0.000964283 ky=-0.000478092 kz=22.7053 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45134e-09 l2=1.15244e-05 x=4.96669e-05 y=-0.0001709 z=-5.76301e-06 kx=2.90388e-05 ky=0.0002286 kz=22.6948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.081e-09 l2=2.966e-05 x=-4.77505e-05 y=-0.000133102 z=-1.48298e-05 kx=0.000350838 ky=-0.00135423 kz=23.0595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.16029e-09 l2=7.16812e-06 x=4.98716e-05 y=-7.02934e-05 z=-3.58484e-06 kx=-0.000359467 ky=0.000936742 kz=22.3668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44875e-09 l2=1.75543e-05 x=4.92239e-05 y=0.000473698 z=-8.77711e-06 kx=-0.00036126 ky=0.00104155 kz=23.086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00873e-09 l2=3.90068e-05 x=4.60392e-05 y=0.000498996 z=-1.95046e-05 kx=0.000346299 ky=0.000896322 kz=22.8086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08917e-09 l2=2.39468e-05 x=4.85457e-05 y=0.000471852 z=-1.19723e-05 kx=-0.000755739 ky=0.000470194 kz=22.311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.22464e-09 l2=1.03446e-05 x=4.97318e-05 y=-5.40883e-05 z=-5.17492e-06 kx=0.0004691 ky=0.000467577 kz=22.7668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29606e-09 l2=8.62366e-06 x=-4.98137e-05 y=0.000307162 z=-4.31365e-06 kx=-0.000531924 ky=0.000518545 kz=22.5523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10004e-09 l2=9.92942e-06 x=-4.97528e-05 y=-4.87091e-05 z=-4.96663e-06 kx=-0.000630631 ky=0.000975878 kz=22.9521 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10379e-09 l2=1.85408e-05 x=4.91329e-05 y=-7.56326e-05 z=-9.27263e-06 kx=0.000780866 ky=-0.00108793 kz=22.7073 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66333e-09 l2=1.23898e-05 x=-4.96149e-05 y=-0.000402092 z=-6.19523e-06 kx=0.000224811 ky=-0.000702579 kz=23.062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11053e-09 l2=8.80889e-06 x=-4.98058e-05 y=-0.000432514 z=-4.40343e-06 kx=0.000709139 ky=-0.000702423 kz=22.5324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36006e-09 l2=1.76188e-05 x=4.92176e-05 y=0.000141213 z=-8.81214e-06 kx=0.000948819 ky=0.000652593 kz=22.6857 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10658e-09 l2=2.63903e-05 x=4.82278e-05 y=-0.000238132 z=-1.31952e-05 kx=-0.000245953 ky=0.000249437 kz=22.545 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31122e-09 l2=7.47984e-06 x=4.98601e-05 y=0.000390838 z=-3.73906e-06 kx=-0.000682475 ky=0.00086296 kz=22.3895 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.78947e-09 l2=3.15826e-06 x=-4.99752e-05 y=-0.00021987 z=-1.58483e-06 kx=-0.000607778 ky=0.000436944 kz=23.2315 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03977e-09 l2=2.60034e-05 x=-4.82801e-05 y=-0.000378662 z=-1.30022e-05 kx=2.66739e-05 ky=-0.00143031 kz=22.95 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06531e-09 l2=4.17875e-05 x=4.54259e-05 y=0.000265328 z=-2.08933e-05 kx=-0.00052509 ky=0.00142568 kz=23.2723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.47275e-09 l2=1.2827e-05 x=-4.95873e-05 y=-7.14157e-05 z=-6.41372e-06 kx=0.000468595 ky=0.000219568 kz=22.7109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5238e-09 l2=4.88725e-06 x=4.99404e-05 y=-0.000396381 z=-2.44319e-06 kx=-0.0009877 ky=-0.00145993 kz=22.4439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95348e-09 l2=1.12431e-05 x=4.96833e-05 y=-0.000243071 z=-5.62035e-06 kx=-0.00101115 ky=-0.00140418 kz=22.8824 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36554e-09 l2=1.22686e-05 x=4.96221e-05 y=-0.000499359 z=-6.13689e-06 kx=0.000899245 ky=-0.00194285 kz=23.2613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53213e-09 l2=1.97019e-05 x=-4.90204e-05 y=-0.000155768 z=-9.85052e-06 kx=0.000542554 ky=-0.000972199 kz=22.3411 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06073e-09 l2=1.38391e-05 x=4.9519e-05 y=0.000476917 z=-6.92003e-06 kx=-2.00878e-05 ky=0.0022005 kz=22.7086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71771e-09 l2=6.15565e-06 x=-4.99051e-05 y=-4.16123e-05 z=-3.08142e-06 kx=-0.00100808 ky=-0.000457634 kz=22.4539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36942e-09 l2=2.92053e-05 x=4.78204e-05 y=6.89497e-05 z=-1.46031e-05 kx=-0.000109271 ky=0.00121344 kz=23.1538 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75697e-09 l2=1.4377e-05 x=-4.9481e-05 y=0.00031168 z=-7.1874e-06 kx=0.000931241 ky=0.00155016 kz=23.0216 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05398e-09 l2=1.2575e-05 x=-4.9603e-05 y=0.000441094 z=-6.28961e-06 kx=-0.000705149 ky=0.00209399 kz=22.4382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06057e-09 l2=5.84534e-06 x=-4.99146e-05 y=-0.000153977 z=-2.9215e-06 kx=0.000781614 ky=8.57337e-05 kz=22.8836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13348e-09 l2=6.37104e-06 x=4.98983e-05 y=-0.000187874 z=-3.18931e-06 kx=0.00123552 ky=-0.000629766 kz=22.6029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15441e-09 l2=2.3806e-05 x=4.8563e-05 y=8.97043e-05 z=-1.19022e-05 kx=-0.000691279 ky=-4.60596e-05 kz=23.1568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.05906e-09 l2=8.64816e-06 x=4.98127e-05 y=0.000496051 z=-4.32634e-06 kx=0.000336097 ky=0.000860138 kz=22.9375 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.88042e-09 l2=4.89607e-06 x=-4.99402e-05 y=0.000375769 z=-2.44964e-06 kx=0.000606889 ky=0.00129112 kz=22.7682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.95645e-09 l2=1.29327e-05 x=4.958e-05 y=-0.000461423 z=-6.46901e-06 kx=0.000775983 ky=-0.000154503 kz=22.8102 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.18846e-09 l2=6.70457e-06 x=-4.98876e-05 y=-0.000422509 z=-3.35374e-06 kx=6.48581e-05 ky=-0.000546799 kz=22.9884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74568e-09 l2=1.56501e-05 x=-4.93838e-05 y=0.000334508 z=-7.82743e-06 kx=-0.000719975 ky=0.00143038 kz=23.1472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.10539e-09 l2=7.03546e-06 x=4.98763e-05 y=0.00018358 z=-3.51821e-06 kx=-0.000489976 ky=-4.30269e-05 kz=22.7111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03492e-09 l2=1.19363e-05 x=-4.96427e-05 y=-0.000133333 z=-5.96846e-06 kx=0.000316719 ky=-0.0002996 kz=22.8908 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.28908e-09 l2=9.45561e-06 x=4.9776e-05 y=-2.70162e-05 z=-4.73004e-06 kx=0.000507015 ky=0.00016533 kz=23.2469 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14226e-09 l2=1.1566e-05 x=4.96644e-05 y=-0.000266071 z=-5.78536e-06 kx=0.000605748 ky=-0.000555402 kz=22.9841 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09315e-09 l2=9.02893e-06 x=4.97956e-05 y=0.000163632 z=-4.51707e-06 kx=0.000944737 ky=-0.000559277 kz=22.8043 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03338e-09 l2=2.03657e-05 x=-4.89526e-05 y=-0.000406275 z=-1.01813e-05 kx=0.000958722 ky=-0.000109089 kz=23.1905 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19082e-09 l2=2.3917e-05 x=4.85489e-05 y=0.000428211 z=-1.19595e-05 kx=0.000174923 ky=0.000203381 kz=23.2296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35507e-09 l2=1.05327e-05 x=-4.97221e-05 y=-0.000321913 z=-5.26576e-06 kx=0.000588366 ky=0.000332449 kz=23.2836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4101e-09 l2=2.15266e-05 x=4.88283e-05 y=0.000229834 z=-1.07624e-05 kx=-0.000734088 ky=0.000666216 kz=22.495 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.26046e-09 l2=6.54571e-06 x=-4.98927e-05 y=3.88766e-05 z=-3.27647e-06 kx=-0.000909475 ky=1.13981e-05 kz=22.8881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.40451e-09 l2=6.45778e-06 x=4.98958e-05 y=-0.000121008 z=-3.22989e-06 kx=-0.000326252 ky=-0.000729828 kz=23.0635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36177e-09 l2=1.50736e-05 x=-4.94286e-05 y=-0.000328249 z=-7.53852e-06 kx=-0.000460532 ky=-0.00068992 kz=22.3371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83081e-09 l2=1.37179e-05 x=4.95274e-05 y=8.31252e-05 z=-6.86048e-06 kx=0.000282736 ky=-0.000130758 kz=23.2894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.817e-09 l2=1.479e-05 x=4.94504e-05 y=0.000191029 z=-7.39592e-06 kx=-0.000226528 ky=0.00023101 kz=22.6607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.4656e-09 l2=1.78846e-06 x=4.9992e-05 y=0.000128532 z=-8.97738e-07 kx=0.001016 ky=0.000595018 kz=22.3397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18579e-09 l2=9.82576e-06 x=4.97583e-05 y=0.000179487 z=-4.91266e-06 kx=-0.00061316 ky=-0.000171671 kz=23.2695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02541e-09 l2=2.35772e-05 x=4.85906e-05 y=0.000118497 z=-1.1789e-05 kx=-3.39241e-05 ky=0.000440124 kz=22.4543 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58153e-09 l2=2.71904e-05 x=4.81159e-05 y=-0.000101051 z=-1.35978e-05 kx=0.000842615 ky=0.000292936 kz=22.7794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30263e-09 l2=2.2207e-05 x=4.87512e-05 y=0.000273221 z=-1.11064e-05 kx=0.00108309 ky=0.000725315 kz=23.2034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.08151e-09 l2=3.79489e-06 x=-4.99641e-05 y=-0.000293403 z=-1.90037e-06 kx=-0.000171017 ky=-0.000822097 kz=22.3574 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.12409e-09 l2=1.31483e-05 x=-4.95662e-05 y=-0.000172296 z=-6.575e-06 kx=0.000331862 ky=-0.00100605 kz=22.7507 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09043e-09 l2=3.11996e-05 x=-4.75038e-05 y=-0.000248698 z=-1.56021e-05 kx=-0.00086103 ky=-0.00150295 kz=23.3071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06309e-09 l2=2.46221e-05 x=4.8461e-05 y=-0.000299293 z=-1.2311e-05 kx=-0.000249333 ky=8.33572e-05 kz=22.3948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16446e-09 l2=2.08671e-05 x=4.88999e-05 y=-0.000165806 z=-1.0432e-05 kx=-0.00101519 ky=-0.000151707 kz=22.7964 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58431e-09 l2=1.15346e-05 x=4.96665e-05 y=-0.000342337 z=-5.76716e-06 kx=-0.000421194 ky=-0.00184266 kz=22.4516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22004e-09 l2=3.12264e-05 x=-4.75006e-05 y=0.000472776 z=-1.5612e-05 kx=0.000870303 ky=1.28353e-05 kz=22.9116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07436e-09 l2=2.38282e-05 x=-4.85602e-05 y=-3.45594e-05 z=-1.19134e-05 kx=0.000619284 ky=-0.000807442 kz=23.2183 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42363e-09 l2=1.67366e-05 x=-4.9295e-05 y=0.000446554 z=-8.36794e-06 kx=0.000487568 ky=0.00212539 kz=22.7176 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41651e-09 l2=1.57902e-05 x=4.93731e-05 y=-1.54194e-05 z=-7.89401e-06 kx=-0.000823229 ky=-0.000350663 kz=22.8327 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58835e-09 l2=1.87734e-05 x=-4.91115e-05 y=-0.000125623 z=-9.38577e-06 kx=0.0008038 ky=0.000374127 kz=22.8503 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17056e-09 l2=1.53425e-05 x=-4.94084e-05 y=0.000369326 z=-7.67018e-06 kx=0.000767124 ky=0.00128171 kz=22.7915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56915e-09 l2=1.96988e-05 x=4.90199e-05 y=-0.000239771 z=-9.85274e-06 kx=0.00119449 ky=-0.000409867 kz=22.9015 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.97233e-09 l2=9.35726e-06 x=-4.97806e-05 y=7.70929e-05 z=-4.68073e-06 kx=-0.000516061 ky=0.000908099 kz=23.035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13817e-09 l2=1.76911e-05 x=-4.92113e-05 y=0.000297005 z=-8.84688e-06 kx=-0.000359048 ky=0.000705528 kz=22.5603 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.67952e-09 l2=3.93456e-06 x=-4.99614e-05 y=0.000326501 z=-1.96867e-06 kx=0.000200992 ky=0.000721855 kz=22.5506 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.76778e-09 l2=9.3428e-06 x=4.97814e-05 y=-0.000499262 z=-4.67306e-06 kx=0.000125288 ky=-0.00223962 kz=23.0035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.99369e-09 l2=5.63967e-06 x=4.99206e-05 y=0.00031852 z=-2.81909e-06 kx=-0.00103652 ky=-0.000369414 kz=23.0649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10962e-09 l2=2.62737e-05 x=-4.82431e-05 y=-0.000365177 z=-1.3139e-05 kx=-0.000754059 ky=-0.000682896 kz=22.8212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29873e-09 l2=1.52093e-05 x=4.94183e-05 y=0.000313406 z=-7.60579e-06 kx=0.00023106 ky=0.000438008 kz=22.688 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37727e-09 l2=1.72021e-05 x=-4.92544e-05 y=0.000343487 z=-8.60369e-06 kx=-0.000891346 ky=0.00154792 kz=22.526 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08519e-09 l2=2.154e-05 x=-4.88259e-05 y=-0.000228945 z=-1.07727e-05 kx=-0.00100495 ky=-0.000847635 kz=22.9179 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.42949e-09 l2=8.50443e-06 x=4.98189e-05 y=6.90807e-05 z=-4.25471e-06 kx=0.000585796 ky=-0.000202137 kz=22.8301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11729e-09 l2=3.10419e-05 x=4.75303e-05 y=-1.28431e-05 z=-1.55212e-05 kx=-0.000126188 ky=-0.000848256 kz=22.8274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08911e-09 l2=1.51247e-05 x=-4.94251e-05 y=-0.00038978 z=-7.56124e-06 kx=0.000770581 ky=-0.000921237 kz=23.1803 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39104e-09 l2=2.78708e-05 x=-4.80187e-05 y=-9.53407e-05 z=-1.39371e-05 kx=-0.000473117 ky=-0.000192653 kz=22.6897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25113e-09 l2=5.35502e-06 x=4.99283e-05 y=-0.000266645 z=-2.67785e-06 kx=-0.000129579 ky=-0.00133577 kz=22.8346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15099e-09 l2=1.56966e-05 x=4.93802e-05 y=9.46293e-05 z=-7.84916e-06 kx=0.000135631 ky=0.000771499 kz=22.682 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30483e-09 l2=7.56101e-06 x=4.98568e-05 y=-0.000172299 z=-3.7838e-06 kx=0.000991142 ky=0.000639553 kz=23.1021 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.94937e-09 l2=2.37024e-06 x=-4.9986e-05 y=-0.000331091 z=-1.19013e-06 kx=-0.00024768 ky=0.000125909 kz=23.0126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53638e-09 l2=8.12796e-06 x=-4.98347e-05 y=-0.000455587 z=-4.06441e-06 kx=0.000156254 ky=5.08518e-05 kz=22.9689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36766e-09 l2=2.3382e-05 x=-4.86139e-05 y=-0.00010437 z=-1.16926e-05 kx=-0.000430808 ky=-0.00083101 kz=22.4383 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41845e-09 l2=2.8962e-05 x=-4.78569e-05 y=-0.000467803 z=-1.44829e-05 kx=-0.000559291 ky=-0.00152296 kz=23.0664 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02471e-09 l2=1.54614e-05 x=4.93989e-05 y=-0.000287954 z=-7.73065e-06 kx=-0.000246843 ky=-0.000586453 kz=22.4111 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23022e-09 l2=2.17403e-05 x=4.8804e-05 y=-0.000127033 z=-1.08719e-05 kx=0.000526724 ky=0.000264924 kz=23.2094 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07003e-09 l2=2.9841e-05 x=4.77217e-05 y=0.00049584 z=-1.49223e-05 kx=0.000597674 ky=0.00203074 kz=23.2573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31006e-09 l2=1.56987e-05 x=-4.93798e-05 y=-0.000200288 z=-7.8519e-06 kx=-0.000883966 ky=-0.000372311 kz=23.2265 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54607e-09 l2=1.24473e-05 x=4.96113e-05 y=0.00037965 z=-6.22395e-06 kx=-0.000207498 ky=0.00153668 kz=22.7544 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46415e-09 l2=5.09001e-06 x=-4.99353e-05 y=3.94355e-05 z=-2.54501e-06 kx=0.00032349 ky=4.20324e-05 kz=22.4019 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07829e-09 l2=1.96485e-05 x=-4.90251e-05 y=-0.00023927 z=-9.82673e-06 kx=-0.000891892 ky=0.000423319 kz=22.7645 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22741e-09 l2=7.70935e-06 x=4.98513e-05 y=0.000483196 z=-3.85399e-06 kx=-0.000590721 ky=0.00204745 kz=22.7471 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.01303e-09 l2=5.4907e-06 x=-4.99248e-05 y=0.000291682 z=-2.74701e-06 kx=0.00060233 ky=0.00111359 kz=22.4022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0541e-09 l2=2.82153e-05 x=-4.79681e-05 y=-0.000221026 z=-1.411e-05 kx=-0.000879062 ky=-0.000324557 kz=22.5204 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03479e-09 l2=1.53944e-05 x=4.94042e-05 y=-0.000471701 z=-7.69694e-06 kx=-0.000363754 ky=-0.00134538 kz=23.1062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13079e-09 l2=3.49399e-05 x=-4.68489e-05 y=0.000330833 z=-1.74705e-05 kx=-9.55141e-06 ky=7.02038e-05 kz=23.1065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45848e-09 l2=1.47922e-05 x=4.94498e-05 y=-0.000428371 z=-7.39855e-06 kx=0.000786418 ky=-0.00110637 kz=22.9075 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51713e-09 l2=1.33685e-05 x=4.9551e-05 y=0.000205754 z=-6.68749e-06 kx=0.00115507 ky=0.000963402 kz=22.9357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30268e-09 l2=2.90105e-05 x=4.78493e-05 y=-4.02514e-05 z=-1.45081e-05 kx=0.00106362 ky=9.68016e-05 kz=22.9166 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87176e-09 l2=1.20968e-05 x=4.96328e-05 y=-7.49583e-05 z=-6.0507e-06 kx=0.000624191 ky=-0.000649996 kz=23.0836 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16705e-09 l2=2.47889e-05 x=-4.84393e-05 y=-0.000263565 z=-1.2396e-05 kx=-0.000450855 ky=6.44364e-05 kz=22.3439 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51011e-09 l2=1.78127e-06 x=-4.99921e-05 y=8.56382e-05 z=-8.91067e-07 kx=0.000149458 ky=-0.000180872 kz=23.2436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67478e-09 l2=1.12709e-05 x=-4.96814e-05 y=0.000217834 z=-5.63796e-06 kx=-0.000524163 ky=-0.000325055 kz=22.3788 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.30252e-09 l2=1.0532e-05 x=4.97218e-05 y=-6.64729e-05 z=-5.2694e-06 kx=0.00102369 ky=-0.00118068 kz=22.7474 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03194e-09 l2=4.76151e-05 x=-4.39674e-05 y=0.000206538 z=-2.38099e-05 kx=-0.000962487 ky=0.000668681 kz=22.5878 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20826e-09 l2=2.34544e-05 x=-4.86053e-05 y=9.90184e-05 z=-1.17283e-05 kx=-0.0002513 ky=-2.84513e-05 kz=22.7352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35236e-09 l2=1.65748e-05 x=-4.93088e-05 y=-0.000196895 z=-8.28616e-06 kx=0.000887241 ky=0.000654552 kz=23.0155 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77104e-09 l2=2.35352e-05 x=-4.85951e-05 y=0.000465437 z=-1.1771e-05 kx=-0.00120234 ky=0.00208511 kz=22.8551 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98486e-09 l2=7.15218e-06 x=-4.98721e-05 y=4.95404e-05 z=-3.57691e-06 kx=0.000309117 ky=0.000267608 kz=22.9064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10215e-09 l2=8.01284e-06 x=4.98395e-05 y=0.000123097 z=-4.00564e-06 kx=-0.000822113 ky=-0.000160781 kz=22.405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56999e-09 l2=1.06764e-05 x=4.97145e-05 y=-0.00034312 z=-5.33742e-06 kx=-0.000735484 ky=0.000124346 kz=23.1854 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88857e-09 l2=1.96942e-05 x=-4.90208e-05 y=-0.000279023 z=-9.84856e-06 kx=-0.000240358 ky=-0.00154431 kz=22.6463 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95138e-09 l2=6.51776e-06 x=-4.98939e-05 y=-0.000331394 z=-3.25844e-06 kx=0.000888024 ky=-0.00112032 kz=23.1061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25244e-09 l2=1.6083e-05 x=4.93492e-05 y=0.000357488 z=-8.0419e-06 kx=-0.000101672 ky=-5.20711e-05 kz=22.5748 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29368e-09 l2=7.16453e-06 x=-4.98716e-05 y=-3.35341e-05 z=-3.58297e-06 kx=-2.81499e-05 ky=0.000922508 kz=22.6607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69099e-09 l2=1.2416e-05 x=-4.96132e-05 y=-0.000470582 z=-6.20906e-06 kx=-9.67642e-05 ky=-0.001863 kz=22.3391 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.82091e-09 l2=5.91775e-06 x=-4.99124e-05 y=0.000169066 z=-2.95942e-06 kx=0.00016627 ky=0.00100424 kz=22.7107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28217e-09 l2=1.07191e-05 x=4.97122e-05 y=-0.000400412 z=-5.35805e-06 kx=-0.000976959 ky=-0.000781762 kz=22.7791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59463e-09 l2=1.2603e-05 x=4.96016e-05 y=-0.000222402 z=-6.30051e-06 kx=-0.000827092 ky=-0.00143173 kz=23.0128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13607e-09 l2=1.91759e-05 x=-4.90723e-05 y=0.000417039 z=-9.58793e-06 kx=0.000274979 ky=-4.89789e-05 kz=22.9957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13142e-09 l2=1.2274e-05 x=-4.96219e-05 y=-0.000126661 z=-6.13888e-06 kx=-0.000612081 ky=-0.00142112 kz=22.7009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45721e-09 l2=1.78748e-05 x=-4.91945e-05 y=0.000350851 z=-8.94042e-06 kx=-0.00106554 ky=0.000533956 kz=23.1255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.00264e-09 l2=4.19522e-06 x=4.99562e-05 y=-0.000477633 z=-2.09943e-06 kx=-0.000534026 ky=-0.000280001 kz=22.6089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.66588e-09 l2=8.54014e-06 x=4.98173e-05 y=-0.000347356 z=-4.27364e-06 kx=0.00102782 ky=-0.000492908 kz=22.8914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09648e-09 l2=3.86791e-05 x=4.61086e-05 y=0.000475095 z=-1.93402e-05 kx=3.44702e-05 ky=0.00119669 kz=22.7223 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36475e-09 l2=2.14968e-05 x=-4.88311e-05 y=-0.000101575 z=-1.07495e-05 kx=-0.000179025 ky=0.000215788 kz=23.2754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80911e-09 l2=1.39599e-05 x=-4.95102e-05 y=0.000190327 z=-6.98299e-06 kx=-0.000978959 ky=-0.000602816 kz=22.9379 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.50278e-09 l2=1.25134e-05 x=-4.96072e-05 y=-0.000399661 z=-6.25733e-06 kx=0.000302004 ky=-0.000964238 kz=23.2678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65546e-09 l2=1.76128e-05 x=4.92182e-05 y=0.00018125 z=-8.80886e-06 kx=0.000780811 ky=0.000985124 kz=23.2222 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.219e-09 l2=2.10794e-05 x=4.88762e-05 y=3.87711e-05 z=-1.05424e-05 kx=0.000974026 ky=0.00111872 kz=22.5697 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77243e-09 l2=1.46438e-05 x=-4.94611e-05 y=-0.000340699 z=-7.32312e-06 kx=-0.000148468 ky=-0.00124545 kz=23.2356 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0901e-09 l2=2.95908e-05 x=4.77603e-05 y=-0.000441888 z=-1.47982e-05 kx=0.00107982 ky=-0.000952067 kz=22.9735 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.718e-09 l2=9.35173e-06 x=4.9781e-05 y=-0.000479625 z=-4.67844e-06 kx=0.000332119 ky=-0.00201266 kz=23.1091 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11066e-09 l2=3.11883e-05 x=-4.75054e-05 y=0.000418458 z=-1.55972e-05 kx=-0.00121773 ky=0.000101174 kz=23.0432 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41303e-09 l2=1.50314e-05 x=-4.94318e-05 y=0.000485781 z=-7.51815e-06 kx=-0.000787935 ky=0.000129999 kz=22.4429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06989e-09 l2=3.02529e-05 x=4.76571e-05 y=0.000277568 z=-1.51271e-05 kx=3.94918e-05 ky=0.000501612 kz=23.1846 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43271e-09 l2=6.90988e-06 x=4.98804e-05 y=0.0003324 z=-3.45874e-06 kx=0.00120175 ky=0.00162993 kz=23.1917 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.28268e-09 l2=5.37866e-06 x=-4.99278e-05 y=0.000264608 z=-2.69526e-06 kx=-0.000592976 ky=-7.11783e-05 kz=22.9202 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07469e-09 l2=2.12483e-05 x=-4.88587e-05 y=0.000165151 z=-1.06231e-05 kx=0.000779555 ky=0.000284281 kz=23.0807 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70635e-09 l2=9.6679e-06 x=-4.97657e-05 y=0.000329617 z=-4.83734e-06 kx=-0.000916658 ky=0.00082677 kz=22.4324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53727e-09 l2=1.13579e-05 x=-4.96768e-05 y=0.000472029 z=-5.67771e-06 kx=0.000907741 ky=0.000654525 kz=22.5524 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07407e-09 l2=1.86168e-05 x=4.91255e-05 y=0.000151065 z=-9.31148e-06 kx=0.00119887 ky=0.000368844 kz=23.2282 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14591e-09 l2=1.63988e-05 x=-4.93236e-05 y=-0.000296594 z=-8.19789e-06 kx=0.000984161 ky=-0.000123487 kz=23.2557 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29341e-09 l2=1.53442e-05 x=4.94078e-05 y=-2.16124e-05 z=-7.67395e-06 kx=0.000545987 ky=-0.00115592 kz=22.3093 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90173e-09 l2=7.73347e-06 x=4.98503e-05 y=-0.000216466 z=-3.86856e-06 kx=0.000394345 ky=3.43649e-05 kz=22.642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09603e-09 l2=5.06455e-06 x=-4.99359e-05 y=0.000278546 z=-2.53293e-06 kx=-4.99217e-05 ky=0.00177578 kz=23.2351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00495e-09 l2=7.27601e-06 x=4.98673e-05 y=0.000385094 z=-3.6412e-06 kx=0.00123117 ky=0.000793685 kz=22.7776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09565e-09 l2=2.09362e-05 x=4.88922e-05 y=-2.39715e-05 z=-1.04677e-05 kx=-0.000432833 ky=-0.000330744 kz=22.7883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75033e-09 l2=7.24632e-06 x=4.98687e-05 y=-0.000456768 z=-3.62444e-06 kx=-4.16683e-05 ky=-0.00175872 kz=22.8169 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02029e-09 l2=3.98116e-05 x=-4.58675e-05 y=-0.000364853 z=-1.99051e-05 kx=0.000608724 ky=-0.000194536 kz=23.134 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.18927e-09 l2=1.10179e-05 x=4.96956e-05 y=0.000370473 z=-5.51135e-06 kx=0.000604822 ky=0.00171738 kz=22.773 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53812e-09 l2=2.26163e-05 x=-4.87044e-05 y=-0.000156583 z=-1.13101e-05 kx=-0.000570941 ky=-0.00146399 kz=22.3332 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29701e-09 l2=1.88643e-05 x=4.91019e-05 y=-0.000199879 z=-9.4354e-06 kx=0.0012065 ky=-0.000608129 kz=22.6017 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.39587e-09 l2=7.60167e-06 x=4.98552e-05 y=0.000247451 z=-3.80524e-06 kx=0.00122364 ky=0.000680376 kz=22.4994 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16782e-09 l2=2.34563e-05 x=4.86054e-05 y=0.000325014 z=-1.17279e-05 kx=-0.000390393 ky=0.00164148 kz=22.8864 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59681e-09 l2=1.29258e-05 x=-4.95805e-05 y=0.000242339 z=-6.46526e-06 kx=-0.000729682 ky=0.000879538 kz=23.2014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39152e-09 l2=7.18445e-06 x=4.98709e-05 y=-2.03966e-05 z=-3.59342e-06 kx=-2.9794e-06 ky=-0.000556259 kz=22.331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62245e-09 l2=8.5519e-06 x=-4.98168e-05 y=-0.000454027 z=-4.27847e-06 kx=-0.000549099 ky=-0.00167807 kz=22.7117 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35133e-09 l2=6.92084e-06 x=4.98801e-05 y=-2.28836e-05 z=-3.46225e-06 kx=0.000293981 ky=-0.00105371 kz=22.436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07301e-09 l2=1.7731e-05 x=4.92077e-05 y=9.25131e-05 z=-8.86675e-06 kx=0.000337428 ky=-0.000146966 kz=22.5713 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.10173e-09 l2=7.94135e-06 x=-4.9842e-05 y=-0.00017617 z=-3.97387e-06 kx=-0.000984595 ky=-0.00072376 kz=22.83 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60328e-09 l2=2.09321e-05 x=-4.88929e-05 y=-0.000395166 z=-1.04649e-05 kx=0.000898913 ky=-0.000334198 kz=22.6842 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1082e-09 l2=2.24673e-05 x=4.87213e-05 y=0.000378266 z=-1.12364e-05 kx=0.00101708 ky=0.00185291 kz=23.0564 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22389e-09 l2=1.24286e-05 x=4.96124e-05 y=7.69615e-05 z=-6.21483e-06 kx=-4.32917e-05 ky=0.000116488 kz=22.6357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79868e-09 l2=1.01064e-05 x=4.97441e-05 y=6.11145e-05 z=-5.05425e-06 kx=5.79121e-05 ky=-0.000933051 kz=22.781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33176e-09 l2=1.86566e-05 x=4.91226e-05 y=0.000195472 z=-9.3271e-06 kx=-0.000848975 ky=0.00031138 kz=22.5309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50238e-09 l2=9.35384e-06 x=-4.97809e-05 y=4.11603e-05 z=-4.67699e-06 kx=0.000309566 ky=-2.68091e-05 kz=22.6516 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79592e-09 l2=1.29496e-05 x=4.95789e-05 y=0.000441134 z=-6.47708e-06 kx=0.000642273 ky=-2.01963e-05 kz=22.7464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28424e-09 l2=1.80391e-05 x=-4.91801e-05 y=-0.000396529 z=-9.01918e-06 kx=0.000468082 ky=-0.0013562 kz=22.4678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19747e-09 l2=3.15588e-06 x=-4.9975e-05 y=0.000133244 z=-1.58099e-06 kx=-0.00113243 ky=-0.000774437 kz=23.1161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03594e-09 l2=2.50061e-05 x=4.84111e-05 y=-0.000365634 z=-1.25057e-05 kx=0.00100014 ky=0.000182769 kz=22.6568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.44242e-09 l2=3.0316e-06 x=-4.99771e-05 y=-0.000370233 z=-1.51804e-06 kx=-8.17673e-06 ky=-0.00128924 kz=22.5466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38111e-09 l2=1.92633e-05 x=-4.90636e-05 y=0.000178748 z=-9.63252e-06 kx=-8.74814e-05 ky=0.000359416 kz=22.8671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36977e-09 l2=1.51649e-05 x=-4.94218e-05 y=0.000283134 z=-7.58333e-06 kx=-0.000100876 ky=-0.000343331 kz=22.4013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13427e-09 l2=6.33651e-06 x=4.98997e-05 y=0.00035397 z=-3.16706e-06 kx=-0.000796796 ky=0.00168542 kz=22.5214 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.43257e-09 l2=1.04486e-05 x=4.97263e-05 y=-0.000342935 z=-5.22826e-06 kx=0.00103479 ky=0.000293094 kz=23.1174 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63997e-09 l2=1.43967e-05 x=-4.94791e-05 y=6.73894e-05 z=-7.2015e-06 kx=-0.000860907 ky=-3.18843e-05 kz=23.298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86554e-09 l2=2.15755e-05 x=4.88227e-05 y=0.000292942 z=-1.07881e-05 kx=-0.000276295 ky=0.00110334 kz=22.8 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.19667e-09 l2=7.49884e-06 x=4.98594e-05 y=0.00037834 z=-3.74935e-06 kx=-0.00053382 ky=0.00137306 kz=22.8568 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.61569e-09 l2=1.42514e-06 x=4.9995e-05 y=0.000159777 z=-7.14777e-07 kx=-0.000974975 ky=-0.000528244 kz=23.1948 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26079e-09 l2=1.47578e-05 x=-4.94529e-05 y=0.000203512 z=-7.37747e-06 kx=0.00096379 ky=0.00146662 kz=22.9087 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46426e-09 l2=9.1989e-06 x=-4.97878e-05 y=0.00020021 z=-4.60259e-06 kx=-0.00110392 ky=-5.29494e-05 kz=22.8382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79424e-09 l2=1.30805e-05 x=-4.95702e-05 y=-0.000294214 z=-6.5435e-06 kx=-0.00106373 ky=-0.000618808 kz=22.4014 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0223e-09 l2=1.43411e-05 x=-4.94835e-05 y=0.000443464 z=-7.16893e-06 kx=0.000997673 ky=0.000402363 kz=23.2027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.87729e-09 l2=1.11068e-05 x=4.96905e-05 y=0.000193382 z=-5.55669e-06 kx=0.00106631 ky=0.000871586 kz=22.3816 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.71127e-09 l2=9.86246e-06 x=-4.97564e-05 y=0.000187962 z=-4.93272e-06 kx=-6.4623e-05 ky=0.00105942 kz=23.1558 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50627e-09 l2=7.24338e-06 x=4.98687e-05 y=-3.36845e-05 z=-3.62241e-06 kx=-1.68084e-05 ky=-0.000457491 kz=22.6961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13534e-09 l2=1.29908e-05 x=-4.95766e-05 y=-6.5692e-05 z=-6.49456e-06 kx=0.000647518 ky=-0.00118979 kz=22.7437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21969e-09 l2=1.978e-05 x=-4.90123e-05 y=3.63204e-05 z=-9.8901e-06 kx=0.000240222 ky=-0.000502816 kz=23.0898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.71347e-09 l2=4.23525e-06 x=-4.99552e-05 y=0.000155689 z=-2.12183e-06 kx=-0.000605022 ky=0.00109548 kz=22.3971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08774e-09 l2=9.81248e-06 x=4.97587e-05 y=0.000484105 z=-4.90752e-06 kx=0.000330103 ky=0.00108112 kz=22.3976 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78527e-09 l2=4.69503e-06 x=4.99449e-05 y=0.000464026 z=-2.34877e-06 kx=0.000163417 ky=-7.99535e-07 kz=22.4493 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13376e-09 l2=3.53484e-05 x=4.67726e-05 y=0.000452374 z=-1.76737e-05 kx=-0.000528274 ky=0.00102218 kz=23.0849 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80909e-09 l2=2.25953e-05 x=4.87076e-05 y=-0.000183672 z=-1.12966e-05 kx=-0.000879522 ky=-0.00116128 kz=22.6009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.09516e-09 l2=1.30984e-06 x=4.99957e-05 y=0.000343655 z=-6.59782e-07 kx=0.00103947 ky=0.00129708 kz=22.4714 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49762e-09 l2=2.11401e-05 x=-4.88697e-05 y=1.2784e-05 z=-1.05727e-05 kx=-0.000896959 ky=0.000989609 kz=23.1479 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13427e-09 l2=2.33748e-05 x=-4.86145e-05 y=-0.00012746 z=-1.16899e-05 kx=-0.000901612 ky=0.000376316 kz=22.9569 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19927e-09 l2=1.33619e-05 x=4.95519e-05 y=-0.000301266 z=-6.67998e-06 kx=-0.000732316 ky=3.47969e-05 kz=23.0892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0673e-09 l2=2.56172e-05 x=-4.83319e-05 y=-0.000358196 z=-1.28083e-05 kx=0.000393914 ky=-0.000871653 kz=22.3378 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05033e-09 l2=2.48745e-05 x=-4.84281e-05 y=0.000143085 z=-1.24395e-05 kx=-0.000787965 ky=0.00136345 kz=22.3377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18473e-09 l2=4.3045e-05 x=-4.51311e-05 y=-0.000261532 z=-2.15229e-05 kx=7.81056e-05 ky=-0.00111512 kz=22.6358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10221e-09 l2=1.08565e-05 x=4.97046e-05 y=-7.86974e-05 z=-5.4278e-06 kx=-0.000453185 ky=-0.000951999 kz=22.9799 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2932e-09 l2=2.82801e-05 x=-4.79587e-05 y=-4.59689e-05 z=-1.41423e-05 kx=-0.000756414 ky=-0.000325061 kz=23.2297 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.93556e-09 l2=1.20428e-05 x=4.96364e-05 y=-0.000278519 z=-6.02077e-06 kx=-0.000741365 ky=0.000338696 kz=22.6353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07187e-09 l2=3.10783e-05 x=4.75236e-05 y=0.000108305 z=-1.55414e-05 kx=0.000835558 ky=-0.00074008 kz=22.4182 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14456e-09 l2=2.24112e-05 x=-4.87287e-05 y=-0.000445716 z=-1.12043e-05 kx=0.000858446 ky=-5.36338e-05 kz=22.3805 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24276e-09 l2=2.0323e-05 x=4.8957e-05 y=0.000375369 z=-1.01606e-05 kx=-0.000693311 ky=0.00131632 kz=22.3487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51763e-09 l2=1.93012e-05 x=4.90599e-05 y=0.000222474 z=-9.65151e-06 kx=6.85156e-05 ky=-3.16112e-05 kz=22.6382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68392e-09 l2=8.73018e-06 x=-4.98091e-05 y=0.000303515 z=-4.36724e-06 kx=-0.00060652 ky=0.000145493 kz=23.0592 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05508e-09 l2=4.01947e-05 x=4.5784e-05 y=-1.1537e-05 z=-2.00965e-05 kx=-0.000674994 ky=-0.000220916 kz=23.189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66154e-09 l2=1.14755e-05 x=4.967e-05 y=0.000382597 z=-5.73694e-06 kx=-0.000773625 ky=-6.23819e-05 kz=23.1566 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23678e-09 l2=1.85645e-05 x=4.91309e-05 y=-0.000282838 z=-9.28293e-06 kx=3.35428e-05 ky=-0.00016152 kz=22.4141 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79505e-09 l2=7.70442e-06 x=4.98514e-05 y=0.000170685 z=-3.85429e-06 kx=0.000532193 ky=0.00110863 kz=22.3361 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.69187e-09 l2=2.2841e-05 x=4.86787e-05 y=0.000461582 z=-1.14203e-05 kx=-0.000465631 ky=0.000543493 kz=22.9148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.4317e-09 l2=2.3797e-06 x=4.99859e-05 y=-0.000292494 z=-1.19491e-06 kx=0.000848613 ky=-0.000501731 kz=22.9456 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39792e-09 l2=5.42511e-06 x=4.99263e-05 y=0.000417466 z=-2.71496e-06 kx=0.000775867 ky=0.00181213 kz=22.6702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.96943e-09 l2=1.78458e-05 x=-4.91977e-05 y=-0.000348879 z=-8.92314e-06 kx=0.000336338 ky=0.00030282 kz=22.8027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31122e-09 l2=1.25712e-05 x=4.96031e-05 y=0.000381279 z=-6.28893e-06 kx=0.00123525 ky=0.0010275 kz=22.8631 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15665e-09 l2=1.39789e-05 x=4.95094e-05 y=0.000317701 z=-6.98907e-06 kx=-0.000662114 ky=0.00017516 kz=22.694 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26043e-09 l2=2.49515e-05 x=-4.84187e-05 y=-4.45501e-05 z=-1.24764e-05 kx=-2.55419e-05 ky=-0.000357079 kz=23.0079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22952e-09 l2=2.07092e-05 x=4.89159e-05 y=0.000417383 z=-1.03565e-05 kx=0.000608773 ky=0.00114311 kz=22.6189 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03195e-09 l2=1.93159e-05 x=-4.90581e-05 y=-0.000249135 z=-9.66046e-06 kx=-0.000931061 ky=-0.000215154 kz=22.7351 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48467e-09 l2=1.14665e-05 x=-4.96703e-05 y=-2.93251e-05 z=-5.73435e-06 kx=-0.000160617 ky=-0.00108931 kz=22.5312 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14066e-09 l2=2.63848e-05 x=4.82286e-05 y=-0.000279167 z=-1.3192e-05 kx=-0.000459563 ky=-0.00036695 kz=22.8581 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74124e-09 l2=9.16016e-06 x=-4.979e-05 y=0.000295322 z=-4.57925e-06 kx=0.000774361 ky=0.000149975 kz=22.7062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55419e-09 l2=1.32679e-05 x=-4.95582e-05 y=-0.000336075 z=-6.6333e-06 kx=0.000639861 ky=-0.00109894 kz=22.6435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.07686e-09 l2=3.25387e-06 x=-4.99736e-05 y=0.000196599 z=-1.62926e-06 kx=-0.000127199 ky=0.00113966 kz=22.7044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02409e-09 l2=4.51184e-05 x=4.46216e-05 y=0.000219539 z=-2.25602e-05 kx=0.000237717 ky=0.000383647 kz=22.9923 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.00556e-09 l2=3.86058e-06 x=-4.99627e-05 y=-0.000361596 z=-1.93385e-06 kx=-0.000724956 ky=0.000304422 kz=23.1914 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20218e-09 l2=2.75865e-05 x=4.80593e-05 y=0.000357598 z=-1.37964e-05 kx=0.00119658 ky=0.00107654 kz=22.8234 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05292e-09 l2=1.20083e-05 x=4.96384e-05 y=-0.000494441 z=-6.00374e-06 kx=-0.000425729 ky=-0.00144599 kz=22.613 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05678e-09 l2=1.71711e-05 x=4.92574e-05 y=7.19147e-05 z=-8.58763e-06 kx=0.000495421 ky=0.000322052 kz=22.7466 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.68705e-09 l2=7.9453e-06 x=4.98419e-05 y=-0.00033486 z=-3.97537e-06 kx=0.000629467 ky=-0.000840549 kz=22.8371 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36647e-09 l2=4.03805e-06 x=-4.99592e-05 y=0.000454601 z=-2.02156e-06 kx=-0.000856232 ky=0.00174247 kz=23.0936 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57153e-09 l2=5.70509e-06 x=-4.99185e-05 y=-3.67102e-05 z=-2.85494e-06 kx=-0.000726849 ky=0.000759267 kz=22.5897 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14333e-09 l2=1.66778e-05 x=4.93e-05 y=0.000401559 z=-8.33939e-06 kx=-0.000271165 ky=0.00172777 kz=22.7989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.66724e-09 l2=1.12766e-05 x=4.96812e-05 y=-0.000336466 z=-5.63993e-06 kx=0.000129037 ky=-0.00083916 kz=22.8181 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80483e-09 l2=1.91594e-05 x=-4.90734e-05 y=0.000429429 z=-9.58309e-06 kx=-0.00113854 ky=0.00190516 kz=22.4657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46493e-09 l2=1.36256e-05 x=4.95335e-05 y=0.000341678 z=-6.81536e-06 kx=0.000844508 ky=9.46741e-05 kz=23.216 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09066e-09 l2=3.60452e-05 x=-4.66392e-05 y=-0.000180086 z=-1.80229e-05 kx=0.000108108 ky=0.000278431 kz=22.9809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.52642e-09 l2=7.39043e-06 x=4.98634e-05 y=-0.000410579 z=-3.69615e-06 kx=-0.000150629 ky=-0.00034359 kz=22.8555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32308e-09 l2=3.45059e-05 x=-4.69298e-05 y=-0.000470033 z=-1.72522e-05 kx=0.000663448 ky=-0.000676551 kz=23.0274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.53192e-09 l2=6.86441e-06 x=-4.98821e-05 y=-5.14067e-05 z=-3.43413e-06 kx=-0.000300073 ky=-0.00021147 kz=22.6471 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70762e-09 l2=1.42481e-05 x=4.94901e-05 y=0.00028494 z=-7.12406e-06 kx=-0.000375323 ky=0.0016173 kz=22.5951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61699e-09 l2=1.39432e-05 x=-4.95119e-05 y=0.000301533 z=-6.97071e-06 kx=0.000793587 ky=-0.000113512 kz=23.2443 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41511e-09 l2=1.49485e-05 x=4.94385e-05 y=-0.000256942 z=-7.47376e-06 kx=-0.000544813 ky=-0.000162216 kz=22.3848 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.32909e-09 l2=1.07881e-05 x=-4.97085e-05 y=0.000468845 z=-5.39434e-06 kx=0.000614419 ky=0.00121764 kz=22.6733 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01479e-09 l2=1.85198e-05 x=4.91348e-05 y=0.000211409 z=-9.26234e-06 kx=0.000882346 ky=-0.000602466 kz=22.7032 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28873e-09 l2=2.04126e-05 x=4.89474e-05 y=0.000187547 z=-1.02065e-05 kx=-0.000179749 ky=0.000256726 kz=22.672 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.38358e-09 l2=2.76264e-05 x=4.8054e-05 y=0.000249182 z=-1.38147e-05 kx=0.000411113 ky=0.000688893 kz=22.9487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65823e-09 l2=1.05131e-05 x=-4.97231e-05 y=-0.00023302 z=-5.25633e-06 kx=0.000469753 ky=-0.000945064 kz=22.5809 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.76404e-09 l2=3.28337e-06 x=-4.99731e-05 y=0.000474694 z=-1.64602e-06 kx=-0.000653358 ky=0.000413441 kz=22.4891 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33149e-09 l2=9.38784e-06 x=-4.97791e-05 y=2.9976e-05 z=-4.69763e-06 kx=-0.00114257 ky=0.000936627 kz=22.384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43888e-09 l2=1.96804e-05 x=4.90225e-05 y=-0.000224716 z=-9.83994e-06 kx=-0.000470123 ky=-0.000400833 kz=23.2985 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27114e-09 l2=3.06828e-05 x=4.75889e-05 y=-4.855e-05 z=-1.53407e-05 kx=-0.000611812 ky=0.000551042 kz=22.8827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55857e-09 l2=4.44651e-06 x=-4.99505e-05 y=4.22275e-05 z=-2.2253e-06 kx=-0.000566985 ky=0.000607326 kz=22.3307 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.66553e-09 l2=4.65587e-06 x=-4.99458e-05 y=0.000140498 z=-2.3328e-06 kx=-0.00093613 ky=0.00141452 kz=23.0009 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72013e-09 l2=1.20332e-05 x=4.96369e-05 y=-0.000285284 z=-6.01653e-06 kx=-0.000413774 ky=-0.00110142 kz=22.5651 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48833e-09 l2=1.26287e-05 x=-4.95998e-05 y=-6.32358e-05 z=-6.31521e-06 kx=-5.96787e-05 ky=-0.00023542 kz=22.6261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05593e-09 l2=3.29912e-05 x=4.72008e-05 y=-5.15395e-05 z=-1.6496e-05 kx=-6.19822e-05 ky=0.000659294 kz=22.3738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10515e-09 l2=2.2794e-05 x=4.86835e-05 y=0.000382354 z=-1.13993e-05 kx=0.000790681 ky=0.000809425 kz=22.8145 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47503e-09 l2=1.23768e-05 x=4.96155e-05 y=-0.000420676 z=-6.19048e-06 kx=0.000618772 ky=-3.14814e-05 kz=23.0288 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.02819e-09 l2=7.10814e-06 x=4.98738e-05 y=0.000127492 z=-3.5536e-06 kx=-0.000912874 ky=-0.000584419 kz=23.0231 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.89004e-09 l2=1.33068e-05 x=4.95555e-05 y=0.000470556 z=-6.65443e-06 kx=4.75341e-05 ky=0.00201368 kz=22.3794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.47541e-09 l2=8.87054e-06 x=4.98031e-05 y=0.00020506 z=-4.43598e-06 kx=-0.000472608 ky=1.25426e-05 kz=23.0293 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02884e-09 l2=1.44574e-05 x=4.94747e-05 y=0.00037372 z=-7.22951e-06 kx=0.000134716 ky=0.00154839 kz=22.9464 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.71744e-09 l2=2.22844e-05 x=-4.87431e-05 y=0.000352165 z=-1.11423e-05 kx=0.000384377 ky=0.00147408 kz=22.8637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53281e-09 l2=1.48997e-05 x=-4.9442e-05 y=0.000220186 z=-7.4508e-06 kx=-9.1525e-05 ky=-0.000613778 kz=22.6237 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73874e-09 l2=1.05646e-05 x=4.97204e-05 y=5.02852e-05 z=-5.28187e-06 kx=-0.000586621 ky=-8.23837e-05 kz=22.4184 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65544e-09 l2=1.05797e-05 x=4.97194e-05 y=-0.000280895 z=-5.29119e-06 kx=0.000235629 ky=-0.00056693 kz=22.4851 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51325e-09 l2=1.05173e-05 x=-4.97229e-05 y=-0.000164873 z=-5.25782e-06 kx=0.000730277 ky=0.000146066 kz=23.1476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18137e-09 l2=4.12812e-05 x=4.55416e-05 y=0.000159233 z=-2.06401e-05 kx=-0.000543923 ky=-0.000508859 kz=23.2508 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25764e-09 l2=1.54245e-05 x=4.9402e-05 y=-0.000267834 z=-7.71241e-06 kx=-0.000453611 ky=-0.00117005 kz=22.7415 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30189e-08 l2=1.78244e-06 x=4.99922e-05 y=-0.000304373 z=-8.97921e-07 kx=8.96842e-05 ky=-0.00126039 kz=23.2743 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23802e-09 l2=1.24308e-05 x=-4.96125e-05 y=-0.000426483 z=-6.21404e-06 kx=0.000933809 ky=-0.000927144 kz=23.2999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12853e-09 l2=1.83342e-05 x=-4.91527e-05 y=-7.16514e-05 z=-9.16718e-06 kx=0.000221655 ky=-1.07441e-05 kz=22.4869 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0685e-09 l2=2.61908e-05 x=4.82549e-05 y=-0.000460127 z=-1.30955e-05 kx=-0.000218862 ky=-0.00111717 kz=23.0422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08134e-09 l2=1.78818e-05 x=-4.91946e-05 y=-0.000225577 z=-8.93939e-06 kx=0.000947351 ky=-0.00124211 kz=22.4437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39866e-09 l2=2.4234e-05 x=4.85101e-05 y=-0.000299344 z=-1.21161e-05 kx=-0.000732776 ky=-0.00131194 kz=22.7237 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11098e-09 l2=1.02262e-05 x=-4.9738e-05 y=0.000383891 z=-5.11326e-06 kx=0.00018574 ky=0.00201734 kz=23.2275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11008e-09 l2=1.22711e-05 x=4.96222e-05 y=-6.58907e-05 z=-6.13623e-06 kx=4.71128e-05 ky=0.000530269 kz=22.4838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.39158e-09 l2=1.77043e-05 x=4.92103e-05 y=-5.84839e-05 z=-8.85295e-06 kx=5.7178e-05 ky=-8.78982e-05 kz=22.6951 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00472e-09 l2=1.75679e-05 x=4.92227e-05 y=-0.000439004 z=-8.78331e-06 kx=-0.00052433 ky=-0.00147543 kz=22.4913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0979e-09 l2=1.84426e-05 x=4.9142e-05 y=-0.000421688 z=-9.22402e-06 kx=0.00101277 ky=-0.00194429 kz=23.0519 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.14844e-09 l2=5.91827e-06 x=4.99124e-05 y=-7.00269e-05 z=-2.96085e-06 kx=0.000297621 ky=-0.000494777 kz=23.1062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10385e-09 l2=2.59935e-05 x=4.8282e-05 y=0.00017227 z=-1.29953e-05 kx=-0.000950539 ky=0.000108151 kz=22.6451 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78904e-09 l2=1.23223e-05 x=-4.96193e-05 y=2.36682e-05 z=-6.15982e-06 kx=0.00101063 ky=3.76327e-07 kz=22.6022 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.23478e-09 l2=7.92069e-06 x=-4.9843e-05 y=0.000476846 z=-3.96115e-06 kx=0.000138282 ky=0.00181441 kz=22.4597 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12081e-09 l2=1.61591e-05 x=4.93429e-05 y=-7.92371e-05 z=-8.08041e-06 kx=0.000135071 ky=0.000452623 kz=22.5553 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31536e-09 l2=1.20708e-05 x=-4.96343e-05 y=-0.000112371 z=-6.03756e-06 kx=-0.00068919 ky=-0.000751147 kz=23.1257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.7093e-09 l2=1.52543e-05 x=4.94148e-05 y=0.000333256 z=-7.62891e-06 kx=0.000423891 ky=0.00072919 kz=23.1505 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2081e-09 l2=2.03531e-05 x=4.89539e-05 y=4.59018e-05 z=-1.01755e-05 kx=-0.000790967 ky=0.00100612 kz=22.7197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74901e-09 l2=2.04446e-05 x=-4.89442e-05 y=0.000430616 z=-1.02226e-05 kx=0.000260404 ky=0.000197766 kz=22.8395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52262e-09 l2=1.05392e-05 x=4.97217e-05 y=-0.000202515 z=-5.2692e-06 kx=-0.000521834 ky=-0.00118404 kz=22.8257 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36759e-09 l2=1.16687e-05 x=4.96582e-05 y=0.000493897 z=-5.83768e-06 kx=0.00118845 ky=0.00203062 kz=22.4572 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91288e-09 l2=2.54361e-05 x=-4.83559e-05 y=-0.000110468 z=-1.27184e-05 kx=0.000277197 ky=0.000364742 kz=23.0549 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26755e-09 l2=3.04331e-05 x=4.76289e-05 y=0.000210872 z=-1.5216e-05 kx=-0.000568517 ky=-7.43812e-05 kz=23.2035 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01387e-09 l2=2.06986e-05 x=-4.89167e-05 y=-1.5135e-05 z=-1.03525e-05 kx=-0.00120146 ky=0.000594331 kz=22.3331 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0237e-09 l2=1.1001e-05 x=-4.96967e-05 y=0.000235706 z=-5.49949e-06 kx=0.00068477 ky=0.0001169 kz=22.5879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.31516e-09 l2=2.48005e-05 x=4.84376e-05 y=-7.3795e-05 z=-1.2403e-05 kx=0.000977501 ky=-0.000431797 kz=22.6311 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3176e-09 l2=2.20193e-05 x=4.87729e-05 y=-0.000116501 z=-1.10105e-05 kx=6.67458e-05 ky=0.000588826 kz=22.995 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30721e-09 l2=2.5938e-05 x=-4.82891e-05 y=-0.00014711 z=-1.29689e-05 kx=0.000373736 ky=-0.00109647 kz=23.2126 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.47835e-09 l2=6.7881e-06 x=-4.98846e-05 y=0.000291032 z=-3.39791e-06 kx=-0.00098371 ky=0.000585801 kz=23.0768 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36689e-09 l2=1.91666e-05 x=-4.90734e-05 y=0.000162029 z=-9.58274e-06 kx=0.000568976 ky=0.0014885 kz=22.6877 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02214e-09 l2=2.13957e-05 x=-4.88424e-05 y=0.000461713 z=-1.06976e-05 kx=0.000365775 ky=0.000697236 kz=22.5879 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23786e-09 l2=2.57218e-05 x=4.83174e-05 y=2.66013e-06 z=-1.28631e-05 kx=0.000732002 ky=0.000449846 kz=22.759 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36747e-09 l2=2.84985e-05 x=4.79262e-05 y=-0.000162581 z=-1.42519e-05 kx=0.000919482 ky=-0.000410815 kz=22.9738 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.63057e-09 l2=9.46285e-06 x=-4.97758e-05 y=-3.80539e-05 z=-4.73199e-06 kx=0.000340584 ky=0.00053415 kz=22.619 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03673e-09 l2=1.71959e-05 x=-4.92555e-05 y=0.000105977 z=-8.59704e-06 kx=0.000672491 ky=0.00134547 kz=22.9242 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.83167e-09 l2=8.4107e-06 x=-4.98229e-05 y=-4.59319e-06 z=-4.20635e-06 kx=-3.78575e-05 ky=0.000646308 kz=23.175 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16816e-09 l2=1.57803e-05 x=-4.9374e-05 y=0.000264118 z=-7.88851e-06 kx=0.00100059 ky=0.000178592 kz=22.3039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22741e-09 l2=1.05239e-05 x=4.97225e-05 y=0.000455585 z=-5.26158e-06 kx=-0.000438548 ky=0.000216172 kz=22.4302 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04357e-09 l2=9.74809e-06 x=4.97618e-05 y=0.000160794 z=-4.87566e-06 kx=0.000492723 ky=0.00023745 kz=22.3684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01871e-09 l2=1.51481e-05 x=4.94227e-05 y=0.000136494 z=-7.57723e-06 kx=0.00120764 ky=8.03218e-05 kz=22.3274 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.55351e-09 l2=8.8073e-06 x=4.98057e-05 y=-4.23641e-05 z=-4.40544e-06 kx=0.000460822 ky=-0.000189755 kz=22.5437 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16368e-09 l2=1.59146e-05 x=4.93627e-05 y=1.31642e-05 z=-7.95885e-06 kx=0.000441071 ky=-0.000394606 kz=22.9993 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15312e-09 l2=2.45462e-05 x=-4.84707e-05 y=1.61862e-06 z=-1.22728e-05 kx=0.00040986 ky=-0.00052287 kz=22.3065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0603e-09 l2=1.97081e-05 x=-4.90189e-05 y=0.000361764 z=-9.85722e-06 kx=-0.00121848 ky=0.00101892 kz=22.5915 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.57054e-09 l2=7.02419e-06 x=-4.98766e-05 y=-0.000291485 z=-3.5146e-06 kx=-0.000333959 ky=-0.00119301 kz=22.9523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22579e-09 l2=1.21661e-05 x=4.96288e-05 y=-0.000144747 z=-6.08238e-06 kx=-0.000578562 ky=-0.000918276 kz=22.3546 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.33517e-09 l2=1.65667e-05 x=4.93089e-05 y=0.000255401 z=-8.28687e-06 kx=0.00106316 ky=-2.29522e-05 kz=22.362 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.1429e-09 l2=1.20567e-05 x=-4.96356e-05 y=0.00030205 z=-6.02845e-06 kx=0.000677193 ky=-0.000111066 kz=22.7746 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.37645e-09 l2=6.47564e-06 x=-4.98952e-05 y=-3.19588e-05 z=-3.23809e-06 kx=0.000419873 ky=-0.00110462 kz=22.8827 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37397e-09 l2=2.4079e-05 x=-4.85287e-05 y=-0.000267509 z=-1.20417e-05 kx=-0.00071084 ky=0.000188935 kz=23.2163 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20245e-09 l2=1.92328e-05 x=4.90664e-05 y=0.000222535 z=-9.61851e-06 kx=0.000698497 ky=0.0014485 kz=22.6341 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25543e-09 l2=1.25885e-05 x=4.96021e-05 y=0.00015132 z=-6.29663e-06 kx=0.000793684 ky=-0.00056914 kz=22.6298 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.17661e-09 l2=3.49996e-06 x=4.99696e-05 y=-0.000314823 z=-1.75228e-06 kx=-0.000820893 ky=-0.00170529 kz=22.9642 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24235e-09 l2=2.00935e-05 x=4.89805e-05 y=-0.000306603 z=-1.00465e-05 kx=-0.000413147 ky=-0.00153124 kz=22.875 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43245e-09 l2=1.88163e-05 x=4.91066e-05 y=-0.000249458 z=-9.41103e-06 kx=0.00100912 ky=-0.000367981 kz=23.1116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88367e-09 l2=2.35301e-05 x=-4.85966e-05 y=0.000278949 z=-1.17649e-05 kx=0.0005221 ky=0.00162294 kz=22.3907 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23498e-09 l2=2.30157e-05 x=-4.86574e-05 y=0.000315896 z=-1.15101e-05 kx=-0.000792673 ky=0.00137599 kz=23.2076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42398e-09 l2=1.14665e-05 x=-4.96704e-05 y=-2.14655e-05 z=-5.73319e-06 kx=0.000347716 ky=-0.000528675 kz=22.9354 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20217e-09 l2=2.13791e-05 x=-4.88444e-05 y=0.000261999 z=-1.0689e-05 kx=0.000537485 ky=0.000251631 kz=22.7275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.82096e-09 l2=8.91213e-06 x=-4.98011e-05 y=-1.43744e-05 z=-4.45854e-06 kx=-0.000477467 ky=-0.00105902 kz=22.4147 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.54593e-09 l2=2.07017e-05 x=-4.89169e-05 y=0.000259073 z=-1.0352e-05 kx=-0.000177245 ky=0.000624811 kz=22.9397 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68435e-09 l2=9.88383e-06 x=4.97554e-05 y=6.6865e-06 z=-4.94108e-06 kx=-0.000757157 ky=-0.000419816 kz=22.4811 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04346e-09 l2=1.79635e-05 x=-4.91871e-05 y=-0.000351067 z=-8.98068e-06 kx=0.000720284 ky=-0.000500041 kz=22.6226 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65438e-09 l2=1.24812e-05 x=-4.96091e-05 y=-0.000413285 z=-6.24145e-06 kx=-2.20899e-05 ky=-0.00188209 kz=22.4899 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15409e-09 l2=1.58793e-05 x=4.93656e-05 y=0.000114472 z=-7.94077e-06 kx=0.000256801 ky=-0.000200466 kz=22.3593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90757e-09 l2=7.08776e-06 x=-4.98742e-05 y=-0.000485339 z=-3.54636e-06 kx=-0.000691868 ky=-0.00219477 kz=22.6115 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52801e-09 l2=1.73992e-05 x=-4.92372e-05 y=-0.000438934 z=-8.70177e-06 kx=-0.000649284 ky=-0.000567678 kz=22.8732 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00711e-09 l2=3.99016e-05 x=-4.58476e-05 y=-0.000193493 z=-1.99508e-05 kx=0.000224208 ky=0.000577047 kz=22.4483 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01083e-09 l2=2.40952e-05 x=-4.85266e-05 y=-0.000429696 z=-1.20498e-05 kx=-0.000793729 ky=-0.00129878 kz=22.5192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01045e-09 l2=2.18522e-05 x=-4.8792e-05 y=0.000424078 z=-1.09253e-05 kx=0.000615571 ky=0.00161934 kz=23.2513 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03005e-09 l2=2.1219e-05 x=-4.88615e-05 y=-0.000491957 z=-1.06103e-05 kx=-0.000115605 ky=-0.00113162 kz=22.368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.31766e-09 l2=4.95085e-06 x=4.99388e-05 y=-0.000231794 z=-2.47635e-06 kx=-0.000341627 ky=-0.000277089 kz=23.1512 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09602e-09 l2=8.33852e-06 x=4.98258e-05 y=-0.000211374 z=-4.17178e-06 kx=0.00091241 ky=-9.56068e-05 kz=23.0804 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20801e-09 l2=1.84271e-05 x=-4.91437e-05 y=0.0004654 z=-9.21529e-06 kx=-0.000525716 ky=0.00079755 kz=22.6646 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.27512e-09 l2=3.33809e-06 x=-4.99722e-05 y=-6.06778e-05 z=-1.67261e-06 kx=-0.000424185 ky=-0.000695159 kz=22.9333 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07982e-09 l2=1.20459e-05 x=4.9636e-05 y=-1.43651e-05 z=-6.02356e-06 kx=3.48545e-05 ky=-0.000752552 kz=22.9086 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98006e-09 l2=4.89169e-06 x=-4.99402e-05 y=-0.000125104 z=-2.44794e-06 kx=-0.000281816 ky=-0.000803923 kz=23.0405 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61652e-09 l2=9.38475e-06 x=4.97793e-05 y=4.33328e-05 z=-4.69432e-06 kx=0.000511984 ky=0.000755512 kz=22.4446 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13428e-09 l2=1.14249e-05 x=4.96729e-05 y=-8.68749e-05 z=-5.71101e-06 kx=-0.00092039 ky=0.000263097 kz=22.7662 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13321e-09 l2=2.74845e-05 x=4.80749e-05 y=-0.000298358 z=-1.37416e-05 kx=-0.000591307 ky=0.000315154 kz=23.0657 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02638e-09 l2=2.16179e-05 x=-4.88173e-05 y=-0.000485236 z=-1.08119e-05 kx=-0.00111916 ky=-0.00219203 kz=22.7424 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04217e-09 l2=3.49611e-05 x=4.68441e-05 y=-0.000197807 z=-1.74833e-05 kx=0.00106389 ky=0.000168179 kz=22.9555 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6927e-09 l2=1.03002e-05 x=4.97342e-05 y=9.57275e-05 z=-5.1507e-06 kx=-0.000119262 ky=-0.000670312 kz=22.621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.31077e-09 l2=4.93226e-06 x=-4.99391e-05 y=3.46233e-05 z=-2.46958e-06 kx=-0.00083902 ky=0.000406731 kz=23.2898 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32951e-09 l2=7.37981e-06 x=4.98637e-05 y=7.24678e-05 z=-3.69217e-06 kx=0.000510341 ky=0.00110907 kz=23.0518 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43782e-09 l2=1.01133e-05 x=4.97437e-05 y=0.000333786 z=-5.059e-06 kx=0.000511229 ky=0.00165051 kz=22.9693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1084e-09 l2=3.38702e-05 x=-4.70444e-05 y=0.000178865 z=-1.69369e-05 kx=-0.00061259 ky=0.00152417 kz=22.6689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.32309e-09 l2=8.32932e-06 x=-4.98264e-05 y=-0.000299773 z=-4.16495e-06 kx=0.000406699 ky=-0.00160989 kz=23.2562 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29254e-09 l2=1.76573e-05 x=-4.92147e-05 y=0.000238059 z=-8.82811e-06 kx=0.000547118 ky=0.000725112 kz=22.9353 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.036e-09 l2=1.88124e-05 x=4.91077e-05 y=-0.000170834 z=-9.40516e-06 kx=-0.000706907 ky=0.000135093 kz=22.4034 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18894e-09 l2=1.59686e-05 x=-4.93586e-05 y=0.000230866 z=-7.98431e-06 kx=0.000276387 ky=-0.000369383 kz=23.0679 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37909e-09 l2=1.93955e-05 x=-4.90504e-05 y=0.000165512 z=-9.69976e-06 kx=-0.000612722 ky=0.00147864 kz=22.7215 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0451e-09 l2=3.93533e-05 x=-4.59662e-05 y=-0.000122965 z=-1.96761e-05 kx=0.000550469 ky=0.000733897 kz=23.2883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13208e-09 l2=3.24655e-05 x=4.72916e-05 y=-0.000341329 z=-1.6234e-05 kx=0.000343948 ky=-0.000100582 kz=23.1136 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26395e-09 l2=1.60562e-05 x=4.93509e-05 y=-0.00043061 z=-8.03144e-06 kx=0.0012662 ky=-0.000400474 kz=23.2571 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40102e-09 l2=1.696e-05 x=4.92756e-05 y=-8.35016e-05 z=-8.48146e-06 kx=0.00034003 ky=0.000538021 kz=22.4904 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35491e-09 l2=2.09143e-05 x=4.88939e-05 y=0.000231713 z=-1.04603e-05 kx=0.00114689 ky=6.86324e-06 kz=22.7346 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26639e-09 l2=2.86076e-05 x=4.79101e-05 y=-0.000369067 z=-1.43059e-05 kx=0.000708764 ky=-0.00123621 kz=22.9979 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25436e-09 l2=1.64056e-05 x=4.93223e-05 y=-0.000489644 z=-8.20654e-06 kx=0.00119144 ky=-0.000510496 kz=22.6676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16283e-09 l2=1.97103e-05 x=4.90196e-05 y=0.000474029 z=-9.85423e-06 kx=-0.000712184 ky=0.00209754 kz=22.8296 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59324e-09 l2=1.39328e-05 x=4.95122e-05 y=-0.000428554 z=-6.96853e-06 kx=0.000614191 ky=-0.000833883 kz=22.8127 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13187e-09 l2=1.48108e-05 x=4.94488e-05 y=0.000499991 z=-7.40513e-06 kx=-0.000398796 ky=0.000514016 kz=23.1013 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28729e-09 l2=1.68098e-05 x=-4.92889e-05 y=-1.99361e-05 z=-8.40407e-06 kx=0.000679158 ky=0.000218147 kz=23.0295 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43701e-09 l2=1.28106e-05 x=-4.95881e-05 y=-6.92034e-05 z=-6.406e-06 kx=1.16573e-05 ky=0.000291288 kz=22.4988 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04963e-09 l2=3.96372e-05 x=-4.59048e-05 y=0.000497323 z=-1.98189e-05 kx=9.80764e-05 ky=0.00157062 kz=22.8593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52598e-09 l2=1.02125e-05 x=4.97386e-05 y=-0.00035708 z=-5.1076e-06 kx=0.000272718 ky=0.000227768 kz=23.1374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07047e-09 l2=2.13025e-05 x=-4.88524e-05 y=0.000338791 z=-1.0652e-05 kx=-7.19146e-05 ky=0.000142233 kz=22.6386 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18337e-09 l2=3.46165e-05 x=-4.69084e-05 y=0.000191479 z=-1.73101e-05 kx=-0.000625172 ky=0.000659309 kz=23.3077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.43138e-09 l2=1.69979e-06 x=-4.99928e-05 y=4.28266e-05 z=-8.53427e-07 kx=-0.00104972 ky=0.000339585 kz=22.6332 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=9.0955e-09 l2=2.25903e-06 x=-4.99873e-05 y=0.000231582 z=-1.13652e-06 kx=-0.00112217 ky=-0.000449652 kz=22.814 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62431e-09 l2=7.85816e-06 x=4.98455e-05 y=-0.000122026 z=-3.93056e-06 kx=7.67652e-05 ky=-0.00122998 kz=22.5225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10101e-09 l2=1.69423e-05 x=4.92768e-05 y=-0.000455585 z=-8.47434e-06 kx=0.00119669 ky=-0.00023627 kz=22.3834 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42053e-09 l2=1.1435e-05 x=-4.96719e-05 y=0.000413059 z=-5.71962e-06 kx=-0.000653123 ky=-0.000185003 kz=23.1432 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05275e-09 l2=2.62921e-05 x=-4.82411e-05 y=-7.39801e-05 z=-1.31462e-05 kx=0.000185565 ky=-0.000716807 kz=22.3051 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27012e-09 l2=1.73898e-05 x=4.92383e-05 y=0.000245009 z=-8.69538e-06 kx=-8.50155e-05 ky=0.0013693 kz=22.9299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03137e-09 l2=6.96537e-06 x=4.98785e-05 y=-5.56186e-05 z=-3.48609e-06 kx=0.0010892 ky=-0.000749185 kz=22.7067 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05169e-09 l2=1.719e-05 x=-4.92558e-05 y=-0.000171361 z=-8.59535e-06 kx=7.21551e-05 ky=0.000335614 kz=22.4986 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.57185e-09 l2=8.58873e-06 x=-4.98154e-05 y=-0.00034387 z=-4.29695e-06 kx=-0.000139878 ky=8.45188e-05 kz=23.058 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35047e-09 l2=1.84262e-05 x=4.91438e-05 y=-0.000257215 z=-9.21482e-06 kx=0.000482529 ky=-0.000293678 kz=22.6693 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04214e-09 l2=2.11729e-05 x=4.88667e-05 y=0.000146594 z=-1.05864e-05 kx=-0.000246778 ky=0.000222801 kz=23.0225 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67358e-09 l2=1.14929e-05 x=-4.96688e-05 y=-0.000123836 z=-5.74681e-06 kx=0.00023067 ky=0.00051963 kz=22.7517 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68515e-09 l2=1.62823e-05 x=4.93327e-05 y=0.000295522 z=-8.14296e-06 kx=0.000448057 ky=0.000482382 kz=22.9217 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0754e-09 l2=1.01128e-05 x=-4.97437e-05 y=5.60761e-05 z=-5.05746e-06 kx=-0.00025209 ky=-0.000498622 kz=22.7747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28369e-09 l2=1.05723e-05 x=-4.97196e-05 y=0.000342875 z=-5.28915e-06 kx=-0.00109345 ky=-0.00033597 kz=22.8689 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26773e-09 l2=2.64108e-05 x=4.82245e-05 y=-8.12778e-05 z=-1.32072e-05 kx=0.000551224 ky=-0.000660795 kz=22.6741 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29853e-09 l2=1.74023e-05 x=4.92376e-05 y=0.000176866 z=-8.69967e-06 kx=-0.00101192 ky=0.00142776 kz=23.3084 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30292e-09 l2=1.44852e-05 x=-4.9473e-05 y=0.000414524 z=-7.24154e-06 kx=0.000782685 ky=0.00107269 kz=22.6033 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.13593e-09 l2=1.08392e-05 x=-4.97054e-05 y=-5.19818e-05 z=-5.42199e-06 kx=-0.000606245 ky=-0.000648434 kz=22.4314 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43202e-09 l2=2.86052e-05 x=-4.79106e-05 y=0.000187052 z=-1.43044e-05 kx=-0.000529789 ky=0.00105237 kz=23.0808 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74128e-09 l2=1.11036e-05 x=-4.96912e-05 y=6.15999e-05 z=-5.55043e-06 kx=0.00103493 ky=0.000379997 kz=23.0889 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06672e-09 l2=8.40603e-06 x=-4.9823e-05 y=-0.000104731 z=-4.20489e-06 kx=-0.000610378 ky=0.000135941 kz=22.5782 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.90326e-09 l2=1.22623e-05 x=4.96228e-05 y=0.000158657 z=-6.13182e-06 kx=-0.000128393 ky=0.000929096 kz=22.6699 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45018e-09 l2=5.84037e-06 x=4.99146e-05 y=-0.000171896 z=-2.92267e-06 kx=0.000790572 ky=-0.000111275 kz=22.4502 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00443e-09 l2=2.20321e-05 x=4.8771e-05 y=-0.000203349 z=-1.10185e-05 kx=0.00091324 ky=-0.000750058 kz=22.3324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01827e-09 l2=1.29975e-05 x=4.95757e-05 y=0.000192605 z=-6.50082e-06 kx=0.000721935 ky=0.000649094 kz=22.5573 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08403e-09 l2=2.6391e-05 x=-4.82274e-05 y=0.000302518 z=-1.31964e-05 kx=-0.000159843 ky=0.000470003 kz=23.0893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57266e-09 l2=1.8776e-05 x=4.91111e-05 y=0.000186851 z=-9.38784e-06 kx=-0.000446286 ky=0.000776867 kz=23.0968 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30866e-09 l2=1.32162e-05 x=-4.95612e-05 y=0.000396725 z=-6.61129e-06 kx=-0.00116309 ky=0.00170447 kz=22.7031 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.66524e-09 l2=3.79127e-06 x=-4.99642e-05 y=0.000276537 z=-1.89972e-06 kx=-0.000349181 ky=0.00141441 kz=23.2972 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.06435e-09 l2=9.89595e-06 x=-4.97545e-05 y=6.99491e-05 z=-4.94991e-06 kx=-0.000649043 ky=0.00112853 kz=23.1071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52538e-09 l2=1.09846e-05 x=-4.96973e-05 y=-0.000117812 z=-5.49491e-06 kx=-0.000842537 ky=-0.000987636 kz=22.5992 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.69495e-09 l2=3.20755e-06 x=-4.99743e-05 y=0.000345737 z=-1.60721e-06 kx=-0.000498731 ky=0.00177679 kz=22.9661 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11575e-09 l2=1.5474e-05 x=-4.93976e-05 y=-0.000245029 z=-7.73907e-06 kx=-0.000700481 ky=-0.00128046 kz=22.9104 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.67007e-09 l2=1.82437e-06 x=-4.99917e-05 y=-0.000267424 z=-9.15525e-07 kx=-0.000230821 ky=-0.00162843 kz=22.8344 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28189e-09 l2=2.39597e-05 x=-4.85438e-05 y=-2.24894e-06 z=-1.19805e-05 kx=8.29675e-07 ky=0.000513061 kz=23.1969 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02057e-09 l2=2.63439e-05 x=4.8234e-05 y=0.000426305 z=-1.31721e-05 kx=-0.000156292 ky=0.00183147 kz=23.3076 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81775e-09 l2=2.147e-05 x=4.88339e-05 y=-0.000446321 z=-1.07374e-05 kx=0.00068489 ky=-0.00195732 kz=22.9698 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80598e-09 l2=1.85468e-05 x=-4.91329e-05 y=0.000144575 z=-9.27314e-06 kx=0.000549603 ky=-0.00056187 kz=22.7846 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20638e-09 l2=3.06727e-05 x=4.75906e-05 y=0.000445722 z=-1.53354e-05 kx=-0.00072352 ky=0.0019982 kz=22.705 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08384e-09 l2=2.5648e-05 x=-4.83278e-05 y=-0.000436041 z=-1.2824e-05 kx=0.000244555 ky=-0.000261057 kz=23.2357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.12159e-09 l2=1.36405e-05 x=4.95327e-05 y=0.000362412 z=-6.82223e-06 kx=0.000437429 ky=0.000405407 kz=23.2872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29684e-09 l2=7.98407e-06 x=4.98404e-05 y=6.78574e-05 z=-3.99324e-06 kx=0.000253363 ky=0.00062088 kz=22.5488 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16852e-09 l2=2.70662e-05 x=-4.81341e-05 y=0.000460783 z=-1.35331e-05 kx=0.000303044 ky=0.000107931 kz=23.1688 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.27222e-09 l2=1.24865e-05 x=-4.96091e-05 y=-0.000421231 z=-6.24228e-06 kx=0.000960204 ky=-0.00144682 kz=22.7556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15016e-09 l2=2.83958e-05 x=4.79424e-05 y=0.000247554 z=-1.4197e-05 kx=-0.000721503 ky=0.000117909 kz=22.952 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03596e-09 l2=1.99065e-05 x=4.89995e-05 y=0.000123294 z=-9.95339e-06 kx=-0.000164471 ky=0.000956978 kz=22.5316 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35857e-09 l2=1.12901e-05 x=4.96804e-05 y=-0.000359419 z=-5.64561e-06 kx=-5.95326e-05 ky=-0.000614568 kz=22.6881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47374e-09 l2=2.72091e-05 x=-4.81141e-05 y=0.000348472 z=-1.36041e-05 kx=0.000561339 ky=0.000930856 kz=22.868 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22851e-09 l2=2.3042e-05 x=-4.86551e-05 y=0.000149285 z=-1.15199e-05 kx=0.000799965 ky=-0.000132044 kz=23.1881 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.67433e-09 l2=8.061e-06 x=-4.98372e-05 y=0.000252268 z=-4.03401e-06 kx=-0.000971061 ky=0.000300264 kz=22.2997 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32422e-09 l2=9.057e-06 x=-4.97947e-05 y=-0.00023076 z=-4.52782e-06 kx=0.000605662 ky=-0.000916941 kz=22.5607 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.16251e-09 l2=2.84948e-06 x=-4.99798e-05 y=8.31171e-05 z=-1.42704e-06 kx=-0.00010099 ky=-0.000953693 kz=23.0765 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27266e-09 l2=2.08747e-05 x=4.88983e-05 y=-0.000489951 z=-1.04393e-05 kx=0.000590548 ky=-0.00023149 kz=22.9791 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02481e-09 l2=2.3165e-05 x=4.86404e-05 y=-0.000326381 z=-1.15818e-05 kx=-0.000572118 ky=-0.00109148 kz=23.3003 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57097e-09 l2=7.85362e-06 x=4.98455e-05 y=0.00022192 z=-3.92975e-06 kx=0.000989175 ky=0.000541527 kz=22.8503 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07748e-09 l2=1.93578e-05 x=4.9054e-05 y=0.0001016 z=-9.68146e-06 kx=0.000928519 ky=0.000457449 kz=22.6395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98758e-09 l2=1.40179e-05 x=4.95065e-05 y=3.14615e-05 z=-7.00925e-06 kx=-0.000313818 ky=0.00104209 kz=22.5886 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51428e-09 l2=7.81996e-06 x=4.98468e-05 y=0.000133832 z=-3.91271e-06 kx=0.000898489 ky=0.00120147 kz=22.6882 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20719e-09 l2=1.87722e-05 x=4.91116e-05 y=0.000320018 z=-9.38473e-06 kx=-0.000928847 ky=0.000303913 kz=22.9261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62774e-09 l2=1.55139e-05 x=4.93946e-05 y=0.000392214 z=-7.75854e-06 kx=0.000358766 ky=0.000663866 kz=23.0404 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20812e-09 l2=2.67264e-05 x=-4.81814e-05 y=0.000149162 z=-1.33634e-05 kx=0.000193138 ky=4.97963e-05 kz=23.0358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43055e-09 l2=1.80648e-05 x=4.91771e-05 y=0.000415028 z=-9.03519e-06 kx=0.000951836 ky=0.000886412 kz=22.771 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24663e-09 l2=1.83576e-05 x=4.91506e-05 y=-0.000305141 z=-9.17852e-06 kx=-0.000422605 ky=-0.000298279 kz=22.7845 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.62633e-09 l2=1.42862e-05 x=4.94876e-05 y=-0.000381823 z=-7.1428e-06 kx=-0.000755305 ky=-0.00201332 kz=23.2801 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18024e-09 l2=2.38009e-05 x=-4.85628e-05 y=6.05186e-05 z=-1.19032e-05 kx=-0.00105289 ky=-0.000676829 kz=23.1275 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.61602e-09 l2=8.51715e-06 x=4.98182e-05 y=0.000375758 z=-4.26184e-06 kx=0.00112139 ky=0.000714766 kz=22.7454 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.30825e-09 l2=9.93391e-06 x=4.9753e-05 y=-0.000231364 z=-4.96729e-06 kx=-0.000591629 ky=0.000149724 kz=22.3377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40274e-09 l2=1.56951e-05 x=-4.93804e-05 y=-0.000314443 z=-7.84833e-06 kx=-3.78408e-05 ky=-0.00141189 kz=23.0685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.08051e-09 l2=1.25769e-05 x=-4.96031e-05 y=0.000236838 z=-6.28961e-06 kx=-6.35483e-05 ky=-0.000555628 kz=22.8071 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57568e-09 l2=1.52676e-05 x=4.94142e-05 y=-0.000492124 z=-7.63307e-06 kx=-0.000707381 ky=-0.00172008 kz=22.6754 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.25444e-09 l2=2.19862e-05 x=-4.87771e-05 y=-0.00025009 z=-1.09928e-05 kx=0.000692333 ky=-0.000332187 kz=22.7723 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88981e-09 l2=7.58346e-06 x=-4.98562e-05 y=0.00014742 z=-3.79064e-06 kx=0.000909894 ky=0.00118213 kz=22.3212 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47733e-09 l2=1.58189e-05 x=-4.93707e-05 y=0.000108246 z=-7.90949e-06 kx=0.00032271 ky=-0.00056163 kz=22.4259 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.63385e-09 l2=1.67028e-05 x=4.92974e-05 y=-0.000329543 z=-8.35424e-06 kx=0.000957604 ky=3.55733e-05 kz=23.0818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01534e-09 l2=1.85353e-05 x=-4.91335e-05 y=-0.000491461 z=-9.26936e-06 kx=-0.000566793 ky=-0.000282974 kz=23.1372 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41872e-09 l2=2.35017e-05 x=-4.86001e-05 y=0.000329908 z=-1.175e-05 kx=0.000705637 ky=0.000120088 kz=22.6253 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.01188e-09 l2=7.13936e-06 x=-4.98723e-05 y=1.52018e-05 z=-3.57358e-06 kx=-0.00111321 ky=-0.000522333 kz=23.207 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01249e-09 l2=9.48096e-06 x=-4.97747e-05 y=-0.000377339 z=-4.74198e-06 kx=-0.000457927 ky=-0.000380646 kz=22.8291 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64138e-09 l2=1.55678e-05 x=-4.93908e-05 y=-0.00036174 z=-7.7832e-06 kx=0.000701754 ky=-0.00100348 kz=22.9057 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49629e-09 l2=1.70414e-05 x=4.92688e-05 y=0.000278752 z=-8.52107e-06 kx=-0.000170121 ky=0.000104267 kz=22.412 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14569e-09 l2=3.34806e-05 x=4.71145e-05 y=0.000308712 z=-1.67411e-05 kx=9.65783e-05 ky=0.00107471 kz=22.9847 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.45843e-09 l2=5.72208e-06 x=4.99182e-05 y=0.000419408 z=-2.86112e-06 kx=-0.000293718 ky=0.00164127 kz=22.6608 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.47268e-09 l2=1.95749e-05 x=4.90323e-05 y=0.00019961 z=-9.79074e-06 kx=0.00118484 ky=-8.42695e-05 kz=22.7547 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.12512e-09 l2=4.71701e-06 x=-4.99445e-05 y=-0.000296077 z=-2.35721e-06 kx=0.000862002 ky=-0.000921859 kz=23.1525 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40572e-09 l2=2.50238e-05 x=-4.84097e-05 y=-0.000106131 z=-1.25113e-05 kx=0.000644588 ky=-0.000719307 kz=23.0261 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0138e-09 l2=1.52297e-05 x=-4.94171e-05 y=2.58634e-05 z=-7.6132e-06 kx=0.00102006 ky=0.000641582 kz=23.1862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.67097e-09 l2=1.55641e-05 x=4.93909e-05 y=-0.000401761 z=-7.7825e-06 kx=-0.000179059 ky=-0.000464352 kz=23.0496 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17674e-09 l2=1.94913e-05 x=4.90412e-05 y=-1.22255e-05 z=-9.74593e-06 kx=-0.000138084 ky=0.000195295 kz=22.6422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11491e-09 l2=9.21499e-06 x=-4.97874e-05 y=-0.000474387 z=-4.60662e-06 kx=0.000642535 ky=-0.000799886 kz=22.3591 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07164e-09 l2=1.30515e-05 x=-4.95724e-05 y=-0.000417309 z=-6.52652e-06 kx=-0.000107502 ky=-0.00153336 kz=22.5965 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.42831e-09 l2=3.15331e-05 x=4.74497e-05 y=-9.6748e-05 z=-1.5766e-05 kx=-0.000613901 ky=-0.000573307 kz=22.8038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07048e-09 l2=2.36701e-05 x=-4.85788e-05 y=-0.000456098 z=-1.18375e-05 kx=-0.000881641 ky=-9.13811e-05 kz=22.9178 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.3183e-09 l2=6.7044e-06 x=4.98875e-05 y=-0.000392216 z=-3.3541e-06 kx=0.000343916 ky=-0.00117634 kz=23.0762 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00131e-09 l2=1.32035e-05 x=4.95625e-05 y=-0.00022127 z=-6.60116e-06 kx=-0.000490968 ky=-0.000820485 kz=22.5449 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24667e-09 l2=1.86806e-05 x=4.91203e-05 y=-1.26607e-05 z=-9.33925e-06 kx=-0.000779985 ky=0.000471012 kz=22.9896 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77544e-09 l2=8.59072e-06 x=4.9815e-05 y=-0.00015999 z=-4.29854e-06 kx=0.00103104 ky=-0.000703988 kz=22.4099 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.74586e-09 l2=9.2815e-06 x=-4.97843e-05 y=0.000147108 z=-4.6413e-06 kx=0.000147628 ky=0.00130606 kz=22.6045 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24006e-09 l2=3.26048e-05 x=4.72671e-05 y=0.000447317 z=-1.63054e-05 kx=0.00117082 ky=0.00189762 kz=23.0522 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04643e-09 l2=1.50067e-05 x=-4.94336e-05 y=4.01127e-05 z=-7.50555e-06 kx=-0.000772356 ky=0.000684735 kz=23.1542 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33028e-09 l2=8.36149e-06 x=4.98251e-05 y=-0.000334163 z=-4.17962e-06 kx=-0.000804866 ky=-0.00034014 kz=22.4396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.43025e-09 l2=2.57308e-05 x=4.83161e-05 y=5.62559e-05 z=-1.28682e-05 kx=0.000994549 ky=-0.000371428 kz=22.9767 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17888e-09 l2=1.94458e-06 x=-4.99906e-05 y=0.000439451 z=-9.71438e-07 kx=0.000866775 ky=0.00138773 kz=22.3419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01517e-09 l2=1.4809e-05 x=-4.9449e-05 y=7.16707e-06 z=-7.40326e-06 kx=0.000809053 ky=0.000826463 kz=22.8677 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08549e-09 l2=2.55552e-05 x=-4.83398e-05 y=0.000426913 z=-1.27786e-05 kx=-0.000223079 ky=-6.73363e-05 kz=22.6345 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.09644e-09 l2=9.0309e-06 x=-4.97959e-05 y=0.000339252 z=-4.51537e-06 kx=0.000525849 ky=0.000892636 kz=23.2384 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20181e-09 l2=2.6493e-05 x=-4.8214e-05 y=-0.000122006 z=-1.32454e-05 kx=0.000797594 ky=-0.000939488 kz=22.3419 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.22941e-09 l2=1.73327e-05 x=-4.92434e-05 y=-0.000257785 z=-8.66654e-06 kx=0.000187412 ky=-0.00071691 kz=22.3044 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.17621e-09 l2=7.73276e-06 x=-4.98505e-05 y=-0.000161381 z=-3.86638e-06 kx=0.000500916 ky=-0.00063361 kz=23.0161 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.40811e-09 l2=1.97453e-05 x=-4.90153e-05 y=0.000210034 z=-9.87577e-06 kx=-0.00109798 ky=-4.59392e-05 kz=22.3673 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64981e-09 l2=1.83117e-05 x=-4.91547e-05 y=0.000490714 z=-9.15679e-06 kx=-6.2033e-05 ky=2.5946e-05 kz=22.367 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53779e-09 l2=1.67756e-05 x=-4.92917e-05 y=0.000120795 z=-8.38777e-06 kx=0.000379064 ky=0.000883219 kz=22.9884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04001e-09 l2=1.60931e-05 x=-4.93483e-05 y=1.90525e-05 z=-8.04743e-06 kx=-0.000156829 ky=0.000838253 kz=23.2089 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08706e-09 l2=2.1083e-05 x=4.88762e-05 y=-0.000373061 z=-1.05425e-05 kx=0.000221175 ky=-0.0013434 kz=22.9671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11085e-09 l2=2.52256e-05 x=4.83827e-05 y=-4.44237e-05 z=-1.26151e-05 kx=0.000828791 ky=-3.23316e-05 kz=22.9162 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03685e-09 l2=3.12914e-05 x=4.74887e-05 y=-0.000340846 z=-1.56478e-05 kx=0.000784829 ky=-0.00035304 kz=22.9324 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.8564e-09 l2=1.21055e-05 x=-4.96327e-05 y=-9.93948e-05 z=-6.0525e-06 kx=0.000773729 ky=-0.000394382 kz=22.9747 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10887e-09 l2=2.55712e-05 x=-4.83374e-05 y=0.000102326 z=-1.27877e-05 kx=-0.000718786 ky=0.000324444 kz=23.2116 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49644e-09 l2=1.08381e-05 x=4.97055e-05 y=0.000172332 z=-5.42017e-06 kx=0.000179733 ky=0.00145612 kz=22.7039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=8.26841e-09 l2=2.84388e-06 x=4.99798e-05 y=-0.000347291 z=-1.42824e-06 kx=0.00100789 ky=-0.000166245 kz=23.2429 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.70699e-09 l2=3.22493e-06 x=4.99742e-05 y=0.000187757 z=-1.61425e-06 kx=-0.000704759 ky=-0.000490651 kz=22.459 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01197e-09 l2=2.24708e-05 x=4.87209e-05 y=7.59976e-05 z=-1.1238e-05 kx=0.000953658 ky=-0.000425192 kz=22.3883 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07521e-09 l2=1.20111e-05 x=4.96379e-05 y=0.000411288 z=-6.00793e-06 kx=0.00083671 ky=0.00129357 kz=22.4825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04183e-09 l2=1.37422e-05 x=4.95256e-05 y=0.00027088 z=-6.87213e-06 kx=0.000241728 ky=0.000689858 kz=23.2695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.35521e-09 l2=1.24019e-05 x=4.96139e-05 y=-0.00031718 z=-6.20413e-06 kx=0.000905348 ky=-0.000108094 kz=22.3548 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29567e-09 l2=3.29428e-05 x=4.72087e-05 y=-0.000124544 z=-1.64738e-05 kx=0.000829044 ky=-0.00143358 kz=23.0198 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41395e-09 l2=1.61925e-05 x=4.93404e-05 y=-0.000471448 z=-8.09623e-06 kx=-0.000323628 ky=-0.000564302 kz=22.3649 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11539e-09 l2=2.05456e-05 x=4.89333e-05 y=-0.000366382 z=-1.02739e-05 kx=0.000240689 ky=2.21992e-05 kz=22.4962 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16461e-09 l2=2.56802e-05 x=4.83232e-05 y=0.000298417 z=-1.28412e-05 kx=0.000222641 ky=0.000626053 kz=22.7639 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.22465e-09 l2=8.54113e-06 x=-4.98172e-05 y=-0.000191653 z=-4.27465e-06 kx=-0.00114644 ky=0.000326732 kz=23.0781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73344e-09 l2=1.40985e-05 x=-4.95004e-05 y=-4.63071e-05 z=-7.05238e-06 kx=-0.0010426 ky=-0.000551324 kz=23.023 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03915e-09 l2=3.19295e-05 x=-4.73822e-05 y=-0.000482731 z=-1.59676e-05 kx=-0.00111345 ky=-0.000620881 kz=22.961 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.33722e-09 l2=5.51957e-06 x=-4.9924e-05 y=1.16718e-05 z=-2.76059e-06 kx=0.000840866 ky=0.000313494 kz=22.6065 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50114e-09 l2=2.0642e-05 x=4.89234e-05 y=-0.000150828 z=-1.03215e-05 kx=-0.000130374 ky=-0.000991638 kz=22.8482 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.18537e-09 l2=2.11666e-05 x=-4.88674e-05 y=0.000412618 z=-1.05833e-05 kx=0.000289887 ky=0.001038 kz=23.2523 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.90812e-09 l2=8.91094e-06 x=4.98013e-05 y=0.000479128 z=-4.45579e-06 kx=-0.000525413 ky=0.00213486 kz=23.1569 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20033e-09 l2=1.65707e-05 x=4.93091e-05 y=7.39502e-05 z=-8.28462e-06 kx=-0.000626171 ky=0.000571247 kz=23.2025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24949e-09 l2=1.05053e-05 x=-4.97232e-05 y=-6.12146e-05 z=-5.25502e-06 kx=-0.000821267 ky=-0.000492877 kz=23.186 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03573e-09 l2=4.52993e-05 x=-4.4575e-05 y=0.00013584 z=-2.26521e-05 kx=-0.00101875 ky=0.00105013 kz=22.9991 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32685e-09 l2=8.80397e-06 x=-4.98061e-05 y=-0.000462541 z=-4.40088e-06 kx=0.000814477 ky=9.45306e-06 kz=22.957 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14819e-09 l2=7.37273e-06 x=4.98639e-05 y=2.53506e-05 z=-3.68742e-06 kx=0.000222235 ky=0.000824954 kz=23.1008 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0584e-09 l2=2.12558e-05 x=4.88578e-05 y=0.000107845 z=-1.06273e-05 kx=-0.000555152 ky=-0.000742558 kz=23.2893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25504e-09 l2=2.77214e-05 x=4.80403e-05 y=3.27201e-05 z=-1.38622e-05 kx=0.000434966 ky=-0.00104329 kz=23.172 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=6.72665e-09 l2=1.77535e-06 x=-4.99922e-05 y=-0.000393377 z=-8.91802e-07 kx=-0.000351023 ky=-0.000375628 kz=23.0548 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35382e-09 l2=2.07431e-05 x=-4.89129e-05 y=-0.00017031 z=-1.03712e-05 kx=0.000491671 ky=-0.00132192 kz=23.0736 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51273e-09 l2=3.0452e-05 x=4.76254e-05 y=-0.000242065 z=-1.52273e-05 kx=0.000260111 ky=-0.0011573 kz=23.0382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.16198e-09 l2=5.95961e-06 x=-4.99112e-05 y=5.64573e-05 z=-2.98048e-06 kx=0.000185365 ky=-0.000967458 kz=22.5318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.95853e-08 l2=9.97264e-07 x=4.99977e-05 y=0.000262978 z=-5.13705e-07 kx=0.000128538 ky=0.000866778 kz=22.9005 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.15041e-09 l2=7.52166e-06 x=-4.98586e-05 y=0.000255169 z=-3.75989e-06 kx=0.000906053 ky=0.000629578 kz=22.4007 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91807e-09 l2=9.08408e-06 x=4.97932e-05 y=-0.000299913 z=-4.54468e-06 kx=0.000784811 ky=-0.00128519 kz=23.1866 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66869e-09 l2=8.42681e-06 x=4.98221e-05 y=-3.43932e-05 z=-4.21582e-06 kx=0.000716743 ky=-0.000976071 kz=22.6026 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.51107e-09 l2=1.40646e-05 x=4.95033e-05 y=-0.000292754 z=-7.03187e-06 kx=-0.000535856 ky=-0.00128364 kz=22.4358 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.30015e-09 l2=1.89481e-05 x=-4.90939e-05 y=-0.000321637 z=-9.47692e-06 kx=-0.00102753 ky=-0.00108842 kz=22.8307 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.86321e-09 l2=1.08258e-05 x=4.97064e-05 y=-0.000443701 z=-5.41222e-06 kx=-0.000738022 ky=-0.000654776 kz=22.4319 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.76714e-09 l2=9.04281e-06 x=4.97954e-05 y=0.000429221 z=-4.52081e-06 kx=-0.000684007 ky=-0.000132129 kz=22.9621 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.99714e-09 l2=1.75652e-05 x=-4.92226e-05 y=0.000328175 z=-8.78493e-06 kx=-0.00061083 ky=0.000455011 kz=22.4998 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44075e-09 l2=1.33995e-05 x=4.95489e-05 y=0.000148133 z=-6.70288e-06 kx=0.00109818 ky=-0.000318088 kz=22.6871 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0283e-09 l2=1.82158e-05 x=4.91632e-05 y=7.57675e-05 z=-9.11039e-06 kx=0.000927524 ky=-0.000937834 kz=22.8971 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.39153e-09 l2=1.39544e-05 x=4.95109e-05 y=0.000315965 z=-6.979e-06 kx=0.000279614 ky=0.0013152 kz=22.9656 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03656e-09 l2=3.24415e-05 x=-4.7296e-05 y=-0.000380379 z=-1.62211e-05 kx=9.64271e-05 ky=-0.000928035 kz=22.5784 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70712e-09 l2=2.03711e-05 x=-4.89514e-05 y=-0.000393808 z=-1.01881e-05 kx=-0.000795815 ky=-0.000942762 kz=22.7377 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5477e-09 l2=2.14148e-05 x=-4.88407e-05 y=0.000162498 z=-1.0706e-05 kx=0.000996418 ky=0.00124994 kz=22.6794 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07541e-09 l2=2.69343e-05 x=-4.81523e-05 y=-7.28969e-05 z=-1.34678e-05 kx=-3.54118e-05 ky=-0.000326042 kz=23.0294 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.12644e-09 l2=7.20778e-06 x=-4.98701e-05 y=0.000496114 z=-3.60486e-06 kx=0.000272943 ky=0.000236204 kz=22.9255 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.84986e-09 l2=3.54587e-06 x=-4.99685e-05 y=-0.000333632 z=-1.77685e-06 kx=-0.00112668 ky=-0.000260438 kz=22.5996 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01199e-09 l2=2.42044e-05 x=4.85127e-05 y=-0.000282706 z=-1.21054e-05 kx=0.00122223 ky=-0.00124314 kz=22.402 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3159e-09 l2=3.83331e-06 x=4.99633e-05 y=0.00049437 z=-1.91701e-06 kx=-0.000136847 ky=0.000288292 kz=22.7721 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04398e-09 l2=1.19377e-05 x=4.96427e-05 y=0.000393003 z=-5.9677e-06 kx=-0.000759912 ky=0.00122766 kz=22.7064 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.00497e-09 l2=7.63461e-06 x=4.98544e-05 y=0.000462322 z=-3.81815e-06 kx=-0.000767943 ky=0.000683994 kz=23.153 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.57721e-09 l2=4.7706e-06 x=4.99432e-05 y=0.000100045 z=-2.38517e-06 kx=-0.000652711 ky=0.000454252 kz=22.9133 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.36335e-09 l2=1.43541e-05 x=4.94826e-05 y=0.000114668 z=-7.1759e-06 kx=-0.000849469 ky=0.00121444 kz=22.7631 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.29752e-09 l2=3.3631e-05 x=4.70885e-05 y=-0.000122154 z=-1.68143e-05 kx=-0.000892065 ky=0.000616259 kz=22.7436 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.68007e-09 l2=1.60916e-05 x=-4.93486e-05 y=-0.000492611 z=-8.0463e-06 kx=0.000152791 ky=-0.000262525 kz=22.7802 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.44361e-09 l2=1.09745e-05 x=-4.9698e-05 y=-0.000274722 z=-5.48919e-06 kx=-0.000326643 ky=-0.00115667 kz=22.4197 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.03255e-09 l2=1.86981e-05 x=-4.91184e-05 y=-0.000200436 z=-9.34881e-06 kx=0.000349997 ky=-0.00120779 kz=23.0299 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.03423e-09 l2=5.63052e-06 x=-4.99207e-05 y=0.000353844 z=-2.8189e-06 kx=-0.000731801 ky=1.41408e-05 kz=22.556 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.79631e-09 l2=1.03682e-05 x=-4.97305e-05 y=-0.000403399 z=-5.18651e-06 kx=-0.000698649 ky=-0.00136144 kz=23.1896 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72006e-09 l2=1.05843e-05 x=-4.97193e-05 y=0.000489597 z=-5.29202e-06 kx=0.000455951 ky=0.000932631 kz=22.3534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02594e-09 l2=3.3522e-05 x=4.71073e-05 y=0.000245761 z=-1.67611e-05 kx=-0.000203347 ky=0.000660181 kz=22.5678 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.44066e-09 l2=2.17374e-05 x=4.8805e-05 y=-0.000161355 z=-1.08675e-05 kx=-0.000881667 ky=0.000100194 kz=22.6578 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25272e-09 l2=1.39473e-05 x=-4.95113e-05 y=-0.000173001 z=-6.97511e-06 kx=-0.000375693 ky=0.000502506 kz=22.6711 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.58643e-09 l2=3.54999e-06 x=-4.99686e-05 y=-0.000291057 z=-1.77503e-06 kx=0.000563713 ky=0.000454567 kz=22.4213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24708e-09 l2=1.7524e-05 x=4.92263e-05 y=0.000456525 z=-8.76344e-06 kx=0.000378991 ky=0.00114451 kz=22.7107 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.30336e-09 l2=9.08927e-06 x=-4.9793e-05 y=0.000444002 z=-4.54789e-06 kx=-0.000748991 ky=0.00211247 kz=23.3062 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.60239e-09 l2=1.12592e-05 x=4.96823e-05 y=-8.97587e-05 z=-5.6301e-06 kx=-0.000369579 ky=-0.000382355 kz=23.306 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00363e-09 l2=2.1252e-05 x=-4.88575e-05 y=0.000142641 z=-1.06284e-05 kx=-0.000874779 ky=0.00114155 kz=22.9382 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.98079e-09 l2=1.23793e-05 x=-4.96152e-05 y=0.00042632 z=-6.19303e-06 kx=-0.00112173 ky=0.00160213 kz=23.0892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5879e-09 l2=7.17413e-06 x=-4.98713e-05 y=0.000224657 z=-3.58853e-06 kx=0.000152082 ky=0.00154168 kz=22.8096 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00466e-09 l2=1.82624e-05 x=4.9159e-05 y=9.16435e-05 z=-9.13285e-06 kx=0.000532358 ky=-0.000674617 kz=22.3873 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.28822e-09 l2=4.52863e-06 x=4.99488e-05 y=-9.32509e-05 z=-2.26389e-06 kx=-0.000490069 ky=-0.00111971 kz=22.8459 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16551e-09 l2=1.5678e-05 x=-4.93816e-05 y=-2.48925e-05 z=-7.84068e-06 kx=-0.000515599 ky=-0.000909023 kz=23.2702 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.80882e-09 l2=1.52568e-05 x=-4.94144e-05 y=-7.54625e-05 z=-7.63165e-06 kx=-0.00107124 ky=-0.00125451 kz=22.4475 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21067e-08 l2=2.10194e-06 x=-4.99891e-05 y=-0.000215066 z=-1.05801e-06 kx=-0.000456215 ky=-0.000161464 kz=23.1083 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1827e-09 l2=4.67995e-06 x=-4.99451e-05 y=0.000277414 z=-2.34294e-06 kx=-0.00107451 ky=-0.000206749 kz=22.6422 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.37537e-09 l2=5.70779e-06 x=4.99185e-05 y=-0.00045235 z=-2.85834e-06 kx=0.000813113 ky=-0.000202626 kz=23.1684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.5149e-09 l2=1.63131e-05 x=4.93303e-05 y=-0.000401289 z=-8.15742e-06 kx=5.83423e-05 ky=3.82796e-05 kz=22.5731 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0419e-09 l2=3.10182e-05 x=-4.75344e-05 y=-0.000289663 z=-1.55084e-05 kx=0.000603763 ky=-0.00144652 kz=22.872 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.49298e-09 l2=1.58928e-05 x=4.93648e-05 y=-0.000432644 z=-7.94618e-06 kx=-0.000439786 ky=-0.00170066 kz=22.4786 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26702e-09 l2=1.52325e-05 x=-4.94167e-05 y=-0.000268304 z=-7.61659e-06 kx=0.00014061 ky=-0.00100348 kz=22.7171 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.88986e-09 l2=2.16386e-05 x=4.88155e-05 y=0.000236047 z=-1.08205e-05 kx=0.000130362 ky=3.50138e-05 kz=22.8357 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01916e-09 l2=9.81196e-06 x=4.97586e-05 y=0.000289363 z=-4.90928e-06 kx=0.00106034 ky=0.00111235 kz=23.0352 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03054e-09 l2=1.49012e-05 x=-4.94419e-05 y=0.000281697 z=-7.4517e-06 kx=-2.90289e-05 ky=-0.000229549 kz=23.1077 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32293e-09 l2=3.74896e-06 x=-4.99649e-05 y=-0.000313248 z=-1.8758e-06 kx=-0.000304549 ky=-0.0014237 kz=23.061 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16616e-09 l2=1.74454e-05 x=-4.9233e-05 y=0.000478062 z=-8.72518e-06 kx=-0.000899325 ky=0.00125636 kz=23.2634 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75275e-09 l2=1.36039e-05 x=4.95351e-05 y=7.04588e-06 z=-6.80442e-06 kx=0.000731481 ky=-0.000844099 kz=23.0761 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15024e-09 l2=1.64568e-05 x=4.93181e-05 y=0.00043627 z=-8.23091e-06 kx=0.00088236 ky=0.000841802 kz=22.5487 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.11382e-09 l2=2.45686e-05 x=-4.8467e-05 y=-0.000295058 z=-1.22873e-05 kx=-0.00113339 ky=-0.00134716 kz=22.8691 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.07776e-09 l2=1.38776e-05 x=4.95163e-05 y=0.00045245 z=-6.93884e-06 kx=-0.00022301 ky=0.000408109 kz=22.3838 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64661e-09 l2=9.04631e-06 x=-4.9795e-05 y=9.37551e-05 z=-4.52449e-06 kx=-0.000234834 ky=-0.000463848 kz=22.9457 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.11752e-09 l2=7.17301e-06 x=4.98713e-05 y=0.000341471 z=-3.58681e-06 kx=-0.000336466 ky=0.00128253 kz=22.3927 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0383e-09 l2=2.81209e-05 x=-4.79829e-05 y=0.000284498 z=-1.40597e-05 kx=0.000607888 ky=0.00148361 kz=22.9635 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.52075e-09 l2=1.55023e-06 x=-4.99941e-05 y=-0.000335318 z=-7.76816e-07 kx=0.000936198 ky=-0.000894115 kz=22.7097 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.6604e-09 l2=1.44703e-05 x=4.94739e-05 y=3.40213e-05 z=-7.23549e-06 kx=-0.000234599 ky=3.88971e-05 kz=23.1301 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60434e-09 l2=9.63901e-06 x=4.97671e-05 y=0.000247503 z=-4.82196e-06 kx=0.000772754 ky=0.00045902 kz=23.2213 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.24351e-09 l2=9.61318e-06 x=-4.97683e-05 y=-0.000173351 z=-4.81088e-06 kx=-0.00122114 ky=-0.000503997 kz=22.781 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.78966e-09 l2=1.52586e-05 x=-4.94149e-05 y=-0.000105449 z=-7.62832e-06 kx=0.000867864 ky=-0.000132938 kz=22.749 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.5381e-09 l2=8.54998e-06 x=-4.98171e-05 y=0.000103474 z=-4.27581e-06 kx=0.000432872 ky=0.000654999 kz=22.7318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48522e-09 l2=1.43948e-05 x=-4.94796e-05 y=-0.00022637 z=-7.19634e-06 kx=0.000837089 ky=7.35295e-06 kz=23.1913 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.20919e-09 l2=2.58738e-05 x=-4.8298e-05 y=0.000174503 z=-1.29356e-05 kx=0.000906982 ky=0.000231399 kz=23.2974 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0297e-09 l2=2.04084e-05 x=-4.89475e-05 y=0.000432046 z=-1.02061e-05 kx=-0.000644612 ky=-9.30569e-06 kz=22.9692 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.98017e-08 l2=1.01314e-06 x=4.99976e-05 y=0.000210904 z=-5.23826e-07 kx=0.00108974 ky=0.000545912 kz=23.1329 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.27011e-09 l2=1.03845e-05 x=-4.97295e-05 y=8.40173e-05 z=-5.1951e-06 kx=-0.0010188 ky=-0.000173479 kz=22.8318 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19429e-09 l2=1.32364e-05 x=4.956e-05 y=8.19344e-05 z=-6.61992e-06 kx=0.00052655 ky=-0.000774708 kz=23.1149 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.4723e-09 l2=1.86299e-05 x=-4.91251e-05 y=4.93839e-05 z=-9.31415e-06 kx=0.000711944 ky=-0.000995565 kz=22.5685 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34334e-09 l2=8.11065e-06 x=-4.98354e-05 y=-0.00046937 z=-4.05497e-06 kx=0.000468486 ky=-0.000755893 kz=22.6113 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03736e-09 l2=1.15885e-05 x=-4.96635e-05 y=0.00019331 z=-5.79326e-06 kx=0.000931153 ky=-0.000535089 kz=23.2539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.36985e-09 l2=1.30086e-05 x=-4.95755e-05 y=-0.000329623 z=-6.50527e-06 kx=0.000321705 ky=-0.000992713 kz=22.9722 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.40392e-09 l2=7.10395e-06 x=4.98737e-05 y=0.00016157 z=-3.55575e-06 kx=0.00071658 ky=0.000465938 kz=22.7048 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1527e-09 l2=3.79749e-05 x=-4.62542e-05 y=-0.000116833 z=-1.89892e-05 kx=-0.000624079 ky=-0.00131589 kz=23.3109 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10515e-09 l2=6.18042e-06 x=4.99043e-05 y=-0.0002955 z=-3.09245e-06 kx=0.000754304 ky=-0.00167448 kz=22.3187 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.50109e-09 l2=1.53499e-05 x=4.94074e-05 y=-0.000155691 z=-7.67694e-06 kx=0.000586494 ky=-0.00143778 kz=22.9637 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.65356e-09 l2=4.74555e-06 x=-4.99437e-05 y=0.000452298 z=-2.37754e-06 kx=-0.00112088 ky=0.00141394 kz=22.9119 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13714e-09 l2=2.04243e-05 x=-4.89465e-05 y=0.000142199 z=-1.0211e-05 kx=0.00081581 ky=-0.000473644 kz=22.6776 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.21564e-09 l2=3.50409e-05 x=4.68295e-05 y=-0.000317027 z=-1.75225e-05 kx=0.000702827 ky=-0.00147351 kz=22.6309 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62502e-09 l2=2.80653e-05 x=-4.79903e-05 y=0.000365652 z=-1.40347e-05 kx=-0.000621039 ky=0.00166886 kz=22.9756 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.72006e-09 l2=9.98293e-06 x=-4.97503e-05 y=5.38983e-05 z=-4.99265e-06 kx=-0.000149632 ky=-0.000625983 kz=23.1704 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.81667e-09 l2=2.0634e-05 x=-4.89244e-05 y=0.000377676 z=-1.03169e-05 kx=0.000452352 ky=0.00173688 kz=22.7894 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.53382e-09 l2=2.0996e-05 x=4.88857e-05 y=-0.000215249 z=-1.04985e-05 kx=-0.000115151 ky=0.000227846 kz=22.8389 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01272e-09 l2=2.92666e-05 x=4.78103e-05 y=0.00020477 z=-1.46357e-05 kx=0.00088497 ky=-0.000322581 kz=22.8676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.19196e-09 l2=1.49096e-05 x=4.94409e-05 y=-0.000428108 z=-7.4578e-06 kx=0.0010837 ky=-0.000648516 kz=22.35 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.24444e-09 l2=1.1207e-05 x=4.96849e-05 y=-0.000494553 z=-5.60701e-06 kx=0.00109012 ky=-0.000889439 kz=22.61 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75125e-09 l2=6.22761e-06 x=4.99031e-05 y=-0.000321736 z=-3.11366e-06 kx=-0.000690584 ky=-0.0012259 kz=22.6128 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.26111e-09 l2=7.16644e-06 x=-4.98715e-05 y=-0.00033374 z=-3.58717e-06 kx=-0.00059957 ky=-0.000898246 kz=22.6671 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.29101e-09 l2=4.60042e-06 x=-4.99472e-05 y=-1.31234e-05 z=-2.30155e-06 kx=0.000594828 ky=-7.0912e-05 kz=22.7129 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.74915e-09 l2=1.86776e-06 x=-4.99913e-05 y=0.000107081 z=-9.3795e-07 kx=-0.000775397 ky=-0.000525447 kz=22.8676 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35537e-09 l2=1.87205e-05 x=4.91164e-05 y=1.33303e-05 z=-9.35976e-06 kx=-0.000534848 ky=0.000613176 kz=23.0038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.77744e-09 l2=1.33556e-05 x=4.95521e-05 y=0.000380608 z=-6.67953e-06 kx=0.000399026 ky=0.00111824 kz=22.9148 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.23459e-09 l2=7.8328e-06 x=4.98464e-05 y=0.000472945 z=-3.91695e-06 kx=-2.92258e-05 ky=0.000363476 kz=23.0462 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.91896e-09 l2=8.42782e-06 x=4.98222e-05 y=0.000490184 z=-4.21437e-06 kx=-0.000222452 ky=0.00114429 kz=22.472 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15953e-09 l2=1.9727e-05 x=-4.90175e-05 y=0.000149129 z=-9.86433e-06 kx=-0.000122754 ky=-0.000170486 kz=22.6029 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01256e-09 l2=1.93616e-05 x=-4.90538e-05 y=0.00045008 z=-9.68222e-06 kx=-0.000411413 ky=0.00144645 kz=22.3903 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.15993e-09 l2=2.49603e-05 x=4.84175e-05 y=0.00022013 z=-1.24808e-05 kx=2.47285e-05 ky=7.72338e-05 kz=23.0363 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.57848e-09 l2=4.11766e-06 x=-4.99577e-05 y=-4.89555e-06 z=-2.06127e-06 kx=-6.67955e-05 ky=-0.000839867 kz=22.818 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.09e-09 l2=8.0433e-06 x=4.98378e-05 y=-0.000332195 z=-4.0248e-06 kx=0.00117963 ky=0.000105996 kz=22.5435 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.28769e-09 l2=4.69022e-06 x=-4.99451e-05 y=0.00020091 z=-2.34947e-06 kx=-0.000325183 ky=0.000698506 kz=22.7669 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.14868e-09 l2=1.46525e-05 x=-4.94604e-05 y=-0.000386489 z=-7.32703e-06 kx=-9.69493e-05 ky=-0.00128395 kz=23.2462 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52564e-09 l2=1.30833e-05 x=4.95706e-05 y=0.00038898 z=-6.54063e-06 kx=-0.000833843 ky=0.00149999 kz=23.0884 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.62506e-09 l2=1.62736e-06 x=4.99934e-05 y=-5.36053e-05 z=-8.12538e-07 kx=-0.000897606 ky=-0.00107316 kz=22.9445 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.03067e-09 l2=2.31431e-05 x=-4.86427e-05 y=0.000173458 z=-1.1573e-05 kx=-0.000190395 ky=0.000243801 kz=22.7124 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=7.20497e-09 l2=1.4728e-06 x=4.99946e-05 y=-0.000400299 z=-7.42481e-07 kx=0.00112854 ky=-0.00118048 kz=22.7638 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.32096e-09 l2=2.26099e-05 x=4.87056e-05 y=-0.000461138 z=-1.13047e-05 kx=-0.000442568 ky=-0.00202507 kz=22.6911 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13851e-09 l2=2.24351e-05 x=4.87256e-05 y=-0.000367082 z=-1.12177e-05 kx=-0.000173903 ky=-0.000227264 kz=22.9174 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.57701e-09 l2=2.2668e-05 x=-4.86983e-05 y=-0.000215841 z=-1.13364e-05 kx=-0.000747553 ky=-0.00107748 kz=22.968 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02545e-09 l2=2.28141e-05 x=-4.86819e-05 y=-0.000209814 z=-1.1406e-05 kx=0.00075643 ky=-0.00060536 kz=23.2595 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16328e-09 l2=5.31256e-06 x=4.99294e-05 y=0.000149606 z=-2.65807e-06 kx=0.000546281 ky=0.00145009 kz=22.5195 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.26371e-09 l2=1.61759e-05 x=-4.93417e-05 y=-0.000374061 z=-8.08821e-06 kx=0.000168991 ky=-0.00201196 kz=23.0441 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.58068e-09 l2=1.71414e-05 x=4.926e-05 y=0.000471199 z=-8.57183e-06 kx=0.000145315 ky=0.00143737 kz=23.0458 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=5.36144e-09 l2=2.07055e-06 x=4.99894e-05 y=0.000101929 z=-1.03676e-06 kx=-0.000536779 ky=0.000296762 kz=22.5059 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.05906e-09 l2=4.06549e-05 x=-4.56819e-05 y=0.000288485 z=-2.03275e-05 kx=0.000254974 ky=0.000580288 kz=23.0039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.17341e-09 l2=1.79418e-05 x=-4.91891e-05 y=-5.18685e-05 z=-8.96957e-06 kx=0.000888303 ky=0.000628208 kz=22.7374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.01568e-09 l2=6.93672e-06 x=-4.98798e-05 y=0.000418198 z=-3.46729e-06 kx=0.000947964 ky=0.000577796 kz=22.7208 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56068e-09 l2=4.58625e-06 x=-4.99475e-05 y=0.000332318 z=-2.29232e-06 kx=0.000710664 ky=0.000259768 kz=22.4038 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.65909e-09 l2=9.8721e-06 x=4.9756e-05 y=-0.000201785 z=-4.93634e-06 kx=-0.000487922 ky=-0.000835711 kz=23.2941 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.21134e-09 l2=9.91757e-06 x=4.97535e-05 y=-0.000110345 z=-4.96198e-06 kx=0.000738675 ky=-0.00103858 kz=23.1286 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.0152e-09 l2=4.41436e-05 x=4.4865e-05 y=0.0002345 z=-2.20721e-05 kx=-9.61672e-05 ky=0.000135476 kz=22.8684 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.2042e-09 l2=3.16228e-05 x=-4.74344e-05 y=0.000185077 z=-1.5812e-05 kx=-2.19324e-05 ky=-0.000380153 kz=22.7278 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.56042e-09 l2=1.52502e-05 x=4.94156e-05 y=-0.000156516 z=-7.62367e-06 kx=-0.00104273 ky=-0.000367194 kz=23.2244 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.70219e-09 l2=4.67733e-06 x=4.99452e-05 y=0.000383007 z=-2.34209e-06 kx=0.000937331 ky=7.18632e-05 kz=22.5593 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34584e-09 l2=1.34747e-05 x=4.95441e-05 y=-0.000344148 z=-6.73818e-06 kx=7.7601e-05 ky=-0.00127149 kz=23.2534 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.75984e-09 l2=1.18392e-05 x=4.96486e-05 y=-1.68644e-05 z=-5.92023e-06 kx=-0.000353427 ky=-0.000687728 kz=22.8374 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00949e-09 l2=2.56135e-05 x=4.83327e-05 y=-0.000365512 z=-1.28051e-05 kx=-0.000992051 ky=0.000236737 kz=22.9571 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64955e-09 l2=1.13631e-05 x=-4.96764e-05 y=0.000259475 z=-5.68132e-06 kx=0.000485386 ky=1.29556e-05 kz=22.8644 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13591e-09 l2=2.03448e-05 x=-4.89549e-05 y=0.000477022 z=-1.01708e-05 kx=0.00100633 ky=0.00198412 kz=22.7862 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.60025e-09 l2=8.15983e-06 x=4.98332e-05 y=5.9241e-06 z=-4.08201e-06 kx=0.00060203 ky=-0.00114086 kz=23.192 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.31263e-09 l2=1.23081e-05 x=4.962e-05 y=0.000182586 z=-6.15464e-06 kx=-0.000252545 ky=0.00148994 kz=23.1559 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.37358e-09 l2=1.80809e-05 x=4.91757e-05 y=6.00794e-05 z=-9.04302e-06 kx=0.000895029 ky=-0.000664743 kz=23.1484 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.65373e-09 l2=1.18221e-05 x=4.96492e-05 y=-0.000447484 z=-5.91384e-06 kx=0.00088524 ky=0.000104433 kz=22.3338 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.35688e-09 l2=2.07087e-05 x=4.89166e-05 y=0.000369046 z=-1.03537e-05 kx=-0.000646289 ky=0.000342665 kz=22.7539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04319e-09 l2=1.41359e-05 x=4.9498e-05 y=-0.000363493 z=-7.06823e-06 kx=-0.000111059 ky=-1.12937e-05 kz=22.5279 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.34725e-09 l2=4.78647e-06 x=4.99428e-05 y=0.000355887 z=-2.39327e-06 kx=-0.000295907 ky=0.00185248 kz=23.037 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1636e-09 l2=1.33517e-05 x=-4.95521e-05 y=0.000234997 z=-6.67902e-06 kx=-0.00119014 ky=0.00135994 kz=22.8975 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13921e-09 l2=3.74874e-05 x=4.63538e-05 y=0.000304069 z=-1.87448e-05 kx=0.000221394 ky=0.000306214 kz=22.3011 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.80645e-09 l2=2.2545e-06 x=4.99874e-05 y=-1.36875e-05 z=-1.12745e-06 kx=-0.000553641 ky=0.000560365 kz=23.0476 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25787e-09 l2=2.15358e-05 x=-4.88267e-05 y=-0.000175975 z=-1.07693e-05 kx=-0.000353221 ky=-0.000452101 kz=23.0368 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.82546e-09 l2=8.61018e-06 x=4.98144e-05 y=0.000137729 z=-4.30781e-06 kx=0.000362445 ky=0.000731144 kz=22.3276 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.66274e-09 l2=1.06031e-05 x=4.97181e-05 y=-0.000153348 z=-5.3037e-06 kx=0.000626776 ky=-0.000881086 kz=23.1396 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.73493e-09 l2=5.36119e-06 x=-4.99282e-05 y=0.000443995 z=-2.67949e-06 kx=0.000885541 ky=5.8162e-05 kz=22.3808 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.24693e-09 l2=2.06653e-05 x=4.89206e-05 y=0.000385173 z=-1.03342e-05 kx=0.000432095 ky=0.00164579 kz=22.317 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48961e-09 l2=9.12891e-06 x=-4.97912e-05 y=-9.87309e-05 z=-4.56636e-06 kx=-0.000529123 ky=0.000783444 kz=22.7999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.46324e-09 l2=1.42209e-05 x=4.94922e-05 y=-0.00046957 z=-7.10909e-06 kx=-0.000957774 ky=-0.00206313 kz=22.8758 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.52261e-09 l2=2.1285e-05 x=-4.88545e-05 y=-0.000146104 z=-1.0643e-05 kx=0.000136194 ky=-0.000939896 kz=22.695 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.41115e-09 l2=2.21457e-05 x=-4.87583e-05 y=-0.00042755 z=-1.10751e-05 kx=-0.000728781 ky=-0.00098882 kz=22.6774 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.20244e-09 l2=1.17488e-05 x=4.96536e-05 y=0.000485127 z=-5.8777e-06 kx=0.00101019 ky=0.000906271 kz=22.8119 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.75793e-09 l2=1.99351e-05 x=-4.89965e-05 y=-0.000206674 z=-9.96909e-06 kx=-0.000313902 ky=-0.00145672 kz=22.7798 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.16539e-09 l2=1.84751e-05 x=4.91391e-05 y=-0.000441481 z=-9.23963e-06 kx=0.000699622 ky=-0.00189015 kz=23.0539 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.33068e-09 l2=2.26221e-05 x=-4.87039e-05 y=0.000409261 z=-1.13121e-05 kx=-0.000178614 ky=0.000977534 kz=22.8039 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.59934e-09 l2=1.93979e-05 x=-4.90504e-05 y=-0.00021974 z=-9.70015e-06 kx=-0.000172385 ky=-0.000915221 kz=22.5989 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=4.62486e-08 l2=4.23207e-07 x=4.99996e-05 y=-0.000289605 z=-2.3628e-07 kx=0.000713388 ky=-0.000160716 kz=22.9832 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.01651e-09 l2=3.04975e-05 x=-4.76188e-05 y=-0.000295417 z=-1.52474e-05 kx=0.000860271 ky=-0.00177549 kz=22.6395 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.70696e-09 l2=1.73513e-05 x=-4.92415e-05 y=0.000283948 z=-8.67802e-06 kx=-0.000702579 ky=0.000516773 kz=23.0893 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13569e-09 l2=3.73416e-05 x=-4.6383e-05 y=-5.40085e-05 z=-1.86723e-05 kx=-0.000468679 ky=0.000868839 kz=22.4956 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.04017e-09 l2=2.7365e-05 x=4.80917e-05 y=2.22978e-05 z=-1.36828e-05 kx=-9.88325e-05 ky=0.000245595 kz=22.7825 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.02494e-09 l2=4.51193e-05 x=-4.46222e-05 y=1.07094e-05 z=-2.25589e-05 kx=0.000636782 ky=0.00065444 kz=22.7025 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.05531e-09 l2=1.21134e-05 x=4.96318e-05 y=0.000412557 z=-6.05895e-06 kx=0.000563481 ky=0.000811399 kz=23.3082 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3606e-09 l2=2.13109e-05 x=-4.8851e-05 y=-0.000164649 z=-1.06586e-05 kx=-0.00112981 ky=0.000731132 kz=22.5912 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.3321e-09 l2=4.87861e-06 x=4.99405e-05 y=0.000113765 z=-2.43993e-06 kx=-1.80091e-05 ky=0.000666178 kz=22.3027 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.10282e-09 l2=1.8258e-05 x=4.91596e-05 y=0.000393461 z=-9.12957e-06 kx=1.20615e-05 ky=0.000245364 kz=22.334 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.13098e-09 l2=2.65805e-05 x=-4.82013e-05 y=-0.000174426 z=-1.32915e-05 kx=-0.000297279 ky=-0.000200782 kz=22.7079 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.64172e-09 l2=1.98349e-05 x=-4.90069e-05 y=9.91831e-05 z=-9.91759e-06 kx=0.000318697 ky=-0.000144966 kz=22.4398 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.48959e-09 l2=1.35578e-05 x=-4.95385e-05 y=0.000357688 z=-6.7789e-06 kx=0.000327297 ky=0.000817412 kz=22.4892 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.08562e-09 l2=3.039e-05 x=4.76348e-05 y=-0.000334676 z=-1.51975e-05 kx=0.000907708 ky=-0.000322605 kz=22.401 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.00147e-09 l2=1.37754e-05 x=-4.95235e-05 y=-3.10214e-05 z=-6.88828e-06 kx=0.000188659 ky=-0.000932269 kz=22.8154 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.92177e-09 l2=1.14718e-05 x=-4.96703e-05 y=0.000317043 z=-5.73479e-06 kx=0.000933058 ky=0.00142951 kz=22.5935 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=2.85944e-09 l2=7.8494e-06 x=4.98457e-05 y=0.000383018 z=-3.92815e-06 kx=0.000908109 ky=0.00110959 kz=22.3999 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.00319e-09 l2=3.9837e-05 x=4.58617e-05 y=0.000306023 z=-1.99186e-05 kx=-0.000234809 ky=0.000414328 kz=22.8668 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.25598e-09 l2=9.53276e-06 x=4.97725e-05 y=0.000189243 z=-4.76536e-06 kx=-0.000738126 ky=0.000814702 kz=22.3348 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=3.91645e-09 l2=7.03838e-06 x=4.98761e-05 y=-0.000419324 z=-3.52152e-06 kx=0.000167376 ky=-0.00155182 kz=22.4652 Single_crystal: sample: Warning: x-ray has unexpectedly left the crystal! l1=1.1895e-09 l2=2.54686e-05 x=4.83512e-05 y=0.000483854 z=-1.27356e-05 kx=0.000327882 ky=0.00141076 kz=22.8197 Single_crystal: sample: Error message was repeated 685 times with absorbed x-rays. Warning: 49627 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4784 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 650 times with absorbed x-rays. Warning: 50094 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4672 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 685 times with absorbed x-rays. Warning: 49779 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4911 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 676 times with absorbed x-rays. Warning: 50277 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4636 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Single_crystal: sample: Error message was repeated 692 times with absorbed x-rays. Single_crystal: sample: Error message was repeated 667 times with absorbed x-rays. Warning: 49881 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 50239 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4788 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4835 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: psd0_I=7.95775e-10 psd0_ERR=2.51646e-13 psd0_N=1e+07 "psd0.dat" Single_crystal: sample: Error message was repeated 696 times with absorbed x-rays. Single_crystal: sample: Error message was repeated 700 times with absorbed x-rays. Warning: 50624 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 49924 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4871 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4873 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: psd4pi_I=1.01961e-17 psd4pi_ERR=1.19605e-20 psd4pi_N=995138 "psd4pi.dat" Detector: detector_I=6.85808e-19 detector_ERR=3.09719e-21 detector_N=66588 "psd1.dat" Single_crystal: sample: Error message was repeated 623 times with absorbed x-rays. Warning: 50133 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4781 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Detector: detector2_I=1.85942e-21 detector2_ERR=1.59321e-22 detector2_N=179 "psd2.dat" Single_crystal: sample: Error message was repeated 637 times with absorbed x-rays. Warning: 50104 events were removed in Component[5] detector=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). Warning: 4765 events were removed in Component[7] detector2=PSD_monitor() (negative time, miss next components, rounding errors, Nan, Inf). [n-62-29-31:08558] 9 more processes have sent help message help-mpi-btl-openib.txt / ib port not selected [n-62-29-31:08558] Set MCA parameter "orte_base_help_aggregate" to 0 to see all help / error messages [n-62-29-31:08558] 9 more processes have sent help message help-mpi-btl-openib.txt / error in device init INFO: Placing instr file copy /zhome/89/0/38697/xTESTS/2022-12-01/McXtrace-1.x_CPU_MPICC_1e7/Test_SX/Test_SX.instr in dataset 1